Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves
Autor(a) principal: | |
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Data de Publicação: | 2021 |
Outros Autores: | , , , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Research, Society and Development |
Texto Completo: | https://rsdjournal.org/index.php/rsd/article/view/14322 |
Resumo: | Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", is popularly used for head, muscle aches, rheumatism and, stomach, uterine, renal and liver disorders. The aims of this study were to investigate the physico-chemical and morphological properties of microencapsulated powder of volatile oil from S. odoratissima leaves, optimize the drying process and verify the influence of drying parameters on microencapsulation by spray-drying. The volatile oils from leaves were extracting by hydrodistillation in a Clevenger type apparatus and analyzed by GC/MS. The emulsions were prepared and spray-dried. Box-Behnken experimental model was used for optimize the effects of drying parameters on the encapsulation responses. The β-caryophyllene content in the microcapsules was determined by HPLC. The results suggest that the best operational conditions for the atomization drying of S. odoratissima volatile oil were inlet temperature of 158°C, feed flow of 0.25L/h and drying nozzle diameter of 0.7mm. These results reveal the technological potential of the microcapsules obtained from S. odoratissima volatile oils. |
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Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves Optimización de los parámetros de secado en la microencapsulación de aceite volátil de hojas de Spiranthera odoratissima Otimização dos parâmetros de secagem na microencapsulação do óleo volátil de folhas de Spiranthera odoratissimaMateriais de paredeDesenho de Box-behnkenβ-cariofilenoGC-MS“Manacá”Rutaceae.Wall materialsBox-behnken designβ-caryophylleneGC-MS“Manacá”Rutaceae. Materiales de paredDiseño Box-behnkenβ-cariofilenoGC-MS“Manacá’Rutaceae.Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", is popularly used for head, muscle aches, rheumatism and, stomach, uterine, renal and liver disorders. The aims of this study were to investigate the physico-chemical and morphological properties of microencapsulated powder of volatile oil from S. odoratissima leaves, optimize the drying process and verify the influence of drying parameters on microencapsulation by spray-drying. The volatile oils from leaves were extracting by hydrodistillation in a Clevenger type apparatus and analyzed by GC/MS. The emulsions were prepared and spray-dried. Box-Behnken experimental model was used for optimize the effects of drying parameters on the encapsulation responses. The β-caryophyllene content in the microcapsules was determined by HPLC. The results suggest that the best operational conditions for the atomization drying of S. odoratissima volatile oil were inlet temperature of 158°C, feed flow of 0.25L/h and drying nozzle diameter of 0.7mm. These results reveal the technological potential of the microcapsules obtained from S. odoratissima volatile oils.Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", se usa popularmente para dolores de cabeza, musculares, reumatismo, estomago, útero, renales y trastornos hepáticos. Los objetivos de este estudio fueron investigar las propiedades físico-químicas y morfológicas del polvo microencapsulado de aceite volátil de hojas de S. odoratissima, optimizar el proceso de secado y verificar la influencia de los parámetros de secado en la microencapsulación por atomización. Los aceites volátiles de las hojas se extrajeron por hidrodestilación en un aparato tipo Clevenger y se analizaron por GC / MS. Las emulsiones se prepararon y se secaron por pulverización. Se utilizó el modelo experimental Box-Behnken para optimizar los efectos de los parámetros de secado en las respuestas de encapsulación. El contenido de β-cariofileno en las microcápsulas se determinó mediante HPLC. Los resultados sugieren que las mejores condiciones operativas para el secado por atomización del aceite volátil de S. odoratissima fueron una temperatura de entrada de 158 °C, un flujo de alimentación de 0,25 L / h, un diámetro de boquilla de secado de 0,7 mm. Estos resultados revelan el potencial tecnológico de las microcápsulas obtenidas a partir de aceites volátiles de S. odoratissima.Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", é utilizada popularmente para tratar dores de cabeça, de estômago, doenças musculares, reumatismo, disordens do útero, rins e fígado. Os objetivos deste estudo foram investigar as propriedades físico-químicas e morfológicas do pó microencapsulado do óleo volátil das folhas de S. odoratissima, otimizar o processo de secagem e verificar a influência dos parâmetros de secagem na microencapsulação por spray-dry. Os óleos voláteis das folhas foram extraídos por hidrodestilação em aparelho tipo Clevenger e analisados por CG / EM. As emulsões foram preparadas e secas por pulverização. O modelo experimental Box-Behnken foi utilizado para otimizar os efeitos dos parâmetros de secagem nas respostas de encapsulamento. O conteúdo de β-cariofileno nas microcápsulas foi determinado por HPLC. Os resultados sugerem que as melhores condições operacionais para a secagem por atomização do óleo volátil de S. odoratissima foram temperatura de entrada de 158 °C, vazão de alimentação de 0,25L/ h, diâmetro do bico de secagem de 0,7mm. Esses resultados revelam o potencial tecnológico das microcápsulas obtidas a partir de óleos voláteis de S. odoratissima.Research, Society and Development2021-04-24info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://rsdjournal.org/index.php/rsd/article/view/1432210.33448/rsd-v10i4.14322Research, Society and Development; Vol. 10 No. 4; e57510414322Research, Society and Development; Vol. 10 Núm. 4; e57510414322Research, Society and Development; v. 10 n. 4; e575104143222525-3409reponame:Research, Society and Developmentinstname:Universidade Federal de Itajubá (UNIFEI)instacron:UNIFEIenghttps://rsdjournal.org/index.php/rsd/article/view/14322/13025Copyright (c) 2021 Sônia Júlia Oliveira de Souza; Leonardo Luiz Borges; Tatiana de Sousa Fiuza; Suzana Ferreira Alves; Luiz Carlos da Cunha; Jerônimo Raimundo de Oliveira Neto; Stone de Sá; Joelma Abadia Marciano de Paula; José Realino de Paulahttps://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccessSouza, Sônia Júlia Oliveira deBorges, Leonardo Luiz Fiuza, Tatiana de Sousa Alves, Suzana Ferreira Cunha, Luiz Carlos da Oliveira Neto, Jerônimo Raimundo de Sá, Stone dePaula, Joelma Abadia Marciano de Paula, José Realino de2021-04-25T11:21:26Zoai:ojs.pkp.sfu.ca:article/14322Revistahttps://rsdjournal.org/index.php/rsd/indexPUBhttps://rsdjournal.org/index.php/rsd/oairsd.articles@gmail.com2525-34092525-3409opendoar:2024-01-17T09:35:28.384885Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)false |
dc.title.none.fl_str_mv |
Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves Optimización de los parámetros de secado en la microencapsulación de aceite volátil de hojas de Spiranthera odoratissima Otimização dos parâmetros de secagem na microencapsulação do óleo volátil de folhas de Spiranthera odoratissima |
title |
Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves |
spellingShingle |
Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves Souza, Sônia Júlia Oliveira de Materiais de parede Desenho de Box-behnken β-cariofileno GC-MS “Manacá” Rutaceae. Wall materials Box-behnken design β-caryophyllene GC-MS “Manacá” Rutaceae. Materiales de pared Diseño Box-behnken β-cariofileno GC-MS “Manacá’ Rutaceae. |
title_short |
Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves |
title_full |
Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves |
title_fullStr |
Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves |
title_full_unstemmed |
Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves |
title_sort |
Optimization of drying parameters in the microencapsulation of volatile oil from Spiranthera odoratissima leaves |
