Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves

Detalhes bibliográficos
Autor(a) principal: Souza, Sônia Júlia Oliveira de
Data de Publicação: 2021
Outros Autores: Borges, Leonardo Luiz, Fiuza, Tatiana de Sousa, Alves, Suzana Ferreira, Cunha, Luiz Carlos da, Oliveira Neto, Jerônimo Raimundo de, Sá, Stone de, Paula, Joelma Abadia Marciano de, Paula, José Realino de
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Research, Society and Development
Texto Completo: https://rsdjournal.org/index.php/rsd/article/view/14322
Resumo: Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", is popularly used for head, muscle aches, rheumatism and, stomach, uterine, renal and liver disorders. The aims of this study were to investigate the physico-chemical and morphological properties of microencapsulated powder of volatile oil from S. odoratissima leaves, optimize the drying process and verify the influence of drying parameters on microencapsulation by spray-drying. The volatile oils from leaves were extracting by hydrodistillation in a Clevenger type apparatus and analyzed by GC/MS. The emulsions were prepared and spray-dried. Box-Behnken experimental model was used for optimize the effects of drying parameters on the encapsulation responses. The β-caryophyllene content in the microcapsules was determined by HPLC. The results suggest that the best operational conditions for the atomization drying of S. odoratissima volatile oil were inlet temperature of 158°C, feed flow of 0.25L/h and drying nozzle diameter of 0.7mm. These results reveal the technological potential of the microcapsules obtained from S. odoratissima volatile oils.
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spelling Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves Optimización de los parámetros de secado en la microencapsulación de aceite volátil de hojas de Spiranthera odoratissima Otimização dos parâmetros de secagem na microencapsulação do óleo volátil de folhas de Spiranthera odoratissimaMateriais de paredeDesenho de Box-behnkenβ-cariofilenoGC-MS“Manacá”Rutaceae.Wall materialsBox-behnken designβ-caryophylleneGC-MS“Manacá”Rutaceae. Materiales de paredDiseño Box-behnkenβ-cariofilenoGC-MS“Manacá’Rutaceae.Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", is popularly used for head, muscle aches, rheumatism and, stomach, uterine, renal and liver disorders. The aims of this study were to investigate the physico-chemical and morphological properties of microencapsulated powder of volatile oil from S. odoratissima leaves, optimize the drying process and verify the influence of drying parameters on microencapsulation by spray-drying. The volatile oils from leaves were extracting by hydrodistillation in a Clevenger type apparatus and analyzed by GC/MS. The emulsions were prepared and spray-dried. Box-Behnken experimental model was used for optimize the effects of drying parameters on the encapsulation responses. The β-caryophyllene content in the microcapsules was determined by HPLC. The results suggest that the best operational conditions for the atomization drying of S. odoratissima volatile oil were inlet temperature of 158°C, feed flow of 0.25L/h and drying nozzle diameter of 0.7mm. These results reveal the technological potential of the microcapsules obtained from S. odoratissima volatile oils.Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", se usa popularmente para dolores de cabeza, musculares, reumatismo, estomago, útero, renales y trastornos hepáticos. Los objetivos de este estudio fueron investigar las propiedades físico-químicas y morfológicas del polvo microencapsulado de aceite volátil de hojas de S. odoratissima, optimizar el proceso de secado y verificar la influencia de los parámetros de secado en la microencapsulación por atomización. Los aceites volátiles de las hojas se extrajeron por hidrodestilación en un aparato tipo Clevenger y se analizaron por GC / MS. Las emulsiones se prepararon y se secaron por pulverización. Se utilizó el modelo experimental Box-Behnken para optimizar los efectos de los parámetros de secado en las respuestas de encapsulación. El contenido de β-cariofileno en las microcápsulas se determinó mediante HPLC. Los resultados sugieren que las mejores condiciones operativas para el secado por atomización del aceite volátil de S. odoratissima fueron una temperatura de entrada de 158 °C, un flujo de alimentación de 0,25 L / h, un diámetro de boquilla de secado de 0,7 mm. Estos resultados revelan el potencial tecnológico de las microcápsulas obtenidas a partir de aceites volátiles de S. odoratissima.Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", é utilizada popularmente para tratar dores de cabeça, de estômago, doenças musculares, reumatismo, disordens do útero, rins e fígado. Os objetivos deste estudo foram investigar as propriedades físico-químicas e morfológicas do pó microencapsulado do óleo volátil das folhas de S. odoratissima, otimizar o processo de secagem e verificar a influência dos parâmetros de secagem na microencapsulação por spray-dry. Os óleos voláteis das folhas foram extraídos por hidrodestilação em aparelho tipo Clevenger e analisados por CG / EM. As emulsões foram preparadas e secas por pulverização. O modelo experimental Box-Behnken foi utilizado para otimizar os efeitos dos parâmetros de secagem nas respostas de encapsulamento. O conteúdo de β-cariofileno nas microcápsulas foi determinado por HPLC. Os resultados sugerem que as melhores condições operacionais para a secagem por atomização do óleo volátil de S. odoratissima foram temperatura de entrada de 158 °C, vazão de alimentação de 0,25L/ h, diâmetro do bico de secagem de 0,7mm. Esses resultados revelam o potencial tecnológico das microcápsulas obtidas a partir de óleos voláteis de S. odoratissima.Research, Society and Development2021-04-24info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://rsdjournal.org/index.php/rsd/article/view/1432210.33448/rsd-v10i4.14322Research, Society and Development; Vol. 10 No. 4; e57510414322Research, Society and Development; Vol. 10 Núm. 4; e57510414322Research, Society and Development; v. 10 n. 4; e575104143222525-3409reponame:Research, Society and Developmentinstname:Universidade Federal de Itajubá (UNIFEI)instacron:UNIFEIenghttps://rsdjournal.org/index.php/rsd/article/view/14322/13025Copyright (c) 2021 Sônia Júlia Oliveira de Souza; Leonardo Luiz Borges; Tatiana de Sousa Fiuza; Suzana Ferreira Alves; Luiz Carlos da Cunha; Jerônimo Raimundo de Oliveira Neto; Stone de Sá; Joelma Abadia Marciano de Paula; José Realino de Paulahttps://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccessSouza, Sônia Júlia Oliveira deBorges, Leonardo Luiz Fiuza, Tatiana de Sousa Alves, Suzana Ferreira Cunha, Luiz Carlos da Oliveira Neto, Jerônimo Raimundo de Sá, Stone dePaula, Joelma Abadia Marciano de Paula, José Realino de2021-04-25T11:21:26Zoai:ojs.pkp.sfu.ca:article/14322Revistahttps://rsdjournal.org/index.php/rsd/indexPUBhttps://rsdjournal.org/index.php/rsd/oairsd.articles@gmail.com2525-34092525-3409opendoar:2024-01-17T09:35:28.384885Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)false
dc.title.none.fl_str_mv Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
Optimización de los parámetros de secado en la microencapsulación de aceite volátil de hojas de Spiranthera odoratissima
Otimização dos parâmetros de secagem na microencapsulação do óleo volátil de folhas de Spiranthera odoratissima
title Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
spellingShingle Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
Souza, Sônia Júlia Oliveira de
Materiais de parede
Desenho de Box-behnken
β-cariofileno
GC-MS
“Manacá”
Rutaceae.
Wall materials
Box-behnken design
β-caryophyllene
GC-MS
“Manacá”
Rutaceae.
