Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará

Detalhes bibliográficos
Autor(a) principal: Nojosa, Antônia Clarycy Barros
Data de Publicação: 2019
Outros Autores: Sampaio, Caroline de Góes, Firmino, Eduardo da Silva, Guerra, Marcelo Henrique Freitas Saraiva, Saldanha, Gabriela Clemente Brito, Vasconcelos, Ana Karine Portela
Tipo de documento: Artigo
Idioma: por
Título da fonte: Research, Society and Development
Texto Completo: https://rsdjournal.org/index.php/rsd/article/view/1440
Resumo: As technology advances, chemical analysis laboratories use statistical techniques to demonstrate the accuracy and precision of analytical methods. To make comparisons between the data obtained from an analysis, Statistical Process Control (CEP) can be used, which is a technique widely used in industry to understand and improve process performance through statistical data processing. Control charts are CEP graphic methods that enable continuous control of analytical processes and allow evaluations and possible optimization of assays. The objective of this study is to use the Statistical Process Control (CEP), the control chart, to evaluate the statistical stability of the spectrophotometer used in the application of the Nimodipino analytical methodology validation technique, using data from the absorbance study of this drug, being the tests performed by students contributing to a learning of work activities. With this study it can be verified that the use of the control chart generates an adequate monitoring to evaluate data fluctuations and to carry out studies of the same, being able to be taught to the students and applied in practical classes accompaniments. It can also be demonstrated that the Minitab 17 program assists quickly in the construction of control charts, obtaining real-time analysis results. This program can be used in other laboratories of the Federal Institute of Ceará for statistical control of analyzes with support for student learning.
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spelling Utilization of statistical process control in an experimental activity at the Federal Institute of CearáUtilización del control estadístico de procesos en una actividad experimental en el Instituto Federal de CearáUtilização de controle estatístico de processo em uma atividade experimental no Instituto Federal do CearáLaboratórioCarta de ControleNimodipinoAprendizagem.LaboratorioCarta de ControlNimodipinaEl aprendizaje.LaboratoryControl ChartNimodipineLearning.As technology advances, chemical analysis laboratories use statistical techniques to demonstrate the accuracy and precision of analytical methods. To make comparisons between the data obtained from an analysis, Statistical Process Control (CEP) can be used, which is a technique widely used in industry to understand and improve process performance through statistical data processing. Control charts are CEP graphic methods that enable continuous control of analytical processes and allow evaluations and possible optimization of assays. The objective of this study is to use the Statistical Process Control (CEP), the control chart, to evaluate the statistical stability of the spectrophotometer used in the application of the Nimodipino analytical methodology validation technique, using data from the absorbance study of this drug, being the tests performed by students contributing to a learning of work activities. With this study it can be verified that the use of the control chart generates an adequate monitoring to evaluate data fluctuations and to carry out studies of the same, being able to be taught to the students and applied in practical classes accompaniments. It can also be demonstrated that the Minitab 17 program assists quickly in the construction of control charts, obtaining real-time analysis results. This program can be used in other laboratories of the Federal Institute of Ceará for statistical control of analyzes with support for student learning.A medida que avanza la tecnología, los laboratorios de análisis químicos utilizan técnicas estadísticas para demostrar la exactitud y precisión de los métodos analíticos. Para hacer comparaciones entre los datos obtenidos de un análisis, se puede utilizar el Control Estadístico de Procesos (CEP), que es una técnica ampliamente utilizada en la industria para comprender y mejorar el rendimiento del proceso a través del procesamiento de datos estadísticos. Los gráficos de control son métodos gráficos de