Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará
Autor(a) principal: | |
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Data de Publicação: | 2019 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | por |
Título da fonte: | Research, Society and Development |
Texto Completo: | https://rsdjournal.org/index.php/rsd/article/view/1440 |
Resumo: | As technology advances, chemical analysis laboratories use statistical techniques to demonstrate the accuracy and precision of analytical methods. To make comparisons between the data obtained from an analysis, Statistical Process Control (CEP) can be used, which is a technique widely used in industry to understand and improve process performance through statistical data processing. Control charts are CEP graphic methods that enable continuous control of analytical processes and allow evaluations and possible optimization of assays. The objective of this study is to use the Statistical Process Control (CEP), the control chart, to evaluate the statistical stability of the spectrophotometer used in the application of the Nimodipino analytical methodology validation technique, using data from the absorbance study of this drug, being the tests performed by students contributing to a learning of work activities. With this study it can be verified that the use of the control chart generates an adequate monitoring to evaluate data fluctuations and to carry out studies of the same, being able to be taught to the students and applied in practical classes accompaniments. It can also be demonstrated that the Minitab 17 program assists quickly in the construction of control charts, obtaining real-time analysis results. This program can be used in other laboratories of the Federal Institute of Ceará for statistical control of analyzes with support for student learning. |
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Utilization of statistical process control in an experimental activity at the Federal Institute of CearáUtilización del control estadístico de procesos en una actividad experimental en el Instituto Federal de CearáUtilização de controle estatístico de processo em uma atividade experimental no Instituto Federal do CearáLaboratórioCarta de ControleNimodipinoAprendizagem.LaboratorioCarta de ControlNimodipinaEl aprendizaje.LaboratoryControl ChartNimodipineLearning.As technology advances, chemical analysis laboratories use statistical techniques to demonstrate the accuracy and precision of analytical methods. To make comparisons between the data obtained from an analysis, Statistical Process Control (CEP) can be used, which is a technique widely used in industry to understand and improve process performance through statistical data processing. Control charts are CEP graphic methods that enable continuous control of analytical processes and allow evaluations and possible optimization of assays. The objective of this study is to use the Statistical Process Control (CEP), the control chart, to evaluate the statistical stability of the spectrophotometer used in the application of the Nimodipino analytical methodology validation technique, using data from the absorbance study of this drug, being the tests performed by students contributing to a learning of work activities. With this study it can be verified that the use of the control chart generates an adequate monitoring to evaluate data fluctuations and to carry out studies of the same, being able to be taught to the students and applied in practical classes accompaniments. It can also be demonstrated that the Minitab 17 program assists quickly in the construction of control charts, obtaining real-time analysis results. This program can be used in other laboratories of the Federal Institute of Ceará for statistical control of analyzes with support for student learning.A medida que avanza la tecnología, los laboratorios de análisis químicos utilizan técnicas estadísticas para demostrar la exactitud y precisión de los métodos analíticos. Para hacer comparaciones entre los datos obtenidos de un análisis, se puede utilizar el Control Estadístico de Procesos (CEP), que es una técnica ampliamente utilizada en la industria para comprender y mejorar el rendimiento del proceso a través del procesamiento de datos estadísticos. Los gráficos de control son métodos gráficos de CEP que permiten el control continuo de los procesos analíticos y permiten evaluaciones y