Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado

Detalhes bibliográficos
Autor(a) principal: Bender, Ana Betine Beutinger
Data de Publicação: 2020
Tipo de documento: Tese
Idioma: por
Título da fonte: Biblioteca Digital de Teses e Dissertações do UFSM
Texto Completo: http://repositorio.ufsm.br/handle/1/20765
Resumo: Grape pomace, the winemaking by-product, is characterized by a significant amount of dietary fiber and phenolic compounds. Most of these compounds are associated with the fibrous matrix. Physical modifications, such as micronization, have been used to modify the functionality of dietary fiber by caused by the breakdown of its polymeric constituents. Because it is underused by the wine industry, there is growing interest in its use. Few studies evaluate the effect of incorporation of micronized ingredients in food products as well as their influence on in vitro digestibility. Therefore, the aim of the present study was to evaluate the effect of micronization on the physicochemical properties of dietary fiber from grape pomace in order to enhance the functional properties of an extruded product. The effects of micronization of grape pomace and its fiber concentrate on dietary fiber fractions, physicochemical properties, phenolic compounds, and antioxidant capacity were evaluated. Factorial design with two independent variables (22) – speed and time – was used to determine the best milling conditions to increase the soluble fiber content. The insoluble fiber constituents, such as cellulose and lignin, were partially degraded and the content decreased after milling, resulting in higher soluble fiber content, which demonstrates the compound redistribution. Micronization had a significant effect on reducing the particle size, as evidenced by scanning electron microscopy. FT-IR spectra revealed changes in typical absorption bands of polysaccharides. After milling, powder solubility increased and water holding, oil and cation binding capacities decreased. Furthermore, micronization enhanced phenolic compound extraction, mainly catechin and epicatechin, and the antioxidant capacity evaluated by ABTS and ORAC assays. The results obtained indicate that micronization modifies the dietary fiber composition of grape pomace, increasing possibilities for use as a functional ingredient in the food industry. In this way grape pomace and micronized grape pomace were added to an extruded product. Physicochemical, technological and sensory characteristics, including phenolic and anthocyanin content, antioxidant capacity, and in vitro starch digestibility, were evaluated. The addition of grape pomace influenced the expansion ration, bulk density, and water absorption and solubility indexes. Regarding the composition, total, insoluble and soluble fiber content increased in fortified formulations. The inclusion of grape pomace and micronized grape pomace increased the total phenolic content, total monomeric anthocyanin and, consequently, the antioxidant capacity (ABTS and ORAC assays). The color and flavor attributes had the highest scores at the sensory analysis. The in vitro starch digestibility showed an increased in resistant starch fraction with addition of grape pomace and micronized grape pomace, which had lower glycemic index. The results demonstrate that the extruded products fortified with grape pomace and micronized grape pomace have interesting technological and functional characteristics, and could be considered as promising ingredients for using in the food industry.