author |
Souza, Sônia Júlia Oliveira de |
author_facet |
Souza, Sônia Júlia Oliveira de Borges, Leonardo Luiz Fiuza, Tatiana de Sousa Alves, Suzana Ferreira Cunha, Luiz Carlos da Oliveira Neto, Jerônimo Raimundo de Sá, Stone de Paula, Joelma Abadia Marciano de Paula, José Realino de |
author_role |
author |
author2 |
Borges, Leonardo Luiz Fiuza, Tatiana de Sousa Alves, Suzana Ferreira Cunha, Luiz Carlos da Oliveira Neto, Jerônimo Raimundo de Sá, Stone de Paula, Joelma Abadia Marciano de Paula, José Realino de |
author2_role |
author author author author author author author author |
dc.contributor.author.fl_str_mv |
Souza, Sônia Júlia Oliveira de Borges, Leonardo Luiz Fiuza, Tatiana de Sousa Alves, Suzana Ferreira Cunha, Luiz Carlos da Oliveira Neto, Jerônimo Raimundo de Sá, Stone de Paula, Joelma Abadia Marciano de Paula, José Realino de |
dc.subject.por.fl_str_mv |
Materiais de parede Desenho de Box-behnken β-cariofileno GC-MS “Manacá” Rutaceae. Wall materials Box-behnken design β-caryophyllene GC-MS “Manacá” Rutaceae. Materiales de pared Diseño Box-behnken β-cariofileno GC-MS “Manacá’ Rutaceae. |
topic |
Materiais de parede Desenho de Box-behnken β-cariofileno GC-MS “Manacá” Rutaceae. Wall materials Box-behnken design β-caryophyllene GC-MS “Manacá” Rutaceae. Materiales de pared Diseño Box-behnken β-cariofileno GC-MS “Manacá’ Rutaceae. |
description |
Spiranthera odoratissima A. St.-Hil. (Rutaceae), "manacá", is popularly used for head, muscle aches, rheumatism and, stomach, uterine, renal and liver disorders. The aims of this study were to investigate the physico-chemical and morphological properties of microencapsulated powder of volatile oil from S. odoratissima leaves, optimize the drying process and verify the influence of drying parameters on microencapsulation by spray-drying. The volatile oils from leaves were extracting by hydrodistillation in a Clevenger type apparatus and analyzed by GC/MS. The emulsions were prepared and spray-dried. Box-Behnken experimental model was used for optimize the effects of drying parameters on the encapsulation responses. The β-caryophyllene content in the microcapsules was determined by HPLC. The results suggest that the best operational conditions for the atomization drying of S. odoratissima volatile oil were inlet temperature of 158°C, feed flow of 0.25L/h and drying nozzle diameter of 0.7mm. These results reveal the technological potential of the microcapsules obtained from S. odoratissima volatile oils. |
publishDate |
2021 |
dc.date.none.fl_str_mv |
2021-04-24 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
https://rsdjournal.org/index.php/rsd/article/view/14322 10.33448/rsd-v10i4.14322 |
url |
https://rsdjournal.org/index.php/rsd/article/view/14322 |
identifier_str_mv |
10.33448/rsd-v10i4.14322 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
https://rsdjournal.org/index.php/rsd/article/view/14322/13025 |
dc.rights.driver.fl_str_mv |
https://creativecommons.org/licenses/by/4.0 info:eu-repo/semantics/openAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by/4.0 |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Research, Society and Development |
publisher.none.fl_str_mv |
Research, Society and Development |
dc.source.none.fl_str_mv |
Research, Society and Development; Vol. 10 No. 4; e57510414322 Research, Society and Development; Vol. 10 Núm. 4; e57510414322 Research, Society and Development; v. 10 n. 4; e57510414322 2525-3409 reponame:Research, Society and Development instname:Universidade Federal de Itajubá (UNIFEI) instacron:UNIFEI |
instname_str |
Universidade Federal de Itajubá (UNIFEI) |
instacron_str |
UNIFEI |
institution |
UNIFEI |
reponame_str |
Research, Society and Development |
collection |
Research, Society and Development |
repository.name.fl_str_mv |
Research, Society and Development - Universidade Federal de Itajubá (UNIFEI) |
repository.mail.fl_str_mv |
rsd.articles@gmail.com |
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1797052747947704320 |