Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
Autor(a) principal: | |
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Data de Publicação: | 2020 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Materials research (São Carlos. Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000100210 |
Resumo: | Composites based on graphene oxide (GO), reduced graphene oxide (RGO) and zinc oxide (ZnO) with different mass ratios (8, 100 and 600) were synthesized through the hydrothermal method at 100 °C and used as reinforcement materials to commercial glass-ionomers cements (GIC). X-ray diffraction (XRD) characterization confirmed the graphite oxidation and ZnO formation as a wurtzite phase. Infrared spectroscopy analyses showed bands of oxygen-containing groups on the GO surface, which reduced after thermal treatment and RGO formation. D and G bands were observed in all samples synthesized, which presented morphology similar to flowers with a crystallite size of 18 nm. The effect on the mechanical properties of GIC after reinforcement with 0.1 wt% of RGO and 3 wt% of the composites was evaluated using a one-way analysis of variance (ANOVA). It was verified slight improvements in the hardness of GIC. |
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Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials ReinforcementReduced graphene oxideZnO compositesglass-ionomer cementmechanical propertiesphysicochemical characterizationComposites based on graphene oxide (GO), reduced graphene oxide (RGO) and zinc oxide (ZnO) with different mass ratios (8, 100 and 600) were synthesized through the hydrothermal method at 100 °C and used as reinforcement materials to commercial glass-ionomers cements (GIC). X-ray diffraction (XRD) characterization confirmed the graphite oxidation and ZnO formation as a wurtzite phase. Infrared spectroscopy analyses showed bands of oxygen-containing groups on the GO surface, which reduced after thermal treatment and RGO formation. D and G bands were observed in all samples synthesized, which presented morphology similar to flowers with a crystallite size of 18 nm. The effect on the mechanical properties of GIC after reinforcement with 0.1 wt% of RGO and 3 wt% of the composites was evaluated using a one-way analysis of variance (ANOVA). It was verified slight improvements in the hardness of GIC.ABM, ABC, ABPol2020-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000100210Materials Research v.23 n.1 2020reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/1980-5373-mr-2019-0580info:eu-repo/semantics/openAccessBenevides,Ana PaulaCampos,Adriano RochaVieira,Lanna Cristinados Reis Perez,CesarCesar,Deborah Vargaseng2020-03-17T00:00:00Zoai:scielo:S1516-14392020000100210Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2020-03-17T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false |
dc.title.none.fl_str_mv |
Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement |
title |
Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement |
spellingShingle |
Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement Benevides,Ana Paula Reduced graphene oxide ZnO composites glass-ionomer cement mechanical properties physicochemical characterization |
title_short |
Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement |
title_full |
Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement |
title_fullStr |
Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement |
title_full_unstemmed |
Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement |
title_sort |
Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement |
author |
Benevides,Ana Paula |
author_facet |
Benevides,Ana Paula Campos,Adriano Rocha Vieira,Lanna Cristina dos Reis Perez,Cesar Cesar,Deborah Vargas |
author_role |
author |
author2 |
Campos,Adriano Rocha Vieira,Lanna Cristina dos Reis Perez,Cesar Cesar,Deborah Vargas |
author2_role |
author author author author |
dc.contributor.author.fl_str_mv |
Benevides,Ana Paula Campos,Adriano Rocha Vieira,Lanna Cristina dos Reis Perez,Cesar Cesar,Deborah Vargas |
dc.subject.por.fl_str_mv |
Reduced graphene oxide ZnO composites glass-ionomer cement mechanical properties physicochemical characterization |
topic |
Reduced graphene oxide ZnO composites glass-ionomer cement mechanical properties physicochemical characterization |
description |
Composites based on graphene oxide (GO), reduced graphene oxide (RGO) and zinc oxide (ZnO) with different mass ratios (8, 100 and 600) were synthesized through the hydrothermal method at 100 °C and used as reinforcement materials to commercial glass-ionomers cements (GIC). X-ray diffraction (XRD) characterization confirmed the graphite oxidation and ZnO formation as a wurtzite phase. Infrared spectroscopy analyses showed bands of oxygen-containing groups on the GO surface, which reduced after thermal treatment and RGO formation. D and G bands were observed in all samples synthesized, which presented morphology similar to flowers with a crystallite size of 18 nm. The effect on the mechanical properties of GIC after reinforcement with 0.1 wt% of RGO and 3 wt% of the composites was evaluated using a one-way analysis of variance (ANOVA). It was verified slight improvements in the hardness of GIC. |
publishDate |
2020 |
dc.date.none.fl_str_mv |
2020-01-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000100210 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000100210 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/1980-5373-mr-2019-0580 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
ABM, ABC, ABPol |
publisher.none.fl_str_mv |
ABM, ABC, ABPol |
dc.source.none.fl_str_mv |
Materials Research v.23 n.1 2020 reponame:Materials research (São Carlos. Online) instname:Universidade Federal de São Carlos (UFSCAR) instacron:ABM ABC ABPOL |
instname_str |
Universidade Federal de São Carlos (UFSCAR) |
instacron_str |
ABM ABC ABPOL |
institution |
ABM ABC ABPOL |
reponame_str |
Materials research (São Carlos. Online) |
collection |
Materials research (São Carlos. Online) |
repository.name.fl_str_mv |
Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR) |
repository.mail.fl_str_mv |
dedz@power.ufscar.br |
_version_ |
1754212676825776128 |