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spelling 2021-05-04T13:21:31Z2021-05-04T13:21:31Z2020-01-20http://repositorio.ufsm.br/handle/1/20765Grape pomace, the winemaking by-product, is characterized by a significant amount of dietary fiber and phenolic compounds. Most of these compounds are associated with the fibrous matrix. Physical modifications, such as micronization, have been used to modify the functionality of dietary fiber by caused by the breakdown of its polymeric constituents. Because it is underused by the wine industry, there is growing interest in its use. Few studies evaluate the effect of incorporation of micronized ingredients in food products as well as their influence on in vitro digestibility. Therefore, the aim of the present study was to evaluate the effect of micronization on the physicochemical properties of dietary fiber from grape pomace in order to enhance the functional properties of an extruded product. The effects of micronization of grape pomace and its fiber concentrate on dietary fiber fractions, physicochemical properties, phenolic compounds, and antioxidant capacity were evaluated. Factorial design with two independent variables (22) – speed and time – was used to determine the best milling conditions to increase the soluble fiber content. The insoluble fiber constituents, such as cellulose and lignin, were partially degraded and the content decreased after milling, resulting in higher soluble fiber content, which demonstrates the compound redistribution. Micronization had a significant effect on reducing the particle size, as evidenced by scanning electron microscopy. FT-IR spectra revealed changes in typical absorption bands of polysaccharides. After milling, powder solubility increased and water holding, oil and cation binding capacities decreased. Furthermore, micronization enhanced phenolic compound extraction, mainly catechin and epicatechin, and the antioxidant capacity evaluated by ABTS and ORAC assays. The results obtained indicate that micronization modifies the dietary fiber composition of grape pomace, increasing possibilities for use as a functional ingredient in the food industry. In this way grape pomace and micronized grape pomace were added to an extruded product. Physicochemical, technological and sensory characteristics, including phenolic and anthocyanin content, antioxidant capacity, and in vitro starch digestibility, were evaluated. The addition of grape pomace influenced the expansion ration, bulk density, and water absorption and solubility indexes. Regarding the composition, total, insoluble and soluble fiber content increased in fortified formulations. The inclusion of grape pomace and micronized grape pomace increased the total phenolic content, total monomeric anthocyanin and, consequently, the antioxidant capacity (ABTS and ORAC assays). The color and flavor attributes had the highest scores at the sensory analysis. The in vitro starch digestibility showed an increased in resistant starch fraction with addition of grape pomace and micronized grape pomace, which had lower glycemic index. The results demonstrate that the extruded products fortified with grape pomace and micronized grape pomace have interesting technological and functional characteristics, and could be considered as promising ingredients for using in the food industry.O bagaço de uva, resíduo da vinificação, caracteriza-se por apresentar quantidade significativa de fibra alimentar e compostos fenólicos. Grande parte destes compostos encontra-se associada à matriz fibrosa. Modificações físicas, como a micronização, vêm sendo utilizadas para alterar a funcionalidade da fibra alimentar, através da quebra de seus constituintes poliméricos. Por tratar-se de material subutilizado pela indústria vinícola, há crescente interesse pelo seu aproveitamento. Poucos estudos avaliam o efeito da incorporação dos ingredientes micronizados em produtos alimentícios bem como a influência destes na digestibilidade in vitro. Diante disto, o objetivo do presente estudo foi avaliar o efeito da micronização sobre as características físico-químicas da fibra do bagaço de uva com o intuito de potencializar as propriedades funcionais de um produto extrusado. Foram avaliados os efeitos da micronização do bagaço de uva e do seu concentrado de fibra nas frações de fibra alimentar, propriedades físico-químicas, compostos fenólicos e capacidade antioxidante. Delineamento fatorial com duas variáveis independentes (22) - rotação e tempo - foi utilizado para determinar as melhores condições de moagem para aumentar o teor de fibra solúvel. Os constituintes da fibra insolúvel, como celulose e lignina, foram degradados parcialmente e os teores diminuíram após a moagem, resultando em maior teor de fibra solúvel, o que demonstra a redistribuição dos compostos. A micronização teve efeito significativo na redução do tamanho de partícula, como evidenciado pela microscopia