Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS)
| Autor(a) principal: | |
|---|---|
| Data de Publicação: | 2012 |
| Outros Autores: | , , , , , , |
| Tipo de documento: | Artigo |
| Idioma: | eng |
| Título da fonte: | Repositório Institucional da FIOCRUZ (ARCA) |
| Texto Completo: | https://www.arca.fiocruz.br/handle/icict/8633 http://dx.doi.org/10.1590/S0100-40422012000100013 |
Resumo: | Universidade Federal Rural do Rio de Janeiro. Instituto de Tecnologia. Seropédica, RJ, Brasil. / Instituto Nacional de Metrologia Normalização e Qualidade Industrial. Diretoria de Metrologia Científica e Industrial. Divisão de Metrologia Química. Duque de Caxias, Xerém, RJ, Brasil. |
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Bandeira, Raquel Duarte da Costa CunhaUekane, Thais MatsueCunha, Carolina Passos daGeaquinho, Luths Raquel de OliveiraCunha, Valnei Smarçaro daCaixeiro, Janaína Marques RodriguesGodoy, Ronoel Luiz de OliveiraCruz, Marcus Henrique Campino de La2014-10-20T15:26:10Z2014-10-20T15:26:10Z2012BANDEIRA, R. D. C. C. et al. Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS). Química Nova, São Paulo, v. 35, n. 1, p. 66-71, 2012.0100-4042https://www.arca.fiocruz.br/handle/icict/8633http://dx.doi.org/10.1590/S0100-40422012000100013engSociedade Brasileira de QuímicaDevelopment and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS)info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleUniversidade Federal Rural do Rio de Janeiro. Instituto de Tecnologia. Seropédica, RJ, Brasil. / Instituto Nacional de Metrologia Normalização e Qualidade Industrial. Diretoria de Metrologia Científica e Industrial. Divisão de Metrologia Química. Duque de Caxias, Xerém, RJ, Brasil.Instituto Nacional de Metrologia Normalização e Qualidade Industrial. Diretoria de Metrologia Científica e Industrial. Divisão de Metrologia Química. Duque de Caxias, Xerém, RJ, Brasil.Instituto Nacional de Metrologia Normalização e Qualidade Industrial. Diretoria de Metrologia Científica e Industrial. Divisão de Metrologia Química. Duque de Caxias, Xerém, RJ, Brasil.Instituto Nacional de Metrologia Normalização e Qualidade Industrial. Diretoria de Metrologia Científica e Industrial. Divisão de Metrologia Química. Duque de Caxias, Xerém, RJ, Brasil.Instituto Nacional de Metrologia Normalização e Qualidade Industrial. Diretoria de Metrologia Científica e Industrial. Divisão de Metrologia Química. Duque de Caxias, Xerém, RJ, Brasil.Instituto Nacional de Metrologia Normalização e Qualidade Industrial. Diretoria de Metrologia Científica e Industrial. Divisão de Metrologia Química. Duque de Caxias, Xerém, RJ, Brasil.Embrapa Agroindústria de Alimentos. Rio de Janeiro, RJ, Brasil.Fundação Oswaldo Cruz. Instituto Nacional de Controle de Qualidade em Saúde. Comissão do Programa de Ensaio de Proficiência de Produtos Sujeitos ao Regime de Vigilância Sanitária. Rio de Janeiro, RJ, Brasil.A method using LC/ESI-MS/MS for the quantitative analysis of Ochratoxin A in roasted coffee was described. Linearity was demonstrated (r = 0.9175). The limits of detection and quantification were 1.0 and 3.0 ng g-1, respectively. Trueness, repeatability and intermediate precision values were 89.0-108.8%; 2.4-13.7%; 12.5-17.8%, respectively. To the best of our knowledge, this is the first report in which Ochratoxin A in roasted coffee is analysed by LC/ESI-MS/MS, contributing to the field of mycotoxin analysis, and it will be used for future production of Certified Reference Material.CoffeeOchratoxin ALC/ESI-MS/MSCaféOcratoxinasCromatografia Gasosa-Espectrometria de Massasinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da FIOCRUZ (ARCA)instname:Fundação Oswaldo Cruz (FIOCRUZ)instacron:FIOCRUZLICENSElicense.txtlicense.txttext/plain; charset=utf-81914https://www.arca.fiocruz.br/bitstream/icict/8633/1/license.txt7d48279ffeed55da8dfe2f8e81f3b81fMD51ORIGINALQuim Nova_35_66-71.pdfQuim Nova_35_66-71.pdfapplication/pdf425122https://www.arca.fiocruz.br/bitstream/icict/8633/2/Quim%20Nova_35_66-71.pdf3d9b32a7ffd5d13b170918a51cdf4f32MD52TEXTQuim Nova_35_66-71.pdf.txtQuim Nova_35_66-71.pdf.txtExtracted texttext/plain31514https://www.arca.fiocruz.br/bitstream/icict/8633/3/Quim%20Nova_35_66-71.pdf.txt490cf92ce6519b623984d4c77364e205MD53icict/86332018-04-05 23:45:37.002oai:www.arca.fiocruz.br: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ório InstitucionalPUBhttps://www.arca.fiocruz.br/oai/requestrepositorio.arca@fiocruz.bropendoar:21352018-04-06T02:45:37Repositório Institucional da FIOCRUZ (ARCA) - Fundação Oswaldo Cruz (FIOCRUZ)false |
