Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement
| Autor(a) principal: | |
|---|---|
| Data de Publicação: | 2022 |
| Outros Autores: | , , , , , , |
| Tipo de documento: | Artigo |
| Idioma: | por |
| Título da fonte: | Research, Society and Development |
| Texto Completo: | https://rsdjournal.org/index.php/rsd/article/view/30021 |
Resumo: | Scientific and technological advances in the development of bone cements have been undergoing changes in order to obtain properties that are suitable for specific applications. The incorporation of other materials such as chitosan, collagen, oxides, polyethylene glycol, among others, which replace or even incorporate characteristics not present, are well explored, however, the influence of the processing of ceramic powders has been little studied. In this sense, the present work obtained the brushite/SrO/chitosan bone cement through the dissolution/precipitation method, using a mixture of wollastonite/strontium powder applied the methods of removing moisture by oven and desiccator. The samples were characterized through the analysis of curing and setting time, compressive strength, X-ray diffraction (XRD) and optical microscopy (OM). The results showed that the moisture removal method promotes variation of phases formed in the cements, as observed in the XRD, generating an improvement in the compressive strength. The temperature and time of the cements showed a reduction during their curing for the MPC samples. The microscopic analysis showed that the moisture removal method promoted greater porosity in the internal structure of the cement, which can provide an improvement in its compatibility with the applied bone region. |
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Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cementInfluencia del procesamiento poscerámico en la síntesis de cemento óseo de brushita/SrO/QuitosanoInfluência do beneficiamento de pós cerâmicos na síntese de cimento ósseo de brushita/SrO/quitosanaCemento óseoBrushitaEstroncioQuitosanoProcesandoEnseñanza en materiales.Cimento ósseoBrushitaEstrôncioQuitosanaBeneficiamentoEnsino em materiais.Bone cementBrushiteStrontiumChitosanProcessingMaterials teaching.Scientific and technological advances in the development of bone cements have been undergoing changes in order to obtain properties that are suitable for specific applications. The incorporation of other materials such as chitosan, collagen, oxides, polyethylene glycol, among others, which replace or even incorporate characteristics not present, are well explored, however, the influence of the processing of ceramic powders has been little studied. In this sense, the present work obtained the brushite/SrO/chitosan bone cement through the dissolution/precipitation method, using a mixture of wollastonite/strontium powder applied the methods of removing moisture by oven and desiccator. The samples were characterized through the analysis of curing and setting time, compressive strength, X-ray diffraction (XRD) and optical microscopy (OM). The results showed that the moisture removal method promotes variation of phases formed in the cements, as observed in the XRD, generating an improvement in the compressive strength. The temperature and time of the cements showed a reduction during their curing for the MPC samples. The microscopic analysis showed that the moisture removal method promoted greater porosity in the internal structure of the cement, which can provide an improvement in its compatibility with the applied bone region.Los avances científicos y tecnológicos en el desarrollo de cementos óseos han ido cambiando con el fin de obtener propiedades adecuadas para aplicaciones específicas. La incorporación de otros materiales como quitosano, colágeno, óxidos, polietilenglicol, entre otros, que reemplacen o incluso incorporen características no presentes, está bien explorada, sin embargo, la influencia del procesamiento de los polvos cerámicos ha sido poco estudiada. En este sentido, el presente trabajo obtuvo el cemento óseo de brushita/SrO/quitosano a través del método de disolución/precipitación, utilizando una mezcla de polvo de wollastonita/estroncio aplicado los métodos de remoción de humedad por horno y desecador. Las muestras se caracterizaron mediante análisis de tiempo de curado y fraguado, resistencia a la compresión, difracción de rayos X (XRD) y microscopía óptica (OM). Los resultados mostraron que el método de remoción de humedad promueve la variación de fases formadas en los cementos, como se observa en la