eletrônica de varredura. Os espectros de FT-IR revelaram alterações nas bandas de absorção típicas de polissacarídeos. Após a moagem, a solubilidade dos pós aumentou e as capacidades de retenção de água, ligação ao óleo e a cátions diminuíram. Além disso, a micronização melhorou a extração de compostos fenólicos, principalmente catequina e epicatequina, e a capacidade antioxidante avaliada pelos métodos ABTS e ORAC. Os resultados obtidos indicam que a micronização modifica a composição da fibra alimentar do bagaço de uva, aumentando as possibilidades de uso como ingrediente funcional na indústria de alimentos. Desta forma, o bagaço de uva e o bagaço de uva micronizado foram adicionados a um produto extrusado. Foram avaliadas as características físico-químicas, tecnológicas e sensoriais, incluindo o conteúdo de fenólicos e antocianinas, a capacidade antioxidante e a digestibilidade do amido in vitro. A adição de bagaço influenciou a taxa de expansão, densidade aparente e os índices de absorção e solubilidade em água. Quanto à composição, o teor de fibra alimentar total, insolúvel e solúvel aumentou nas formulações fortificadas. A inclusão de bagaço de uva e bagaço de uva micronizado aumentou o conteúdo de fenólicos totais, antocianinas monoméricas totais e, consequentemente, a capacidade antioxidante (métodos ABTS e ORAC). Os atributos cor e sabor apresentaram os maiores escores na análise sensorial. A digestibilidade do amido in vitro revelou aumento no teor de amido resistente nas formulações contendo bagaço de uva, que apresentaram menor índice glicêmico. Os resultados demonstram que os produtos extrusados fortificados com bagaço de uva e bagaço de uva micronizado apresentam características tecnológicas e funcionais interessantes e mostram-se como ingredientes promissores para utilização na indústria de alimentos.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPESporUniversidade Federal de Santa MariaCentro de Ciências RuraisPrograma de Pós-Graduação em Ciência e Tecnologia dos AlimentosUFSMBrasilCiência e Tecnologia dos AlimentosAttribution-NonCommercial-NoDerivatives 4.0 Internationalhttp://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessExtrusãoMoagem ultrafinaResíduo agroindustrialVitiviniculturaExtrusionUltrafine grindingAgro-industrial by-productsVitivinicultureCNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOSMicronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusadoMicronization as an alternative for valuation of grape pomace: characterization and application in extruded productinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisPenna, Neidi Garciahttp://lattes.cnpq.br/8386196315488275Silva, Leila Picolli daFerrigolo, Fernanda Rodrigues GoulartMonteiro, Sabrina SauthierEmanuelli, TatianaBallus, Cristiano Augustohttp://lattes.cnpq.br/1322840102711871Bender, Ana Betine Beutinger500700000006600600600600600600600600f1dc20fa-80da-4de4-9cc7-7bd2c74e094044643021-0802-4498-98dc-bb33359fb4b86a92a23d-88fe-49b0-82ae-315721820ffe3ce28ac2-88e8-4421-bee2-8acf1fa32d5907f4d475-0e6b-4a3c-ade7-cbb192ad87837457e618-e257-4f1d-b319-f58982632184bc87b329-3330-4d30-a095-d877887dd26creponame:Biblioteca Digital de Teses e Dissertações do UFSMinstname:Universidade Federal de Santa Maria (UFSM)instacron:UFSMORIGINALTES_PPGCTA_2020_BENDER_ANA.pdfTES_PPGCTA_2020_BENDER_ANA.pdfTeseapplication/pdf5805955http://repositorio.ufsm.br/bitstream/1/20765/1/TES_PPGCTA_2020_BENDER_ANA.pdf1f72bcae5caddf4e41a691bb1871d35cMD51CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; 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dc.title.por.fl_str_mv Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
dc.title.alternative.eng.fl_str_mv Micronization as an alternative for valuation of grape pomace: characterization and application in extruded product
title Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
spellingShingle Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
Bender, Ana Betine Beutinger
Extrusão
Moagem ultrafina
Resíduo agroindustrial
Vitivinicultura
Extrusion
Ultrafine grinding
Agro-industrial by-products
Vitiviniculture
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
title_short Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
title_full Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
title_fullStr Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
title_full_unstemmed Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
title_sort Micronização como alternativa para valorização do bagaço de uva: caracterização e aplicação em snack extrusado
author Bender, Ana Betine Beutinger
author_facet Bender, Ana Betine Beutinger
author_role author
dc.contributor.advisor1.fl_str_mv Penna, Neidi Garcia
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/8386196315488275
dc.contributor.advisor-co1.fl_str_mv Silva, Leila Picolli da
dc.contributor.referee1.fl_str_mv Ferrigolo, Fernanda Rodrigues Goulart
dc.contributor.referee2.fl_str_mv Monteiro, Sabrina Sauthier
