Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process
Autor(a) principal: | |
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Data de Publicação: | 2023 |
Outros Autores: | , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
DOI: | 10.1016/j.jmrt.2023.01.066 |
Texto Completo: | http://dx.doi.org/10.1016/j.jmrt.2023.01.066 http://hdl.handle.net/11449/246960 |
Resumo: | In the current research, a complex microstructure and crystallographic data were developed through quenching and partitioning (Q&P) process to improve tensile properties of commercial pearlitic carbon-silicon steel. Two-stage Q&P process, including full austenitization, quenching at 220 °C, followed by two different partitioning temperatures, was applied to the as-received specimen to generate a complex microstructure composed of tempered martensite, bainite, ultrafine carbides/martensite-austenite/retained austenite particles. Microstructure and crystallographic data were investigated by scanning electron microscopy, electron backscattered diffraction (EBSD), and X-ray diffraction techniques. Then, hardness and tensile properties were evaluated to confirm the improvement of mechanical properties. Dilatation-temperature curves exhibited the kinetics of martensitic and bainitic transformation during quenching and isothermal partitioning stages. The presence of nano-carbide particles inside athermal martensite was confirmed by electron microscopy due to the pre-formed martensite carbon depletion during the partitioning stage coupled with bainitic transformation. The formation of preferential atomic-compact <111> direction in BCC (martensite/bainite) plates characterized by EBSD, could enhance ductility by providing adequate slip systems. Point-to-point misorientation analyses demonstrated a slight dominance of low angle boundaries proportion in bainitic dominance structure in Q&P-220-375 specimen, which could be used in phase characterization. Results revealed that the development of nanoscale carbide dispersed in refined bainite/martensite matrix boosted the yield and ultimate tensile strength by over 100% and 110% compared to the initial pearlitic microstructure. However, ductility reduced to half value in Q&P-220-325 and Q&P-220-375 specimens. |
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Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) processCarbon saturated martensiteKernel average misorientationSlip systemsIn the current research, a complex microstructure and crystallographic data were developed through quenching and partitioning (Q&P) process to improve tensile properties of commercial pearlitic carbon-silicon steel. Two-stage Q&P process, including full austenitization, quenching at 220 °C, followed by two different partitioning temperatures, was applied to the as-received specimen to generate a complex microstructure composed of tempered martensite, bainite, ultrafine carbides/martensite-austenite/retained austenite particles. Microstructure and crystallographic data were investigated by scanning electron microscopy, electron backscattered diffraction (EBSD), and X-ray diffraction techniques. Then, hardness and tensile properties were evaluated to confirm the improvement of mechanical properties. Dilatation-temperature curves exhibited the kinetics of martensitic and bainitic transformation during quenching and isothermal partitioning stages. The presence of nano-carbide particles inside athermal martensite was confirmed by electron microscopy due to the pre-formed martensite carbon depletion during the partitioning stage coupled with bainitic transformation. The formation of preferential atomic-compact <111> direction in BCC (martensite/bainite) plates characterized by EBSD, could enhance ductility by providing adequate slip systems. Point-to-point misorientation analyses demonstrated a slight dominance of low angle boundaries proportion in bainitic dominance structure in Q&P-220-375 specimen, which could be used in phase characterization. Results revealed that the development of nanoscale carbide dispersed in refined bainite/martensite matrix boosted the yield and ultimate tensile strength by over 100% and 110% compared to the initial pearlitic microstructure. However, ductility reduced to half value in Q&P-220-325 and Q&P-220-375 specimens.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)Financiadora de Estudos e ProjetosFundação Cearense de Apoio ao Desenvolvimento Científico e TecnológicoUniversité de Franche-ComtéFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Ministério da Ciência, Tecnologia e InovaçãoDepartment of Mechanical Engineering University of BonabEscuela de Tecnologıa Mecanica Universidad Tecnologica de Pereira, Carrera 27 #10-02 AlamosMetallurgical and Materials Engineering Department University of São Paulo, Av. Prof. Mello MoraesMaterials Characterization Laboratory (LACAM) Department of Metallurgical and Materials Engineering Federal University of Ceará Campus Do PiciMetallurgical Processes Laboratory Institute for Technological Research, Av. Prof. Almeida Prado, 532 São PauloDepartment of Strength of Materials and Structural Engineering Barcelona School of Engineering (ETSEIB) Universitat Politècnica de CatalunyaCentro de Engenharia Modelagem e Ciências Sociais Aplicadas Universidade Federal Do ABC, Santo AndréDepartment of Aeronautical Engineering School of Engineering of São João (FESJ) São Paulo State University, São João da Boa VistaDepartment of Aeronautical Engineering School of Engineering of São João (FESJ) São Paulo State University, São João da Boa VistaFAPESP: 2021/02926-4CNPq: 304157/2020-1Ministério da Ciência, Tecnologia e Inovação: 442577/2019-2University of BonabUniversidad Tecnologica de PereiraUniversidade de