DRX, generando una mejora en la resistencia a la compresión. La temperatura y el tiempo de los cementos mostraron una reducción durante su curado para las muestras de MPC. El análisis microscópico mostró que el método de eliminación de humedad promovió una mayor porosidad en la estructura interna del cemento, lo que puede proporcionar una mejora en su compatibilidad con la región ósea aplicada.O avanço científico e tecnológico para desenvolvimento de cimentos ósseos, vem sofrendo modificações, de modo a obter propriedades que se adéquem para aplicações específicas. A incorporação de outros materiais tais como quitosana, colágeno, óxidos, polietilenoglicol, entre outros, que substituam ou até mesmo incorporem características não presentes, são bem exploradas, entretanto, a influência do beneficiamento dos pós cerâmicos, vem sendo pouco estudadas. Neste sentido, o presente trabalho obteve o cimento ósseo de brushita/SrO/quitosana através do método de dissolução/precipitação, utilizando uma mistura de pó wollastonita/estrôncio aplicado os métodos de remoção de umidade por estufa e dessecador. As amostras foram caracterizadas através da análise do tempo de cura e de pega, resistência a compressão, difração de raios X (DRX) e microscopia ótica (MO). Os resultados mostraram que o método de remoção de umidade, promove variação de fases formadas nos cimentos, conforme observado no DRX, gerando uma melhora na resistência compressiva. A temperatura e tempo dos cimentos apresentaram redução durante sua cura para as amostras MPC. A análise microscópica mostrou que o método de remoção da umidade, promoveu uma maior porosidade na estrutura interna do cimento, o que pode proporcionar uma melhora em sua compatibilidade a região óssea aplicada.Research, Society and Development2022-05-30info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://rsdjournal.org/index.php/rsd/article/view/3002110.33448/rsd-v11i7.30021Research, Society and Development; Vol. 11 No. 7; e43711730021Research, Society and Development; Vol. 11 Núm. 7; e43711730021Research, Society and Development; v. 11 n. 7; e437117300212525-3409reponame:Research, Society and Developmentinstname:Universidade Federal de Itajubá (UNIFEI)instacron:UNIFEIporhttps://rsdjournal.org/index.php/rsd/article/view/30021/26032Copyright (c) 2022 Matheus Araújo Santos; Geovanna Vitória da Silva Gonçalves; Eunice Paloma Nascimento Lima; Márcio José Batista Cardoso; Wladymyr Jefferson Bacalhau de Sousa; João Emídio da Silva Neto; Klaidson Antonio Sousa Farias; Marcus Vinicius Lia Fookhttps://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccessSantos, Matheus Araújo Gonçalves, Geovanna Vitória da Silva Lima, Eunice Paloma Nascimento Cardoso, Márcio José Batista Sousa, Wladymyr Jefferson Bacalhau de Silva Neto, João Emídio da Farias, Klaidson Antonio Sousa Fook, Marcus Vinicius Lia 2022-06-06T15:12:05Zoai:ojs.pkp.sfu.ca:article/30021Revistahttps://rsdjournal.org/index.php/rsd/indexPUBhttps://rsdjournal.org/index.php/rsd/oairsd.articles@gmail.com2525-34092525-3409opendoar:2024-01-17T09:46:55.479813Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)false |
| dc.title.none.fl_str_mv |
Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement Influencia del procesamiento poscerámico en la síntesis de cemento óseo de brushita/SrO/Quitosano Influência do beneficiamento de pós cerâmicos na síntese de cimento ósseo de brushita/SrO/quitosana |
| title |
Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement |
| spellingShingle |
Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement Santos, Matheus Araújo Cemento óseo Brushita Estroncio Quitosano Procesando Enseñanza en materiales. Cimento ósseo Brushita Estrôncio Quitosana Beneficiamento Ensino em materiais. Bone cement Brushite Strontium Chitosan Processing Materials teaching. |
| title_short |
Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement |
| title_full |
Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement |
| title_fullStr |
Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement |
| title_full_unstemmed |
Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement |
| title_sort |
Influence of post-ceramic processing on the synthesis of brushite/SrO/chitosan bone cement |
| author |
Santos, Matheus Araújo |
| author_facet |
Santos, Matheus Araújo Gonçalves, Geovanna Vitória da Silva Lima, Eunice Paloma Nascimento Cardoso, Márcio José Batista Sousa, Wladymyr Jefferson Bacalhau de Silva Neto, João Emídio da Farias, Klaidson Antonio Sousa Fook, Marcus Vinicius Lia |
| author_role |
author |
