Synthesis, crystal structure and biological activity of novel diester cyclophanes
Autor(a) principal: | |
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Data de Publicação: | 2012 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Journal of the Brazilian Chemical Society (Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532012001000002 |
Resumo: | A series of novel diester cyclophanes was synthesized by esterification of 1,2-benzenedicarbonyl chloride with eight different diols under high dilution conditions. The structures of the compounds were verified by elemental analysis, ¹H nuclear magnetic resonance (NMR), IR spectroscopy and high resolution mass spectrometry (HRMS). The crystal structures of two compounds were characterized by single crystal X-ray diffractometry (XRD). All the new cyclophanes were evaluated for biological activities and the results showed that some of these compounds have low antibacterial or antifungal activities. |
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Journal of the Brazilian Chemical Society (Online) |
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Synthesis, crystal structure and biological activity of novel diester cyclophanessynthesisester cyclophanescrystalantibacterial activityantifungal activityA series of novel diester cyclophanes was synthesized by esterification of 1,2-benzenedicarbonyl chloride with eight different diols under high dilution conditions. The structures of the compounds were verified by elemental analysis, ¹H nuclear magnetic resonance (NMR), IR spectroscopy and high resolution mass spectrometry (HRMS). The crystal structures of two compounds were characterized by single crystal X-ray diffractometry (XRD). All the new cyclophanes were evaluated for biological activities and the results showed that some of these compounds have low antibacterial or antifungal activities.Sociedade Brasileira de Química2012-10-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532012001000002Journal of the Brazilian Chemical Society v.23 n.10 2012reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.1590/S0103-50532012005000045info:eu-repo/semantics/openAccessZhang,PengfeiYang,BingqinFang,XianwenCheng,ZhaoYang,Meipaneng2012-12-05T00:00:00Zoai:scielo:S0103-50532012001000002Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2012-12-05T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false |
dc.title.none.fl_str_mv |
Synthesis, crystal structure and biological activity of novel diester cyclophanes |
title |
Synthesis, crystal structure and biological activity of novel diester cyclophanes |
spellingShingle |
Synthesis, crystal structure and biological activity of novel diester cyclophanes Zhang,Pengfei synthesis ester cyclophanes crystal antibacterial activity antifungal activity |
title_short |
Synthesis, crystal structure and biological activity of novel diester cyclophanes |
title_full |
Synthesis, crystal structure and biological activity of novel diester cyclophanes |
title_fullStr |
Synthesis, crystal structure and biological activity of novel diester cyclophanes |
title_full_unstemmed |
Synthesis, crystal structure and biological activity of novel diester cyclophanes |
title_sort |
Synthesis, crystal structure and biological activity of novel diester cyclophanes |
author |
Zhang,Pengfei |
author_facet |
Zhang,Pengfei Yang,Bingqin Fang,Xianwen Cheng,Zhao Yang,Meipan |
author_role |
author |
author2 |
Yang,Bingqin Fang,Xianwen Cheng,Zhao Yang,Meipan |
author2_role |
author author author author |
dc.contributor.author.fl_str_mv |
Zhang,Pengfei Yang,Bingqin Fang,Xianwen Cheng,Zhao Yang,Meipan |
dc.subject.por.fl_str_mv |
synthesis ester cyclophanes crystal antibacterial activity antifungal activity |
topic |
synthesis ester cyclophanes crystal antibacterial activity antifungal activity |
description |
A series of novel diester cyclophanes was synthesized by esterification of 1,2-benzenedicarbonyl chloride with eight different diols under high dilution conditions. The structures of the compounds were verified by elemental analysis, ¹H nuclear magnetic resonance (NMR), IR spectroscopy and high resolution mass spectrometry (HRMS). The crystal structures of two compounds were characterized by single crystal X-ray diffractometry (XRD). All the new cyclophanes were evaluated for biological activities and the results showed that some of these compounds have low antibacterial or antifungal activities. |
publishDate |
2012 |
dc.date.none.fl_str_mv |
2012-10-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532012001000002 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532012001000002 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/S0103-50532012005000045 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
dc.source.none.fl_str_mv |
Journal of the Brazilian Chemical Society v.23 n.10 2012 reponame:Journal of the Brazilian Chemical Society (Online) instname:Sociedade Brasileira de Química (SBQ) instacron:SBQ |
instname_str |
Sociedade Brasileira de Química (SBQ) |
instacron_str |
SBQ |
institution |
SBQ |
reponame_str |
Journal of the Brazilian Chemical Society (Online) |
collection |
Journal of the Brazilian Chemical Society (Online) |
repository.name.fl_str_mv |
Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ) |
repository.mail.fl_str_mv |
||office@jbcs.sbq.org.br |
_version_ |
1750318174363975680 |