São Paulo (USP)Federal University of CearáInstitute for Technological ResearchUniversitat Politècnica de CatalunyaUniversidade Federal do ABC (UFABC)Universidade Estadual Paulista (UNESP)Mohtadi-Bonab, M. A.Ariza, Edwan A.Loureiro, Rodrigo C.P.Centeno, DanyCarvalho, Felipe M.Avila, Julian A. [UNESP]Masoumi, Mohammad2023-07-29T12:55:16Z2023-07-29T12:55:16Z2023-03-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article845-858http://dx.doi.org/10.1016/j.jmrt.2023.01.066Journal of Materials Research and Technology, v. 23, p. 845-858.2238-7854http://hdl.handle.net/11449/24696010.1016/j.jmrt.2023.01.0662-s2.0-85149630285Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of Materials Research and Technologyinfo:eu-repo/semantics/openAccess2023-07-29T12:55:16Zoai:repositorio.unesp.br:11449/246960Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T17:28:06.357810Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process |
title |
Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process |
spellingShingle |
Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process Mohtadi-Bonab, M. A. Carbon saturated martensite Kernel average misorientation Slip systems Mohtadi-Bonab, M. A. Carbon saturated martensite Kernel average misorientation Slip systems |
title_short |
Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process |
title_full |
Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process |
title_fullStr |
Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process |
title_full_unstemmed |
Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process |
title_sort |
Improvement of tensile properties by controlling the microstructure and crystallographic data in commercial pearlitic carbon-silicon steel via quenching and partitioning (Q&P) process |
author |
Mohtadi-Bonab, M. A. |
author_facet |
Mohtadi-Bonab, M. A. Mohtadi-Bonab, M. A. Ariza, Edwan A. Loureiro, Rodrigo C.P. Centeno, Dany Carvalho, Felipe M. Avila, Julian A. [UNESP] Masoumi, Mohammad Ariza, Edwan A. Loureiro, Rodrigo C.P. Centeno, Dany Carvalho, Felipe M. Avila, Julian A. [UNESP] Masoumi, Mohammad |
author_role |
author |
author2 |
Ariza, Edwan A. Loureiro, Rodrigo C.P. Centeno, Dany Carvalho, Felipe M. Avila, Julian A. [UNESP] Masoumi, Mohammad |
author2_role |
author author author author author author |
dc.contributor.none.fl_str_mv |
University of Bonab Universidad Tecnologica de Pereira Universidade de São Paulo (USP) Federal University of Ceará Institute for Technological Research Universitat Politècnica de Catalunya Universidade Federal do ABC (UFABC) Universidade Estadual Paulista (UNESP) |
dc.contributor.author.fl_str_mv |
Mohtadi-Bonab, M. A. Ariza, Edwan A. Loureiro, Rodrigo C.P. Centeno, Dany Carvalho, Felipe M. Avila, Julian A. [UNESP] Masoumi, Mohammad |
dc.subject.por.fl_str_mv |
Carbon saturated martensite Kernel average misorientation Slip systems |
topic |
Carbon saturated martensite Kernel average misorientation Slip systems |
description |
In the current research, a complex microstructure and crystallographic data were developed through quenching and partitioning (Q&P) process to improve tensile properties of commercial pearlitic carbon-silicon steel. Two-stage Q&P process, including full austenitization, quenching at 220 °C, followed by two different partitioning temperatures, was applied to the as-received specimen to generate a complex microstructure composed of tempered martensite, bainite, ultrafine carbides/martensite-austenite/retained austenite particles. Microstructure and crystallographic data were investigated by scanning electron microscopy, electron backscattered diffraction (EBSD), and X-ray diffraction techniques. Then, hardness and tensile properties were evaluated to confirm the improvement of mechanical properties. Dilatation-temperature curves exhibited the kinetics of martensitic and bainitic transformation during quenching and isothermal partitioning stages. The presence of nano-carbide particles inside athermal martensite was confirmed by electron microscopy due to the pre-formed martensite carbon depletion during the partitioning stage coupled with bainitic transformation. The formation of preferential atomic-compact <111> direction in BCC (martensite/bainite) plates characterized by EBSD, could enhance ductility by providing adequate slip systems. Point-to-point misorientation analyses demonstrated a slight dominance of low angle boundaries proportion in bainitic dominance structure in Q&P-220-375 specimen, which could be used in phase characterization. Results revealed that the development of nanoscale carbide dispersed in refined bainite/martensite matrix boosted the yield and ultimate tensile strength by over 100% and 110% compared to the initial pearlitic microstructure. However, ductility reduced to half value in Q&P-220-325 and Q&P-220-375 specimens. |
publishDate |
2023 |
dc.date.none.fl_str_mv |
2023-07-29T12:55:16Z 2023-07-29T12:55:16Z 2023-03-01 |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.1016/j.jmrt.2023.01.066 Journal of Materials Research and Technology, v. 23, p. 845-858. 2238-7854 http://hdl.handle.net/11449/246960 10.1016/j.jmrt.2023.01.066 2-s2.0-85149630285 |
url |
http://dx.doi.org/10.1016/j.jmrt.2023.01.066 http://hdl.handle.net/11449/246960 |
identifier_str_mv |
Journal of Materials Research and Technology, v. 23, p. 845-858. 2238-7854 10.1016/j.jmrt.2023.01.066 2-s2.0-85149630285 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Journal of Materials Research and Technology |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
845-858 |
dc.source.none.fl_str_mv |
Scopus reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1822182399411224576 |
dc.identifier.doi.none.fl_str_mv |
10.1016/j.jmrt.2023.01.066 |