una posible optimización de los ensayos. El objetivo de este estudio es utilizar el Control Estadístico de Procesos (CEP), el cuadro de control, para evaluar la estabilidad estadística del espectrofotómetro utilizado en la aplicación de la técnica de validación de metodología analítica Nimodipino, utilizando datos del estudio de absorbancia de este medicamento. siendo las pruebas realizadas por los alumnos que contribuyen al aprendizaje de las actividades laborales. Con este estudio se puede verificar que el uso del cuadro de control genera un monitoreo adecuado para evaluar las fluctuaciones de datos y realizar estudios de los mismos, pudiendo ser enseñado a los alumnos y aplicado en clases prácticas de acompañamiento. También se puede demostrar que el programa Minitab 17 ayuda rápidamente en la construcción de gráficos de control, obteniendo resultados de análisis en tiempo real. Este programa puede utilizarse en otros laboratorios del Instituto Federal de Ceará para el control estadístico de análisis con apoyo para el aprendizaje de los estudiantes.Com o avanço da tecnologia, os laboratórios de análises químicas utilizam-se de técnicas estatísticas para demonstrar a precisão e exatidão dos métodos analíticos. Para realizar comparações entre os dados obtidos de uma análise, pode-se utilizar o Controle Estatístico de Processo (CEP) que consiste em uma técnica muito utilizada na indústria para entender e melhorar o desempenho dos processos, através de tratamento estatístico de dados. As cartas de controle são métodos gráficos do CEP que possibilitam um controle contínuo dos processos analíticos e permitem avaliações e possível otimização dos ensaios. O objetivo desse estudo é utilizar o Controle Estatístico de Processo (CEP), a carta de controle, para avaliar a estabilidade estatística do espectrofotômetro utilizado na aplicação da técnica de validação de metodologia analítica do medicamento Nimodipino, utilizando dados do estudo de absorbância desse fármaco, sendo os testes realizados por alunos contribuindo para uma aprendizagem das atividades laborais. Com esse estudo pode-se verificar que a utilização da carta de controle gera um monitoramento adequado para avaliar oscilações de dados e realizar estudos dos mesmos, podendo ser ensinada para os alunos e aplicada em acompanhamentos de aulas práticas. Também pode-se demonstrar que o programa Minitab 17 auxilia de forma rápida na construção das cartas de controle, obtendo resultados em tempo real das análises. Esse programa pode ser utilizado em outros laboratórios do Instituto Federal do Ceará para controle estatístico das análises com apoio para a aprendizagem dos alunos.Research, Society and Development2019-08-24info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://rsdjournal.org/index.php/rsd/article/view/144010.33448/rsd-v8i11.1440Research, Society and Development; Vol. 8 No. 11; e108111440Research, Society and Development; Vol. 8 Núm. 11; e108111440Research, Society and Development; v. 8 n. 11; e1081114402525-3409reponame:Research, Society and Developmentinstname:Universidade Federal de Itajubá (UNIFEI)instacron:UNIFEIporhttps://rsdjournal.org/index.php/rsd/article/view/1440/1140Copyright (c) 2019 Antônia Clarycy Barros Nojosa, Caroline de Góes Sampaio, Eduardo da Silva Firmino, Marcelo Henrique Freitas Saraiva Guerra, Gabriela Clementino Brito Saldanha, Ana Karine Portela Vasconcelosinfo:eu-repo/semantics/openAccessNojosa, Antônia Clarycy BarrosSampaio, Caroline de GóesFirmino, Eduardo da SilvaGuerra, Marcelo Henrique Freitas SaraivaSaldanha, Gabriela Clemente BritoVasconcelos, Ana Karine Portela2020-03-25T16:06:49Zoai:ojs.pkp.sfu.ca:article/1440Revistahttps://rsdjournal.org/index.php/rsd/indexPUBhttps://rsdjournal.org/index.php/rsd/oairsd.articles@gmail.com2525-34092525-3409opendoar:2024-01-17T09:26:28.458840Research, Society and Development - Universidade Federal de Itajubá (UNIFEI)false |
dc.title.none.fl_str_mv |
Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará Utilización del control estadístico de procesos en una actividad experimental en el Instituto Federal de Ceará Utilização de controle estatístico de processo em uma atividade experimental no Instituto Federal do Ceará |
title |
Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará |
spellingShingle |
Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará Nojosa, Antônia Clarycy Barros Laboratório Carta de Controle Nimodipino Aprendizagem. Laboratorio Carta de Control Nimodipina El aprendizaje. Laboratory Control Chart Nimodipine Learning. |
title_short |
Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará |
title_full |
Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará |
title_fullStr |
Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará |
title_full_unstemmed |
Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará |
title_sort |
Utilization of statistical process control in an experimental activity at the Federal Institute of Ceará |
author |
Nojosa, Antônia Clarycy Barros |
author_facet |
Nojosa, Antônia Clarycy Barros Sampaio, Caroline de Góes Firmino, Eduardo da Silva Guerra, Marcelo Henrique Freitas Saraiva Saldanha, Gabriela Clemente Brito Vasconcelos, Ana Karine Portela |
author_role |
author |
author2 |
Sampaio, Caroline de Góes Firmino, Eduardo da Silva Guerra, Marcelo Henrique Freitas Saraiva Saldanha, Gabriela Clemente Brito Vasconcelos, Ana Karine Portela |
author2_role |
author author author author author |
dc.contributor.author.fl_str_mv |
Nojosa, Antônia Clarycy Barros Sampaio, Caroline de Góes Firmino, Eduardo da Silva Guerra, Marcelo Henrique Freitas Saraiva Saldanha, Gabriela Clemente Brito Vasconcelos, Ana Karine Portela |
dc.subject.por.fl_str_mv |
Laboratório Carta de Controle Nimodipino Aprendizagem. Laboratorio Carta de Control Nimodipina El aprendizaje. Laboratory Control Chart Nimodipine Learning. |
topic |
Laboratório Carta de Controle Nimodipino Aprendizagem. Laboratorio Carta de Control Nimodipina El aprendizaje. Laboratory Control Chart Nimodipine Learning. |
description |
As technology advances, chemical analysis laboratories use statistical techniques to demonstrate the accuracy and precision of analytical methods. To make comparisons between the data obtained from an analysis, Statistical Process Control (CEP) can be used, which is a technique widely used in industry to understand and improve process performance through statistical data processing. Control charts are CEP graphic methods that enable continuous control of analytical processes and allow evaluations and possible optimization of assays. The objective of this study is to use the Statistical Process Control (CEP), the control chart, to evaluate the statistical stability of the spectrophotometer used in the application of the Nimodipino analytical methodology validation technique, using data from the absorbance study of this drug, being the tests performed by students contributing to a learning of work activities. With this study it can be verified that the use of the control chart generates an adequate monitoring to evaluate data fluctuations and to carry out studies of the same, being able to be taught to the students and applied in practical classes accompaniments. It can also be demonstrated that the Minitab 17 program assists quickly in the construction of control charts, obtaining real-time analysis results. This program can be used in other laboratories of the Federal Institute of Ceará for statistical control of analyzes with support for student learning. |
publishDate |
2019 |
dc.date.none.fl_str_mv |
2019-08-24 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
https://rsdjournal.org/index.php/rsd/article/view/1440 10.33448/rsd-v8i11.1440 |
url |
https://rsdjournal.org/index.php/rsd/article/view/1440 |
identifier_str_mv |
10.33448/rsd-v8i11.1440 |
dc.language.iso.fl_str_mv |
por |
language |
por |
dc.relation.none.fl_str_mv |
https://rsdjournal.org/index.php/rsd/article/view/1440/1140 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Research, Society and Development |
publisher.none.fl_str_mv |
Research, Society and Development |
dc.source.none.fl_str_mv |
Research, Society and Development; Vol. 8 No. 11; e108111440 Research, Society and Development; Vol. 8 Núm. 11; e108111440 Research, Society and Development; v. 8 n. 11; e108111440 2525-3409 reponame:Research, Society and Development instname:Universidade Federal de Itajubá (UNIFEI) instacron:UNIFEI |
instname_str |
Universidade Federal de Itajubá (UNIFEI) |
instacron_str |
UNIFEI |
institution |
UNIFEI |
reponame_str |
Research, Society and Development |
collection |
Research, Society and Development |
repository.name.fl_str_mv |
Research, Society and Development - Universidade Federal de Itajubá (UNIFEI) |
repository.mail.fl_str_mv |
rsd.articles@gmail.com |
_version_ |
1797052644072620032 |