Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system

Detalhes bibliográficos
Autor(a) principal: Saleta, M. E.
Data de Publicação: 2017
Outros Autores: Eleotério, M., Mesquita, A. [UNESP], Mastelaro, V. R., Granado, E.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://dx.doi.org/10.1107/S1600577517008633
http://hdl.handle.net/11449/170095
Resumo: This work reports the setting up of the X-ray diffraction and spectroscopy beamline at the Brazilian Synchrotron Light Laboratory for performing total scattering experiments to be analyzed by atomic pair distribution function (PDF) studies. The results of a PDF refinement for Al2O3 standard are presented and compared with data acquired at a beamline of the Advanced Photon Source, where it is common to perform this type of experiment. A preliminary characterization of the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system, with x = 0.11, 0.12 and 0.15, is also shown.A setup for total scattering experiments at the multi-purpose XDS beamline of the Brazilian Synchrotron Light Laboratory (LNLS) is described. Also, a preliminary characterization of the Pb1-xLaxZr0.40Ti0.60O3 (x = 0.11, 0.12 and 0.15) ferroelectric system using pair distribution function analysis is presented.
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spelling Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric systematomic pair distribution functionferroelectric relaxorX-ray total scatteringThis work reports the setting up of the X-ray diffraction and spectroscopy beamline at the Brazilian Synchrotron Light Laboratory for performing total scattering experiments to be analyzed by atomic pair distribution function (PDF) studies. The results of a PDF refinement for Al2O3 standard are presented and compared with data acquired at a beamline of the Advanced Photon Source, where it is common to perform this type of experiment. A preliminary characterization of the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system, with x = 0.11, 0.12 and 0.15, is also shown.A setup for total scattering experiments at the multi-purpose XDS beamline of the Brazilian Synchrotron Light Laboratory (LNLS) is described. Also, a preliminary characterization of the Pb1-xLaxZr0.40Ti0.60O3 (x = 0.11, 0.12 and 0.15) ferroelectric system using pair distribution function analysis is presented.Instituto de Física 'Gleb Wataghin' Universidade de Campinas (UNICAMP)Laboratório Nacional de Luz Síncrotron, Caixa Postal 6192Instituto Geociências and Ciências Exatas Universidade Estadual Paulista (UNESP)Instituto de Física de São Carlos Universidade de São Paulo, CP 369CONICET - Centro Atómico Bariloche CNEAInstituto Geociências and Ciências Exatas Universidade Estadual Paulista (UNESP)Universidade Estadual de Campinas (UNICAMP)Laboratório Nacional de Luz SíncrotronUniversidade Estadual Paulista (Unesp)Universidade de São Paulo (USP)CNEASaleta, M. E.Eleotério, M.Mesquita, A. [UNESP]Mastelaro, V. R.Granado, E.2018-12-11T16:49:14Z2018-12-11T16:49:14Z2017-09-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article1098-1104application/pdfhttp://dx.doi.org/10.1107/S1600577517008633Journal of Synchrotron Radiation, v. 24, n. 5, p. 1098-1104, 2017.1600-57750909-0495http://hdl.handle.net/11449/17009510.1107/S16005775170086332-s2.0-850287105382-s2.0-85028710538.pdfScopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of Synchrotron Radiation1,6501,650info:eu-repo/semantics/openAccess2023-12-30T06:16:19Zoai:repositorio.unesp.br:11449/170095Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T21:40:33.618807Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system
title Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system
spellingShingle Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system
Saleta, M. E.
atomic pair distribution function
ferroelectric relaxor
X-ray total scattering
title_short Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system
title_full Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system
title_fullStr Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system
title_full_unstemmed Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system
title_sort Atomic pair distribution function at the Brazilian Synchrotron Light Laboratory: Application to the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system
author Saleta, M. E.
author_facet Saleta, M. E.
Eleotério, M.
Mesquita, A. [UNESP]
Mastelaro, V. R.
Granado, E.
author_role author
author2 Eleotério, M.
Mesquita, A. [UNESP]
Mastelaro, V. R.
Granado, E.
author2_role author
author
author
author
dc.contributor.none.fl_str_mv Universidade Estadual de Campinas (UNICAMP)
Laboratório Nacional de Luz Síncrotron
Universidade Estadual Paulista (Unesp)
Universidade de São Paulo (USP)
CNEA
dc.contributor.author.fl_str_mv Saleta, M. E.
Eleotério, M.
Mesquita, A. [UNESP]
Mastelaro, V. R.
Granado, E.
dc.subject.por.fl_str_mv atomic pair distribution function
ferroelectric relaxor
X-ray total scattering
topic atomic pair distribution function
ferroelectric relaxor
X-ray total scattering
description This work reports the setting up of the X-ray diffraction and spectroscopy beamline at the Brazilian Synchrotron Light Laboratory for performing total scattering experiments to be analyzed by atomic pair distribution function (PDF) studies. The results of a PDF refinement for Al2O3 standard are presented and compared with data acquired at a beamline of the Advanced Photon Source, where it is common to perform this type of experiment. A preliminary characterization of the Pb1-xLaxZr0.40Ti0.60O3 ferroelectric system, with x = 0.11, 0.12 and 0.15, is also shown.A setup for total scattering experiments at the multi-purpose XDS beamline of the Brazilian Synchrotron Light Laboratory (LNLS) is described. Also, a preliminary characterization of the Pb1-xLaxZr0.40Ti0.60O3 (x = 0.11, 0.12 and 0.15) ferroelectric system using pair distribution function analysis is presented.
publishDate 2017
dc.date.none.fl_str_mv 2017-09-01
2018-12-11T16:49:14Z
2018-12-11T16:49:14Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.1107/S1600577517008633
Journal of Synchrotron Radiation, v. 24, n. 5, p. 1098-1104, 2017.
1600-5775
0909-0495
http://hdl.handle.net/11449/170095
10.1107/S1600577517008633
2-s2.0-85028710538
2-s2.0-85028710538.pdf
url http://dx.doi.org/10.1107/S1600577517008633
http://hdl.handle.net/11449/170095
identifier_str_mv Journal of Synchrotron Radiation, v. 24, n. 5, p. 1098-1104, 2017.
1600-5775
0909-0495
10.1107/S1600577517008633
2-s2.0-85028710538
2-s2.0-85028710538.pdf
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Journal of Synchrotron Radiation
1,650
1,650
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 1098-1104
application/pdf
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv
_version_ 1808129345472954368

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