Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement

Detalhes bibliográficos
Autor(a) principal: Benevides,Ana Paula
Data de Publicação: 2020
Outros Autores: Campos,Adriano Rocha, Vieira,Lanna Cristina, dos Reis Perez,Cesar, Cesar,Deborah Vargas
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Materials research (São Carlos. Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000100210
Resumo: Composites based on graphene oxide (GO), reduced graphene oxide (RGO) and zinc oxide (ZnO) with different mass ratios (8, 100 and 600) were synthesized through the hydrothermal method at 100 °C and used as reinforcement materials to commercial glass-ionomers cements (GIC). X-ray diffraction (XRD) characterization confirmed the graphite oxidation and ZnO formation as a wurtzite phase. Infrared spectroscopy analyses showed bands of oxygen-containing groups on the GO surface, which reduced after thermal treatment and RGO formation. D and G bands were observed in all samples synthesized, which presented morphology similar to flowers with a crystallite size of 18 nm. The effect on the mechanical properties of GIC after reinforcement with 0.1 wt% of RGO and 3 wt% of the composites was evaluated using a one-way analysis of variance (ANOVA). It was verified slight improvements in the hardness of GIC.
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spelling Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials ReinforcementReduced graphene oxideZnO compositesglass-ionomer cementmechanical propertiesphysicochemical characterizationComposites based on graphene oxide (GO), reduced graphene oxide (RGO) and zinc oxide (ZnO) with different mass ratios (8, 100 and 600) were synthesized through the hydrothermal method at 100 °C and used as reinforcement materials to commercial glass-ionomers cements (GIC). X-ray diffraction (XRD) characterization confirmed the graphite oxidation and ZnO formation as a wurtzite phase. Infrared spectroscopy analyses showed bands of oxygen-containing groups on the GO surface, which reduced after thermal treatment and RGO formation. D and G bands were observed in all samples synthesized, which presented morphology similar to flowers with a crystallite size of 18 nm. The effect on the mechanical properties of GIC after reinforcement with 0.1 wt% of RGO and 3 wt% of the composites was evaluated using a one-way analysis of variance (ANOVA). It was verified slight improvements in the hardness of GIC.ABM, ABC, ABPol2020-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000100210Materials Research v.23 n.1 2020reponame:Materials research (São Carlos. Online)instname:Universidade Federal de São Carlos (UFSCAR)instacron:ABM ABC ABPOL10.1590/1980-5373-mr-2019-0580info:eu-repo/semantics/openAccessBenevides,Ana PaulaCampos,Adriano RochaVieira,Lanna Cristinados Reis Perez,CesarCesar,Deborah Vargaseng2020-03-17T00:00:00Zoai:scielo:S1516-14392020000100210Revistahttp://www.scielo.br/mrPUBhttps://old.scielo.br/oai/scielo-oai.phpdedz@power.ufscar.br1980-53731516-1439opendoar:2020-03-17T00:00Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)false
dc.title.none.fl_str_mv Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
title Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
spellingShingle Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
Benevides,Ana Paula
Reduced graphene oxide
ZnO composites
glass-ionomer cement
mechanical properties
physicochemical characterization
title_short Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
title_full Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
title_fullStr Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
title_full_unstemmed Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
title_sort Reduced Graphene Oxide-Zinc Oxide Flower-Like Composite for Glass-Ionomer Materials Reinforcement
author Benevides,Ana Paula
author_facet Benevides,Ana Paula
Campos,Adriano Rocha
Vieira,Lanna Cristina
dos Reis Perez,Cesar
Cesar,Deborah Vargas
author_role author
author2 Campos,Adriano Rocha
Vieira,Lanna Cristina
dos Reis Perez,Cesar
Cesar,Deborah Vargas
author2_role author
author
author
author
dc.contributor.author.fl_str_mv Benevides,Ana Paula
Campos,Adriano Rocha
Vieira,Lanna Cristina
dos Reis Perez,Cesar
Cesar,Deborah Vargas
dc.subject.por.fl_str_mv Reduced graphene oxide
ZnO composites
glass-ionomer cement
mechanical properties
physicochemical characterization
topic Reduced graphene oxide
ZnO composites
glass-ionomer cement
mechanical properties
physicochemical characterization
description Composites based on graphene oxide (GO), reduced graphene oxide (RGO) and zinc oxide (ZnO) with different mass ratios (8, 100 and 600) were synthesized through the hydrothermal method at 100 °C and used as reinforcement materials to commercial glass-ionomers cements (GIC). X-ray diffraction (XRD) characterization confirmed the graphite oxidation and ZnO formation as a wurtzite phase. Infrared spectroscopy analyses showed bands of oxygen-containing groups on the GO surface, which reduced after thermal treatment and RGO formation. D and G bands were observed in all samples synthesized, which presented morphology similar to flowers with a crystallite size of 18 nm. The effect on the mechanical properties of GIC after reinforcement with 0.1 wt% of RGO and 3 wt% of the composites was evaluated using a one-way analysis of variance (ANOVA). It was verified slight improvements in the hardness of GIC.
publishDate 2020
dc.date.none.fl_str_mv 2020-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000100210
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392020000100210
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/1980-5373-mr-2019-0580
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv ABM, ABC, ABPol
publisher.none.fl_str_mv ABM, ABC, ABPol
dc.source.none.fl_str_mv Materials Research v.23 n.1 2020
reponame:Materials research (São Carlos. Online)
instname:Universidade Federal de São Carlos (UFSCAR)
instacron:ABM ABC ABPOL
instname_str Universidade Federal de São Carlos (UFSCAR)
instacron_str ABM ABC ABPOL
institution ABM ABC ABPOL
reponame_str Materials research (São Carlos. Online)
collection Materials research (São Carlos. Online)
repository.name.fl_str_mv Materials research (São Carlos. Online) - Universidade Federal de São Carlos (UFSCAR)
repository.mail.fl_str_mv dedz@power.ufscar.br
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