CEP que permiten el control continuo de los procesos analíticos y permiten evaluaciones y una posible optimización de los ensayos. El objetivo de este estudio es utilizar el Control Estadístico de Procesos (CEP), el cuadro de control, para evaluar la estabilidad estadística del espectrofotómetro utilizado en la aplicación de la técnica de validación de metodología analítica Nimodipino, utilizando datos del estudio de absorbancia de este medicamento. siendo las pruebas realizadas por los alumnos que contribuyen al aprendizaje de las actividades laborales. Con este estudio se puede verificar que el uso del cuadro de control genera un monitoreo adecuado para evaluar las fluctuaciones de datos y realizar estudios de los mismos, pudiendo ser enseñado a los alumnos y aplicado en clases prácticas de acompañamiento. También se puede demostrar que el programa Minitab 17 ayuda rápidamente en la construcción de gráficos de control, obteniendo resultados de análisis en tiempo real. Este programa puede utilizarse en otros laboratorios del Instituto Federal de Ceará para el control estadístico de análisis con apoyo para el aprendizaje de los estudiantes.Com o avanço da tecnologia, os laboratórios de análises químicas utilizam-se de técnicas estatísticas para demonstrar a precisão e exatidão dos métodos analíticos. Para realizar comparações entre os dados obtidos de uma análise, pode-se utilizar o Controle Estatístico de Processo (CEP) que consiste em uma técnica muito utilizada na indústria para entender e melhorar o desempenho dos processos, através de tratamento estatístico de dados. As cartas de controle são métodos gráficos do CEP que possibilitam um controle contínuo dos processos analíticos e permitem avaliações e possível otimização dos ensaios. O objetivo desse estudo é utilizar o Controle Estatístico de Processo (CEP), a carta de controle, para avaliar a estabilidade estatística do espectrofotômetro utilizado na aplicação da técnica de validação de metodologia analítica do medicamento Nimodipino, utilizando dados do estudo de absorbância desse fármaco, sendo os testes realizados por alunos contribuindo para uma aprendizagem das atividades laborais. Com esse estudo pode-se verificar que a utilização da carta de controle gera um monitoramento adequado para avaliar oscilações de dados e realizar estudos dos mesmos, podendo ser ensinada para os alunos e aplicada em acompanhamentos de aulas práticas. Também pode-se demonstrar que o programa Minitab 17 auxilia de forma rápida na construção das cartas de controle, obtendo resultados em tempo real das análises. Esse programa pode ser utilizado em outros laboratórios do Instituto Federal do Ceará para controle estatístico das análises com apoio para a aprendizagem dos alunos.Research, Society and Development2019-08-24info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://rsdjournal.org/index.php/rsd/article/view/144010.33448/rsd-v8i11.1440Research, Society and Development; Vol. 8 No. 11; e108111440Research, Society and Development; Vol. 8 Núm. 11; e108111440Research, Society and Development; v. 8 n. 11; e1081114402525-3409reponame:Research, Society and Developmentinstname:Universidade Federal de Itajubá (UNIFEI)instacron:UNIFEIporhttps://rsdjournal.org/index.php/rsd/article/view/1440/1140Copyright (c) 2019 Antônia Clarycy Barros Nojosa, Caroline de Góes Sampaio, Eduardo da Silva Firmino, Marcelo Henrique Freitas Saraiva Guerra, Gabriela Clementino Brito Saldanha, Ana Karine Portela Vasconcelosinfo:eu-repo/semantics/openAccessNojosa, Antônia Clarycy BarrosSampaio, Caroline de GóesFirmino, Eduardo da SilvaGuerra, Marcelo Henrique Freitas SaraivaSaldanha, Gabriela Clemente BritoVasconcelos, Ana Karine Portela2020-03-25T16:06:49Zoai:ojs.pkp.sfu.ca:article/1440Revistahttps://rsdjournal.org/index.php/rsd/indexPUBhttps://rsdjournal.org/index.php/rsd/oairsd.articles@gmail.com2525-34092525-3409opendoar:2024-01-17T09:26:28.458840Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)false
dc.title.none.fl_str_mv Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
Utilización del control estadístico de procesos en una actividad experimental en el Instituto Federal de Ceará
Utilização de controle estatístico de processo em uma atividade experimental no Instituto Federal do Ceará
title Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
spellingShingle Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
Nojosa, Antônia Clarycy Barros
Laboratório
Carta de Controle
Nimodipino
Aprendizagem.
