Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography

Detalhes bibliográficos
Autor(a) principal: Da Silva, V. C. [UNESP]
Data de Publicação: 2006
Outros Autores: Silvab, G. H., Da S Bolzani, V., Lopes, Márcia Nasser [UNESP]
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://dx.doi.org/10.1590/S0100-46702006000400008
http://hdl.handle.net/11449/69282
Resumo: Enantiomeric aglycone lignans contained in a mixture were separated from a fraction of the extract of the stems of Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography. An efficient and fast separation can be achieved with methanol-water (30:70, v/v). Their structures were identified as (+)-lyoniresinol 3α-O-β-glucopyranoside and (-)-lyoniresinol 3α-O-β-glucopyranoside, being reported for the first time in Rubiaceae.
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spelling Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatographyAlibertia sessilisEnantiomeric aglycone lignansHPLCRubiaceaeEnantiomeric aglycone lignans contained in a mixture were separated from a fraction of the extract of the stems of Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography. An efficient and fast separation can be achieved with methanol-water (30:70, v/v). Their structures were identified as (+)-lyoniresinol 3α-O-β-glucopyranoside and (-)-lyoniresinol 3α-O-β-glucopyranoside, being reported for the first time in Rubiaceae.Departamento de Química Orgânica Instituto de Química Universidade Estadual Júlio de Mesquita Filho, CP 355, CEP 14800-900, Araraquara, SPDepartamento de Química Orgânica Instituto de Química Universidade Estadual Júlio de Mesquita Filho, CP 355, CEP 14800-900, Araraquara, SPUniversidade Estadual Paulista (Unesp)Da Silva, V. C. [UNESP]Silvab, G. H.Da S Bolzani, V.Lopes, Márcia Nasser [UNESP]2014-05-27T11:22:03Z2014-05-27T11:22:03Z2006-12-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article55-58application/pdfhttp://dx.doi.org/10.1590/S0100-46702006000400008Ecletica Quimica, v. 31, n. 4, p. 55-58, 2006.0100-4670http://hdl.handle.net/11449/6928210.1590/S0100-46702006000400008S0100-467020060004000082-s2.0-339471424732-s2.0-33947142473.pdf3310170899693944Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengEclética Químicainfo:eu-repo/semantics/openAccess2024-12-04T14:10:43Zoai:repositorio.unesp.br:11449/69282Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestrepositoriounesp@unesp.bropendoar:29462024-12-04T14:10:43Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography
title Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography
spellingShingle Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography
Da Silva, V. C. [UNESP]
Alibertia sessilis
Enantiomeric aglycone lignans
HPLC
Rubiaceae
title_short Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography
title_full Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography
title_fullStr Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography
title_full_unstemmed Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography
title_sort Isolation of lignans glycosides from Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography
author Da Silva, V. C. [UNESP]
author_facet Da Silva, V. C. [UNESP]
Silvab, G. H.
Da S Bolzani, V.
Lopes, Márcia Nasser [UNESP]
author_role author
author2 Silvab, G. H.
Da S Bolzani, V.
Lopes, Márcia Nasser [UNESP]
author2_role author
author
author
dc.contributor.none.fl_str_mv Universidade Estadual Paulista (Unesp)
dc.contributor.author.fl_str_mv Da Silva, V. C. [UNESP]
Silvab, G. H.
Da S Bolzani, V.
Lopes, Márcia Nasser [UNESP]
dc.subject.por.fl_str_mv Alibertia sessilis
Enantiomeric aglycone lignans
HPLC
Rubiaceae
topic Alibertia sessilis
Enantiomeric aglycone lignans
HPLC
Rubiaceae
description Enantiomeric aglycone lignans contained in a mixture were separated from a fraction of the extract of the stems of Alibertia sessilis (Vell.) K. Schum. (Rubiaceae) by preparative high-performance liquid chromatography. An efficient and fast separation can be achieved with methanol-water (30:70, v/v). Their structures were identified as (+)-lyoniresinol 3α-O-β-glucopyranoside and (-)-lyoniresinol 3α-O-β-glucopyranoside, being reported for the first time in Rubiaceae.
publishDate 2006
dc.date.none.fl_str_mv 2006-12-01
2014-05-27T11:22:03Z
2014-05-27T11:22:03Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.1590/S0100-46702006000400008
Ecletica Quimica, v. 31, n. 4, p. 55-58, 2006.
0100-4670
http://hdl.handle.net/11449/69282
10.1590/S0100-46702006000400008
S0100-46702006000400008
2-s2.0-33947142473
2-s2.0-33947142473.pdf
3310170899693944
url http://dx.doi.org/10.1590/S0100-46702006000400008
http://hdl.handle.net/11449/69282
identifier_str_mv Ecletica Quimica, v. 31, n. 4, p. 55-58, 2006.
0100-4670
10.1590/S0100-46702006000400008
S0100-46702006000400008
2-s2.0-33947142473
2-s2.0-33947142473.pdf
3310170899693944
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Eclética Química
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 55-58
application/pdf
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv repositoriounesp@unesp.br
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