| dc.title.en.fl_str_mv |
Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS) |
| title |
Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS) |
| spellingShingle |
Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS) Bandeira, Raquel Duarte da Costa Cunha Coffee Ochratoxin A LC/ESI-MS/MS Café Ocratoxinas Cromatografia Gasosa-Espectrometria de Massas |
| title_short |
Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS) |
| title_full |
Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS) |
| title_fullStr |
Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS) |
| title_full_unstemmed |
Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS) |
| title_sort |
Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS) |
| author |
Bandeira, Raquel Duarte da Costa Cunha |
| author_facet |
Bandeira, Raquel Duarte da Costa Cunha Uekane, Thais Matsue Cunha, Carolina Passos da Geaquinho, Luths Raquel de Oliveira Cunha, Valnei Smarçaro da Caixeiro, Janaína Marques Rodrigues Godoy, Ronoel Luiz de Oliveira Cruz, Marcus Henrique Campino de La |
| author_role |
author |
| author2 |
Uekane, Thais Matsue Cunha, Carolina Passos da Geaquinho, Luths Raquel de Oliveira Cunha, Valnei Smarçaro da Caixeiro, Janaína Marques Rodrigues Godoy, Ronoel Luiz de Oliveira Cruz, Marcus Henrique Campino de La |
| author2_role |
author author author author author author author |
| dc.contributor.author.fl_str_mv |
Bandeira, Raquel Duarte da Costa Cunha Uekane, Thais Matsue Cunha, Carolina Passos da Geaquinho, Luths Raquel de Oliveira Cunha, Valnei Smarçaro da Caixeiro, Janaína Marques Rodrigues Godoy, Ronoel Luiz de Oliveira Cruz, Marcus Henrique Campino de La |
| dc.subject.en.en.fl_str_mv |
Coffee Ochratoxin A LC/ESI-MS/MS |
| topic |
Coffee Ochratoxin A LC/ESI-MS/MS Café Ocratoxinas Cromatografia Gasosa-Espectrometria de Massas |
| dc.subject.decs.pt_BR.fl_str_mv |
Café Ocratoxinas Cromatografia Gasosa-Espectrometria de Massas |
| description |
Universidade Federal Rural do Rio de Janeiro. Instituto de Tecnologia. Seropédica, RJ, Brasil. / Instituto Nacional de Metrologia Normalização e Qualidade Industrial. Diretoria de Metrologia Científica e Industrial. Divisão de Metrologia Química. Duque de Caxias, Xerém, RJ, Brasil. |
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2012 |
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2012 |
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2014-10-20T15:26:10Z |
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2014-10-20T15:26:10Z |
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info:eu-repo/semantics/article |
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BANDEIRA, R. D. C. C. et al. Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS). Química Nova, São Paulo, v. 35, n. 1, p. 66-71, 2012. |
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https://www.arca.fiocruz.br/handle/icict/8633 |
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0100-4042 |
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http://dx.doi.org/10.1590/S0100-40422012000100013 |
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BANDEIRA, R. D. C. C. et al. Development and validation of a method for the analysis of Ochratoxin A in roasted coffee by liquid chromatography/electrospray-mass spectrometry in Tandem (LC/ESI-MS/MS). Química Nova, São Paulo, v. 35, n. 1, p. 66-71, 2012. 0100-4042 |
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https://www.arca.fiocruz.br/handle/icict/8633 http://dx.doi.org/10.1590/S0100-40422012000100013 |
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Sociedade Brasileira de Química |
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Sociedade Brasileira de Química |
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