Laboratorio
Carta de Control
Nimodipina
El aprendizaje.
Laboratory
Control Chart
Nimodipine
Learning.
title_short Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
title_full Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
title_fullStr Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
title_full_unstemmed Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
title_sort Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
author Nojosa, Antônia Clarycy Barros
author_facet Nojosa, Antônia Clarycy Barros
Sampaio, Caroline de Góes
Firmino, Eduardo da Silva
Guerra, Marcelo Henrique Freitas Saraiva
Saldanha, Gabriela Clemente Brito
Vasconcelos, Ana Karine Portela
author_role author
author2 Sampaio, Caroline de Góes
Firmino, Eduardo da Silva
Guerra, Marcelo Henrique Freitas Saraiva
Saldanha, Gabriela Clemente Brito
Vasconcelos, Ana Karine Portela
author2_role author
author
author
author
author
dc.contributor.author.fl_str_mv Nojosa, Antônia Clarycy Barros
Sampaio, Caroline de Góes
Firmino, Eduardo da Silva
Guerra, Marcelo Henrique Freitas Saraiva
Saldanha, Gabriela Clemente Brito
Vasconcelos, Ana Karine Portela
dc.subject.por.fl_str_mv Laboratório
Carta de Controle
Nimodipino
Aprendizagem.
Laboratorio
Carta de Control
Nimodipina
El aprendizaje.
Laboratory
Control Chart
Nimodipine
Learning.
topic Laboratório
Carta de Controle
Nimodipino
Aprendizagem.
Laboratorio
Carta de Control
Nimodipina
El aprendizaje.
Laboratory
Control Chart
Nimodipine
Learning.
description As technology advances, chemical analysis laboratories use statistical techniques to demonstrate the accuracy and precision of analytical methods. To make comparisons between the data obtained from an analysis, Statistical Process Control (CEP) can be used, which is a technique widely used in industry to understand and improve process performance through statistical data processing. Control charts are CEP graphic methods that enable continuous control of analytical processes and allow evaluations and possible optimization of assays. The objective of this study is to use the Statistical Process Control (CEP), the control chart, to evaluate the statistical stability of the spectrophotometer used in the application of the Nimodipino analytical methodology validation technique, using data from the absorbance study of this drug, being the tests performed by students contributing to a learning of work activities. With this study it can be verified that the use of the control chart generates an adequate monitoring to evaluate data fluctuations and to carry out studies of the same, being able to be taught to the students and applied in practical classes accompaniments. It can also be demonstrated that the Minitab 17 program assists quickly in the construction of control charts, obtaining real-time analysis results. This program can be used in other laboratories of the Federal Institute of Ceará for statistical control of analyzes with support for student learning.
publishDate 2019
dc.date.none.fl_str_mv 2019-08-24
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://rsdjournal.org/index.php/rsd/article/view/1440
10.33448/rsd-v8i11.1440
url https://rsdjournal.org/index.php/rsd/article/view/1440
identifier_str_mv 10.33448/rsd-v8i11.1440
dc.language.iso.fl_str_mv por
language por
dc.relation.none.fl_str_mv https://rsdjournal.org/index.php/rsd/article/view/1440/1140
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Research, Society and Development
publisher.none.fl_str_mv Research, Society and Development
dc.source.none.fl_str_mv Research, Society and Development; Vol. 8 No. 11; e108111440
Research, Society and Development; Vol. 8 Núm. 11; e108111440
Research, Society and Development; v. 8 n. 11; e108111440
2525-3409
reponame:Research, Society and Development
instname:Universidade Federal de Itajubá (UNIFEI)
instacron:UNIFEI
instname_str Universidade Federal de Itajubá (UNIFEI)
instacron_str UNIFEI
institution UNIFEI
reponame_str Research, Society and Development
collection Research, Society and Development
repository.name.fl_str_mv Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)
repository.mail.fl_str_mv rsd.articles@gmail.com
_version_ 1797052644072620032