Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry
Autor(a) principal: | |
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Data de Publicação: | 2013 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://dx.doi.org/10.3390/molecules18032803 http://hdl.handle.net/11449/74758 |
Resumo: | The present study investigates the chemical composition of the African plant Parkia biglobosa (Fabaceae) roots and barks by Liquid Chromatography - Electrospray Ionization and Direct Injection Tandem Mass Spectrometry analysis. Mass spectral data indicated that B-type oligomers are present, namely procyanidins and prodelphinidins, with their gallate and glucuronide derivatives, some of them in different isomeric forms. The analysis evidenced the presence of up to 40 proanthocyanidins, some of which are reported for the first time. In this study, the antiradical activity of extracts of roots and barks from Parkia biglobosa was evaluated using DPPH method and they showed satisfactory activities. |
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Repositório Institucional da UNESP |
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Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometryAntiradicalFabaceaeFIA-ESI-IT-MSnHPLC/ESI-MSParkia biglobosaProanthocyanidinsantioxidantplant extractproanthocyanidinbarkchemistryflow injection analysisplant roottandem mass spectrometryAntioxidantsFlow Injection AnalysisPlant BarkPlant ExtractsPlant RootsTandem Mass SpectrometryThe present study investigates the chemical composition of the African plant Parkia biglobosa (Fabaceae) roots and barks by Liquid Chromatography - Electrospray Ionization and Direct Injection Tandem Mass Spectrometry analysis. Mass spectral data indicated that B-type oligomers are present, namely procyanidins and prodelphinidins, with their gallate and glucuronide derivatives, some of them in different isomeric forms. The analysis evidenced the presence of up to 40 proanthocyanidins, some of which are reported for the first time. In this study, the antiradical activity of extracts of roots and barks from Parkia biglobosa was evaluated using DPPH method and they showed satisfactory activities.Department of Organic Chemistry Institute of Chemistry UNESP - Sao Paulo State University, 14800-900, Araraquara, Sao PauloDepartment of Organic Chemistry Faculty of Science University of Yaounde i, PO Box 812, YaoundeCenter of Chemical and Instrumental Analysis Embrapa Agroenergy PqEB, W3 North, 70770-901, Brasilia, Distrito FederalExperimental Campus of Sao Vicente UNESP - Sao Paulo State University, 11350-000, Sao Vicente, Sao PauloDepartment of Organic Chemistry Institute of Chemistry UNESP - Sao Paulo State University, 14800-900, Araraquara, Sao PauloExperimental Campus of Sao Vicente UNESP - Sao Paulo State University, 11350-000, Sao Vicente, Sao PauloUniversidade Estadual Paulista (Unesp)University of Yaounde iEmpresa Brasileira de Pesquisa Agropecuária (EMBRAPA)Tala, Viviane Raïssa Sipowo [UNESP]Da Silva, Viviane Candida [UNESP]Rodrigues, Clenilson Martins [UNESP]Nkengfack, Augustin EphremSantos, Lourdes Campaner dos [UNESP]Vilegas, Wagner [UNESP]2014-05-27T11:28:37Z2014-05-27T11:28:37Z2013-03-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article2803-2820application/pdfhttp://dx.doi.org/10.3390/molecules18032803Molecules, v. 18, n. 3, p. 2803-2820, 2013.1420-3049http://hdl.handle.net/11449/7475810.3390/molecules18032803WOS:0003166117000272-s2.0-848755828682-s2.0-84875582868.pdf7927877224326837353825364060297735382536406029770000-0003-3032-2556Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengMolecules3.0980,855info:eu-repo/semantics/openAccess2023-11-23T06:16:02Zoai:repositorio.unesp.br:11449/74758Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T18:32:34.954421Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry |
title |
Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry |
spellingShingle |
Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry Tala, Viviane Raïssa Sipowo [UNESP] Antiradical Fabaceae FIA-ESI-IT-MSn HPLC/ESI-MS Parkia biglobosa Proanthocyanidins antioxidant plant extract proanthocyanidin bark chemistry flow injection analysis plant root tandem mass spectrometry Antioxidants Flow Injection Analysis Plant Bark Plant Extracts Plant Roots Tandem Mass Spectrometry |
title_short |
Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry |
title_full |
Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry |
title_fullStr |
Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry |
title_full_unstemmed |
Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry |
title_sort |
Characterization of proanthocyanidins from Parkia biglobosa (Jacq.) G. Don. (Fabaceae) by flow injection analysis - Electrospray ionization ion trap tandem mass spectrometry and liquid chromatography/electrospray ionization mass spectrometry |
author |
Tala, Viviane Raïssa Sipowo [UNESP] |
author_facet |
Tala, Viviane Raïssa Sipowo [UNESP] Da Silva, Viviane Candida [UNESP] Rodrigues, Clenilson Martins [UNESP] Nkengfack, Augustin Ephrem Santos, Lourdes Campaner dos [UNESP] Vilegas, Wagner [UNESP] |
author_role |
author |
author2 |
Da Silva, Viviane Candida [UNESP] Rodrigues, Clenilson Martins [UNESP] Nkengfack, Augustin Ephrem Santos, Lourdes Campaner dos [UNESP] Vilegas, Wagner [UNESP] |
author2_role |
author author author author author |
dc.contributor.none.fl_str_mv |
Universidade Estadual Paulista (Unesp) University of Yaounde i Empresa Brasileira de Pesquisa Agropecuária (EMBRAPA) |
dc.contributor.author.fl_str_mv |
Tala, Viviane Raïssa Sipowo [UNESP] Da Silva, Viviane Candida [UNESP] Rodrigues, Clenilson Martins [UNESP] Nkengfack, Augustin Ephrem Santos, Lourdes Campaner dos [UNESP] Vilegas, Wagner [UNESP] |
dc.subject.por.fl_str_mv |
Antiradical Fabaceae FIA-ESI-IT-MSn HPLC/ESI-MS Parkia biglobosa Proanthocyanidins antioxidant plant extract proanthocyanidin bark chemistry flow injection analysis plant root tandem mass spectrometry Antioxidants Flow Injection Analysis Plant Bark Plant Extracts Plant Roots Tandem Mass Spectrometry |
topic |
Antiradical Fabaceae FIA-ESI-IT-MSn HPLC/ESI-MS Parkia biglobosa Proanthocyanidins antioxidant plant extract proanthocyanidin bark chemistry flow injection analysis plant root tandem mass spectrometry Antioxidants Flow Injection Analysis Plant Bark Plant Extracts Plant Roots Tandem Mass Spectrometry |
description |
The present study investigates the chemical composition of the African plant Parkia biglobosa (Fabaceae) roots and barks by Liquid Chromatography - Electrospray Ionization and Direct Injection Tandem Mass Spectrometry analysis. Mass spectral data indicated that B-type oligomers are present, namely procyanidins and prodelphinidins, with their gallate and glucuronide derivatives, some of them in different isomeric forms. The analysis evidenced the presence of up to 40 proanthocyanidins, some of which are reported for the first time. In this study, the antiradical activity of extracts of roots and barks from Parkia biglobosa was evaluated using DPPH method and they showed satisfactory activities. |
publishDate |
2013 |
dc.date.none.fl_str_mv |
2013-03-01 2014-05-27T11:28:37Z 2014-05-27T11:28:37Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.3390/molecules18032803 Molecules, v. 18, n. 3, p. 2803-2820, 2013. 1420-3049 http://hdl.handle.net/11449/74758 10.3390/molecules18032803 WOS:000316611700027 2-s2.0-84875582868 2-s2.0-84875582868.pdf 7927877224326837 3538253640602977 3538253640602977 0000-0003-3032-2556 |
url |
http://dx.doi.org/10.3390/molecules18032803 http://hdl.handle.net/11449/74758 |
identifier_str_mv |
Molecules, v. 18, n. 3, p. 2803-2820, 2013. 1420-3049 10.3390/molecules18032803 WOS:000316611700027 2-s2.0-84875582868 2-s2.0-84875582868.pdf 7927877224326837 3538253640602977 0000-0003-3032-2556 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Molecules 3.098 0,855 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
2803-2820 application/pdf |
dc.source.none.fl_str_mv |
Scopus reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1808128944488054784 |