| author2 |
Gonçalves, Geovanna Vitória da Silva Lima, Eunice Paloma Nascimento Cardoso, Márcio José Batista Sousa, Wladymyr Jefferson Bacalhau de Silva Neto, João Emídio da Farias, Klaidson Antonio Sousa Fook, Marcus Vinicius Lia |
| author2_role |
author author author author author author author |
| dc.contributor.author.fl_str_mv |
Santos, Matheus Araújo Gonçalves, Geovanna Vitória da Silva Lima, Eunice Paloma Nascimento Cardoso, Márcio José Batista Sousa, Wladymyr Jefferson Bacalhau de Silva Neto, João Emídio da Farias, Klaidson Antonio Sousa Fook, Marcus Vinicius Lia |
| dc.subject.por.fl_str_mv |
Cemento óseo Brushita Estroncio Quitosano Procesando Enseñanza en materiales. Cimento ósseo Brushita Estrôncio Quitosana Beneficiamento Ensino em materiais. Bone cement Brushite Strontium Chitosan Processing Materials teaching. |
| topic |
Cemento óseo Brushita Estroncio Quitosano Procesando Enseñanza en materiales. Cimento ósseo Brushita Estrôncio Quitosana Beneficiamento Ensino em materiais. Bone cement Brushite Strontium Chitosan Processing Materials teaching. |
| description |
Scientific and technological advances in the development of bone cements have been undergoing changes in order to obtain properties that are suitable for specific applications. The incorporation of other materials such as chitosan, collagen, oxides, polyethylene glycol, among others, which replace or even incorporate characteristics not present, are well explored, however, the influence of the processing of ceramic powders has been little studied. In this sense, the present work obtained the brushite/SrO/chitosan bone cement through the dissolution/precipitation method, using a mixture of wollastonite/strontium powder applied the methods of removing moisture by oven and desiccator. The samples were characterized through the analysis of curing and setting time, compressive strength, X-ray diffraction (XRD) and optical microscopy (OM). The results showed that the moisture removal method promotes variation of phases formed in the cements, as observed in the XRD, generating an improvement in the compressive strength. The temperature and time of the cements showed a reduction during their curing for the MPC samples. The microscopic analysis showed that the moisture removal method promoted greater porosity in the internal structure of the cement, which can provide an improvement in its compatibility with the applied bone region. |
| publishDate |
2022 |
| dc.date.none.fl_str_mv |
2022-05-30 |
| dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
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article |
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publishedVersion |
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https://rsdjournal.org/index.php/rsd/article/view/30021 10.33448/rsd-v11i7.30021 |
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https://rsdjournal.org/index.php/rsd/article/view/30021 |
| identifier_str_mv |
10.33448/rsd-v11i7.30021 |
| dc.language.iso.fl_str_mv |
por |
| language |
por |
| dc.relation.none.fl_str_mv |
https://rsdjournal.org/index.php/rsd/article/view/30021/26032 |
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https://creativecommons.org/licenses/by/4.0 info:eu-repo/semantics/openAccess |
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https://creativecommons.org/licenses/by/4.0 |
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openAccess |
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application/pdf |
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Research, Society and Development |
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Research, Society and Development |
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Research, Society and Development; Vol. 11 No. 7; e43711730021 Research, Society and Development; Vol. 11 Núm. 7; e43711730021 Research, Society and Development; v. 11 n. 7; e43711730021 2525-3409 reponame:Research, Society and Development instname:Universidade Federal de Itajubá (UNIFEI) instacron:UNIFEI |
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Universidade Federal de Itajubá (UNIFEI) |
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UNIFEI |
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Research, Society and Development |
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Research, Society and Development |
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Research, Society and Development - Universidade Federal de Itajubá (UNIFEI) |
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