Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification
Autor(a) principal: | |
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Data de Publicação: | 2018 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://dx.doi.org/10.1590/1980-5373-MR-2017-0508 http://hdl.handle.net/11449/164331 |
Resumo: | The purpose of this study is the surface modification of Ti10Mo8Nb experimental alloy by using TiO2 nanostructure growth. Ingots of the Ti10Mo8Nb experimental alloy were produced by fusion from sheets of molybdenum, niobium, and titanium commercially pure in an arc melting furnace under argon atmosphere. The potentiostatic anodic oxidation was performed using an electrolyte formed of glycerol and H2O (1: 1 by vol.) with the addition of 2.7% (w/v) NH4F under 20 V for 3 h at room temperature. After the surface treatment, the samples were annealing. The surface of the alloy was analyzed by scanning electron microscopy (SEM), X-ray diffraction (XRD), contact angle, surface energy measurements. In vitro studies, such as cell and bacterial adhesion, were performed to evaluate the response of this treatment. The Ti10Mo8Nb alloy exhibited beta phase after the processing. After the surface treatment, a nanoporous layer of TiO was obtained. The anatase phase was found in the annealed samples (450 degrees C for 3 hours). In vitro analyzes showed cell growth viability and decreased bacterial proliferation due to the larger specific surface area. |
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Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface ModificationTitanium alloyssurface modificationcell-material interactionsbacterial adherenceThe purpose of this study is the surface modification of Ti10Mo8Nb experimental alloy by using TiO2 nanostructure growth. Ingots of the Ti10Mo8Nb experimental alloy were produced by fusion from sheets of molybdenum, niobium, and titanium commercially pure in an arc melting furnace under argon atmosphere. The potentiostatic anodic oxidation was performed using an electrolyte formed of glycerol and H2O (1: 1 by vol.) with the addition of 2.7% (w/v) NH4F under 20 V for 3 h at room temperature. After the surface treatment, the samples were annealing. The surface of the alloy was analyzed by scanning electron microscopy (SEM), X-ray diffraction (XRD), contact angle, surface energy measurements. In vitro studies, such as cell and bacterial adhesion, were performed to evaluate the response of this treatment. The Ti10Mo8Nb alloy exhibited beta phase after the processing. After the surface treatment, a nanoporous layer of TiO was obtained. The anatase phase was found in the annealed samples (450 degrees C for 3 hours). In vitro analyzes showed cell growth viability and decreased bacterial proliferation due to the larger specific surface area.Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Univ Estadual Paulista UNESP, Escola Engn, Guaratingueta, SP, BrazilUniv Estadual Paulista UNESP, Dept Biociencias & Diagnost Bucal, Sao Jose Dos Campos, SP, BrazilColorado State Univ, Dept Mech Engn, Sch Biomed Engn, Ft Collins, CO 80523 USAUniv Estadual Paulista UNESP, Escola Engn, Guaratingueta, SP, BrazilUniv Estadual Paulista UNESP, Dept Biociencias & Diagnost Bucal, Sao Jose Dos Campos, SP, BrazilCNPq: 486352/2013-7Univ Fed Sao Carlos, Dept Engenharia MaterialsUniversidade Estadual Paulista (Unesp)Colorado State UnivAquiles Carobolante, Joao Pedro [UNESP]Pereira, Cristiane Aparecida [UNESP]Dias-Netipanyj, Marcela Ferreira [UNESP]Popat, Ketul ChandrakantRosifini Alves Claro, Ana Paula [UNESP]2018-11-26T17:52:09Z2018-11-26T17:52:09Z2018-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article5application/pdfhttp://dx.doi.org/10.1590/1980-5373-MR-2017-0508Materials Research-ibero-american Journal Of Materials. Sao Carlos: Univ Fed Sao Carlos, Dept Engenharia Materials, v. 21, n. 4, 5 p., 2018.1516-1439http://hdl.handle.net/11449/16433110.1590/1980-5373-MR-2017-0508S1516-14392018000400232WOS:000435591700001S1516-14392018000400232.pdfWeb of Sciencereponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengMaterials Research-ibero-american Journal Of Materials0,398info:eu-repo/semantics/openAccess2023-12-29T06:17:33Zoai:repositorio.unesp.br:11449/164331Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T21:34:39.795606Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification |
title |
Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification |
spellingShingle |
Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification Aquiles Carobolante, Joao Pedro [UNESP] Titanium alloys surface modification cell-material interactions bacterial adherence |
title_short |
Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification |
title_full |
Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification |
title_fullStr |
Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification |
title_full_unstemmed |
Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification |
title_sort |
Cell and Bacteria-Baterial Interactions on the Ti10Mo8Nb Alloy After Surface Modification |
author |
Aquiles Carobolante, Joao Pedro [UNESP] |
author_facet |
Aquiles Carobolante, Joao Pedro [UNESP] Pereira, Cristiane Aparecida [UNESP] Dias-Netipanyj, Marcela Ferreira [UNESP] Popat, Ketul Chandrakant Rosifini Alves Claro, Ana Paula [UNESP] |
author_role |
author |
author2 |
Pereira, Cristiane Aparecida [UNESP] Dias-Netipanyj, Marcela Ferreira [UNESP] Popat, Ketul Chandrakant Rosifini Alves Claro, Ana Paula [UNESP] |
author2_role |
author author author author |
dc.contributor.none.fl_str_mv |
Universidade Estadual Paulista (Unesp) Colorado State Univ |
dc.contributor.author.fl_str_mv |
Aquiles Carobolante, Joao Pedro [UNESP] Pereira, Cristiane Aparecida [UNESP] Dias-Netipanyj, Marcela Ferreira [UNESP] Popat, Ketul Chandrakant Rosifini Alves Claro, Ana Paula [UNESP] |
dc.subject.por.fl_str_mv |
Titanium alloys surface modification cell-material interactions bacterial adherence |
topic |
Titanium alloys surface modification cell-material interactions bacterial adherence |
description |
The purpose of this study is the surface modification of Ti10Mo8Nb experimental alloy by using TiO2 nanostructure growth. Ingots of the Ti10Mo8Nb experimental alloy were produced by fusion from sheets of molybdenum, niobium, and titanium commercially pure in an arc melting furnace under argon atmosphere. The potentiostatic anodic oxidation was performed using an electrolyte formed of glycerol and H2O (1: 1 by vol.) with the addition of 2.7% (w/v) NH4F under 20 V for 3 h at room temperature. After the surface treatment, the samples were annealing. The surface of the alloy was analyzed by scanning electron microscopy (SEM), X-ray diffraction (XRD), contact angle, surface energy measurements. In vitro studies, such as cell and bacterial adhesion, were performed to evaluate the response of this treatment. The Ti10Mo8Nb alloy exhibited beta phase after the processing. After the surface treatment, a nanoporous layer of TiO was obtained. The anatase phase was found in the annealed samples (450 degrees C for 3 hours). In vitro analyzes showed cell growth viability and decreased bacterial proliferation due to the larger specific surface area. |
publishDate |
2018 |
dc.date.none.fl_str_mv |
2018-11-26T17:52:09Z 2018-11-26T17:52:09Z 2018-01-01 |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.1590/1980-5373-MR-2017-0508 Materials Research-ibero-american Journal Of Materials. Sao Carlos: Univ Fed Sao Carlos, Dept Engenharia Materials, v. 21, n. 4, 5 p., 2018. 1516-1439 http://hdl.handle.net/11449/164331 10.1590/1980-5373-MR-2017-0508 S1516-14392018000400232 WOS:000435591700001 S1516-14392018000400232.pdf |
url |
http://dx.doi.org/10.1590/1980-5373-MR-2017-0508 http://hdl.handle.net/11449/164331 |
identifier_str_mv |
Materials Research-ibero-american Journal Of Materials. Sao Carlos: Univ Fed Sao Carlos, Dept Engenharia Materials, v. 21, n. 4, 5 p., 2018. 1516-1439 10.1590/1980-5373-MR-2017-0508 S1516-14392018000400232 WOS:000435591700001 S1516-14392018000400232.pdf |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Materials Research-ibero-american Journal Of Materials 0,398 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
5 application/pdf |
dc.publisher.none.fl_str_mv |
Univ Fed Sao Carlos, Dept Engenharia Materials |
publisher.none.fl_str_mv |
Univ Fed Sao Carlos, Dept Engenharia Materials |
dc.source.none.fl_str_mv |
Web of Science reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
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1808129337847709696 |