Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.

Detalhes bibliográficos
Autor(a) principal: SANTOS-OLIVEIRA, Ralph
Data de Publicação: 2011
Outros Autores: CUSTÓDIO, Cintia de Andrade, FUSCO, Alessandra Silva, FERNANDES, Ricardo Ribeiro Alves, SEQNR, roliveira@ien.gov.br, http://lattes.cnpq.br/2376670019296363, IEN
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional do IEN
Texto Completo: http://carpedien.ien.gov.br:8080/handle/ien/1620
Resumo: A gas chromatographic method for determination of ethanol in an fluorodeoxyglucose (FDG)-18 solution was developed. The pre-validation tests were made to test some parameters. Three samples in the concentration of 400, 4000 and 7200 ppm, respectively were analyzed using the novel methodology. The results of the technique were not good. Although the method seems to be capable to identify ethanol in solution, the pre-validation demonstrated a problem in the technique. The linearity results showed an R2 of 0.66. Further tests must be made to implement this technique in a daily routine.
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spelling SANTOS-OLIVEIRA, RalphCUSTÓDIO, Cintia de AndradeFUSCO, Alessandra SilvaFERNANDES, Ricardo Ribeiro AlvesSEQNRroliveira@ien.gov.brhttp://lattes.cnpq.br/2376670019296363IEN2015-11-12T15:43:06Z2015-11-12T15:43:06Z2011-0614 apr. 2011.1996-0840http://carpedien.ien.gov.br:8080/handle/ien/1620Submitted by Jéssica Ramos (jessicafslr@yahoo.com.br) on 2015-11-12T15:43:06Z No. of bitstreams: 1 Analysis of gas-chromatographic method for the.pdf: 102532 bytes, checksum: 43bcd0828aed892362de3e707278cb57 (MD5)Made available in DSpace on 2015-11-12T15:43:06Z (GMT). No. of bitstreams: 1 Analysis of gas-chromatographic method for the.pdf: 102532 bytes, checksum: 43bcd0828aed892362de3e707278cb57 (MD5) Previous issue date: 2011-06A gas chromatographic method for determination of ethanol in an fluorodeoxyglucose (FDG)-18 solution was developed. The pre-validation tests were made to test some parameters. Three samples in the concentration of 400, 4000 and 7200 ppm, respectively were analyzed using the novel methodology. The results of the technique were not good. Although the method seems to be capable to identify ethanol in solution, the pre-validation demonstrated a problem in the technique. The linearity results showed an R2 of 0.66. Further tests must be made to implement this technique in a daily routine.engInstituto de Engenharia NuclearIENBrasilValidationchemical analysisquality control.Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articlev. 5,n. 6,p. 155-157.info:eu-repo/semantics/openAccessreponame:Repositório Institucional do IENinstname:Instituto de Engenharia Nuclearinstacron:IENLICENSElicense.txtlicense.txttext/plain; charset=utf-81748http://carpedien.ien.gov.br:8080/xmlui/bitstream/ien/1620/2/license.txt8a4605be74aa9ea9d79846c1fba20a33MD52ORIGINALAnalysis of gas-chromatographic method for the.pdfAnalysis of gas-chromatographic method for the.pdfapplication/pdf102532http://carpedien.ien.gov.br:8080/xmlui/bitstream/ien/1620/1/Analysis+of+gas-chromatographic+method+for+the.pdf43bcd0828aed892362de3e707278cb57MD51ien/1620oai:carpedien.ien.gov.br:ien/16202015-12-14 13:39:27.71Dspace IENlsales@ien.gov.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
dc.title.pt_BR.fl_str_mv Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.
title Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.
spellingShingle Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.
SANTOS-OLIVEIRA, Ralph
Validation
chemical analysis
quality control.
title_short Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.
title_full Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.
title_fullStr Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.
title_full_unstemmed Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.
title_sort Analysis of gas-chromatographic method for the determination of ethanol in an 18-F-fluorodeoxyglucose (FDG-18) solution: shor communication.
author SANTOS-OLIVEIRA, Ralph
author_facet SANTOS-OLIVEIRA, Ralph
CUSTÓDIO, Cintia de Andrade
FUSCO, Alessandra Silva
FERNANDES, Ricardo Ribeiro Alves
SEQNR
roliveira@ien.gov.br
http://lattes.cnpq.br/2376670019296363
IEN
author_role author
author2 CUSTÓDIO, Cintia de Andrade
FUSCO, Alessandra Silva
FERNANDES, Ricardo Ribeiro Alves
SEQNR
roliveira@ien.gov.br
http://lattes.cnpq.br/2376670019296363
IEN
author2_role author
author
author
author
author
author
author
dc.contributor.author.fl_str_mv SANTOS-OLIVEIRA, Ralph
CUSTÓDIO, Cintia de Andrade
FUSCO, Alessandra Silva
FERNANDES, Ricardo Ribeiro Alves
SEQNR
roliveira@ien.gov.br
http://lattes.cnpq.br/2376670019296363
IEN
dc.subject.por.fl_str_mv Validation
chemical analysis
quality control.
topic Validation
chemical analysis
quality control.
dc.description.abstract.por.fl_txt_mv A gas chromatographic method for determination of ethanol in an fluorodeoxyglucose (FDG)-18 solution was developed. The pre-validation tests were made to test some parameters. Three samples in the concentration of 400, 4000 and 7200 ppm, respectively were analyzed using the novel methodology. The results of the technique were not good. Although the method seems to be capable to identify ethanol in solution, the pre-validation demonstrated a problem in the technique. The linearity results showed an R2 of 0.66. Further tests must be made to implement this technique in a daily routine.
description A gas chromatographic method for determination of ethanol in an fluorodeoxyglucose (FDG)-18 solution was developed. The pre-validation tests were made to test some parameters. Three samples in the concentration of 400, 4000 and 7200 ppm, respectively were analyzed using the novel methodology. The results of the technique were not good. Although the method seems to be capable to identify ethanol in solution, the pre-validation demonstrated a problem in the technique. The linearity results showed an R2 of 0.66. Further tests must be made to implement this technique in a daily routine.
publishDate 2011
dc.date.accepted.none.fl_str_mv 14 apr. 2011.
dc.date.issued.fl_str_mv 2011-06
dc.date.accessioned.fl_str_mv 2015-11-12T15:43:06Z
dc.date.available.fl_str_mv 2015-11-12T15:43:06Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
status_str publishedVersion
format article
dc.identifier.uri.fl_str_mv http://carpedien.ien.gov.br:8080/handle/ien/1620
dc.identifier.issn.none.fl_str_mv 1996-0840
identifier_str_mv 1996-0840
url http://carpedien.ien.gov.br:8080/handle/ien/1620
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv Instituto de Engenharia Nuclear
dc.publisher.initials.fl_str_mv IEN
dc.publisher.country.fl_str_mv Brasil
publisher.none.fl_str_mv Instituto de Engenharia Nuclear
dc.source.none.fl_str_mv reponame:Repositório Institucional do IEN
instname:Instituto de Engenharia Nuclear
instacron:IEN
reponame_str Repositório Institucional do IEN
collection Repositório Institucional do IEN
instname_str Instituto de Engenharia Nuclear
instacron_str IEN
institution IEN
bitstream.url.fl_str_mv http://carpedien.ien.gov.br:8080/xmlui/bitstream/ien/1620/2/license.txt
http://carpedien.ien.gov.br:8080/xmlui/bitstream/ien/1620/1/Analysis+of+gas-chromatographic+method+for+the.pdf
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