dc.contributor.referee3.fl_str_mv Emanuelli, Tatiana
dc.contributor.referee4.fl_str_mv Ballus, Cristiano Augusto
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/1322840102711871
dc.contributor.author.fl_str_mv Bender, Ana Betine Beutinger
contributor_str_mv Penna, Neidi Garcia
Silva, Leila Picolli da
Ferrigolo, Fernanda Rodrigues Goulart
Monteiro, Sabrina Sauthier
Emanuelli, Tatiana
Ballus, Cristiano Augusto
dc.subject.por.fl_str_mv Extrusão
Moagem ultrafina
Resíduo agroindustrial
Vitivinicultura
topic Extrusão
Moagem ultrafina
Resíduo agroindustrial
Vitivinicultura
Extrusion
Ultrafine grinding
Agro-industrial by-products
Vitiviniculture
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
dc.subject.eng.fl_str_mv Extrusion
Ultrafine grinding
Agro-industrial by-products
Vitiviniculture
dc.subject.cnpq.fl_str_mv CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
description Grape pomace, the winemaking by-product, is characterized by a significant amount of dietary fiber and phenolic compounds. Most of these compounds are associated with the fibrous matrix. Physical modifications, such as micronization, have been used to modify the functionality of dietary fiber by caused by the breakdown of its polymeric constituents. Because it is underused by the wine industry, there is growing interest in its use. Few studies evaluate the effect of incorporation of micronized ingredients in food products as well as their influence on in vitro digestibility. Therefore, the aim of the present study was to evaluate the effect of micronization on the physicochemical properties of dietary fiber from grape pomace in order to enhance the functional properties of an extruded product. The effects of micronization of grape pomace and its fiber concentrate on dietary fiber fractions, physicochemical properties, phenolic compounds, and antioxidant capacity were evaluated. Factorial design with two independent variables (22) – speed and time – was used to determine the best milling conditions to increase the soluble fiber content. The insoluble fiber constituents, such as cellulose and lignin, were partially degraded and the content decreased after milling, resulting in higher soluble fiber content, which demonstrates the compound redistribution. Micronization had a significant effect on reducing the particle size, as evidenced by scanning electron microscopy. FT-IR spectra revealed changes in typical absorption bands of polysaccharides. After milling, powder solubility increased and water holding, oil and cation binding capacities decreased. Furthermore, micronization enhanced phenolic compound extraction, mainly catechin and epicatechin, and the antioxidant capacity evaluated by ABTS and ORAC assays. The results obtained indicate that micronization modifies the dietary fiber composition of grape pomace, increasing possibilities for use as a functional ingredient in the food industry. In this way grape pomace and micronized grape pomace were added to an extruded product. Physicochemical, technological and sensory characteristics, including phenolic and anthocyanin content, antioxidant capacity, and in vitro starch digestibility, were evaluated. The addition of grape pomace influenced the expansion ration, bulk density, and water absorption and solubility indexes. Regarding the composition, total, insoluble and soluble fiber content increased in fortified formulations. The inclusion of grape pomace and micronized grape pomace increased the total phenolic content, total monomeric anthocyanin and, consequently, the antioxidant capacity (ABTS and ORAC assays). The color and flavor attributes had the highest scores at the sensory analysis. The in vitro starch digestibility showed an increased in resistant starch fraction with addition of grape pomace and micronized grape pomace, which had lower glycemic index. The results demonstrate that the extruded products fortified with grape pomace and micronized grape pomace have interesting technological and functional characteristics, and could be considered as promising ingredients for using in the food industry.
publishDate 2020
dc.date.issued.fl_str_mv 2020-01-20
dc.date.accessioned.fl_str_mv 2021-05-04T13:21:31Z
dc.date.available.fl_str_mv 2021-05-04T13:21:31Z
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Centro de Ciências Rurais
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dc.publisher.initials.fl_str_mv UFSM
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dc.publisher.department.fl_str_mv Ciência e Tecnologia dos Alimentos
publisher.none.fl_str_mv Universidade Federal de Santa Maria
Centro de Ciências Rurais
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MD5
MD5
MD5
repository.name.fl_str_mv Biblioteca Digital de Teses e Dissertações do UFSM - Universidade Federal de Santa Maria (UFSM)
repository.mail.fl_str_mv atendimento.sib@ufsm.br||tedebc@gmail.com
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