Materiales de pared
Diseño Box-behnken
β-cariofileno
GC-MS
“Manacá’
Rutaceae.
title_short Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
title_full Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
title_fullStr Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
title_full_unstemmed Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
title_sort Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
author Souza, Sônia Júlia Oliveira de
author_facet Souza, Sônia Júlia Oliveira de
Borges, Leonardo Luiz
Fiuza, Tatiana de Sousa
Alves, Suzana Ferreira
Cunha, Luiz Carlos da
Oliveira Neto, Jerônimo Raimundo de
Sá, Stone de
Paula, Joelma Abadia Marciano de
Paula, José Realino de
author_role author
author2 Borges, Leonardo Luiz
Fiuza, Tatiana de Sousa
Alves, Suzana Ferreira
Cunha, Luiz Carlos da
Oliveira Neto, Jerônimo Raimundo de
Sá, Stone de
Paula, Joelma Abadia Marciano de
Paula, José Realino de
author2_role author
author
author
author
author
author
author
author
dc.contributor.author.fl_str_mv Souza, Sônia Júlia Oliveira de
Borges, Leonardo Luiz
Fiuza, Tatiana de Sousa
Alves, Suzana Ferreira
Cunha, Luiz Carlos da
Oliveira Neto, Jerônimo Raimundo de
Sá, Stone de
Paula, Joelma Abadia Marciano de
Paula, José Realino de
dc.subject.por.fl_str_mv Materiais de parede
Desenho de Box-behnken
β-cariofileno
GC-MS
“Manacá”
Rutaceae.
Wall materials
Box-behnken design
β-caryophyllene
GC-MS
“Manacá”
Rutaceae.
Materiales de pared
Diseño Box-behnken
β-cariofileno
GC-MS
“Manacá’
Rutaceae.
topic Materiais de parede
Desenho de Box-behnken
β-cariofileno
GC-MS
“Manacá”
Rutaceae.
Wall materials
Box-behnken design
β-caryophyllene
GC-MS
“Manacá”
Rutaceae.
Materiales de pared
Diseño Box-behnken
β-cariofileno
GC-MS
“Manacá’
Rutaceae.
description Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", is popularly used for head, muscle aches, rheumatism and, stomach, uterine, renal and liver disorders. The aims of this study were to investigate the physico-chemical and morphological properties of microencapsulated powder of volatile oil from S. odoratissima leaves, optimize the drying process and verify the influence of drying parameters on microencapsulation by spray-drying. The volatile oils from leaves were extracting by hydrodistillation in a Clevenger type apparatus and analyzed by GC/MS. The emulsions were prepared and spray-dried. Box-Behnken experimental model was used for optimize the effects of drying parameters on the encapsulation responses. The β-caryophyllene content in the microcapsules was determined by HPLC. The results suggest that the best operational conditions for the atomization drying of S. odoratissima volatile oil were inlet temperature of 158°C, feed flow of 0.25L/h and drying nozzle diameter of 0.7mm. These results reveal the technological potential of the microcapsules obtained from S. odoratissima volatile oils.
publishDate 2021
dc.date.none.fl_str_mv 2021-04-24
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://rsdjournal.org/index.php/rsd/article/view/14322
10.33448/rsd-v10i4.14322
url https://rsdjournal.org/index.php/rsd/article/view/14322
identifier_str_mv 10.33448/rsd-v10i4.14322
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv https://rsdjournal.org/index.php/rsd/article/view/14322/13025
dc.rights.driver.fl_str_mv https://creativecommons.org/licenses/by/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv https://creativecommons.org/licenses/by/4.0
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Research, Society and Development
publisher.none.fl_str_mv Research, Society and Development
dc.source.none.fl_str_mv Research, Society and Development; Vol. 10 No. 4; e57510414322
Research, Society and Development; Vol. 10 Núm. 4; e57510414322
Research, Society and Development; v. 10 n. 4; e57510414322
2525-3409
reponame:Research, Society and Development
instname:Universidade Federal de Itajubá (UNIFEI)
instacron:UNIFEI
instname_str Universidade Federal de Itajubá (UNIFEI)
instacron_str UNIFEI
institution UNIFEI
reponame_str Research, Society and Development
collection Research, Society and Development
repository.name.fl_str_mv Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)
repository.mail.fl_str_mv rsd.articles@gmail.com
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