Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy

Detalhes bibliográficos
Autor(a) principal: Monte,F.J.Q.
Data de Publicação: 1998
Outros Autores: Kintzinger,J.P.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Journal of the Brazilian Chemical Society (Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50531998000100005
Resumo: The complete ¹H and 13C chemical shift assignments of extended hydrogen spin systems in triterpenoid derivatives (methyl 2alpha, 3beta, 24-tri-O-acetylurs-12-en-28-oate and methyl 2alpha, 3beta, 24-tri-O-acetylolean-12-en-28-oate) was accomplished making use of one and two dimensional NMR techniques (HMBC, HMQC, COSY and NOESY).
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spelling Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopytriterpenoidscomplete ¹H and 13C-NMR signal assignments1D NMR; 2D NMR (¹H x 13C-HMBC, ¹H x 13C -HMQC, ¹H x ¹H-COSY, ¹H x ¹H-NOESY)The complete ¹H and 13C chemical shift assignments of extended hydrogen spin systems in triterpenoid derivatives (methyl 2alpha, 3beta, 24-tri-O-acetylurs-12-en-28-oate and methyl 2alpha, 3beta, 24-tri-O-acetylolean-12-en-28-oate) was accomplished making use of one and two dimensional NMR techniques (HMBC, HMQC, COSY and NOESY).Sociedade Brasileira de Química1998-02-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50531998000100005Journal of the Brazilian Chemical Society v.9 n.1 1998reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.1590/S0103-50531998000100005info:eu-repo/semantics/openAccessMonte,F.J.Q.Kintzinger,J.P.eng2008-03-17T00:00:00Zoai:scielo:S0103-50531998000100005Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2008-03-17T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false
dc.title.none.fl_str_mv Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
title Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
spellingShingle Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
Monte,F.J.Q.
triterpenoids
complete ¹H and 13C-NMR signal assignments
1D NMR; 2D NMR (¹H x 13C-HMBC, ¹H x 13C -HMQC, ¹H x ¹H-COSY, ¹H x ¹H-NOESY)
title_short Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
title_full Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
title_fullStr Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
title_full_unstemmed Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
title_sort Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
author Monte,F.J.Q.
author_facet Monte,F.J.Q.
Kintzinger,J.P.
author_role author
author2 Kintzinger,J.P.
author2_role author
dc.contributor.author.fl_str_mv Monte,F.J.Q.
Kintzinger,J.P.
dc.subject.por.fl_str_mv triterpenoids
complete ¹H and 13C-NMR signal assignments
1D NMR; 2D NMR (¹H x 13C-HMBC, ¹H x 13C -HMQC, ¹H x ¹H-COSY, ¹H x ¹H-NOESY)
topic triterpenoids
complete ¹H and 13C-NMR signal assignments
1D NMR; 2D NMR (¹H x 13C-HMBC, ¹H x 13C -HMQC, ¹H x ¹H-COSY, ¹H x ¹H-NOESY)
description The complete ¹H and 13C chemical shift assignments of extended hydrogen spin systems in triterpenoid derivatives (methyl 2alpha, 3beta, 24-tri-O-acetylurs-12-en-28-oate and methyl 2alpha, 3beta, 24-tri-O-acetylolean-12-en-28-oate) was accomplished making use of one and two dimensional NMR techniques (HMBC, HMQC, COSY and NOESY).
publishDate 1998
dc.date.none.fl_str_mv 1998-02-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50531998000100005
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50531998000100005
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/S0103-50531998000100005
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Sociedade Brasileira de Química
publisher.none.fl_str_mv Sociedade Brasileira de Química
dc.source.none.fl_str_mv Journal of the Brazilian Chemical Society v.9 n.1 1998
reponame:Journal of the Brazilian Chemical Society (Online)
instname:Sociedade Brasileira de Química (SBQ)
instacron:SBQ
instname_str Sociedade Brasileira de Química (SBQ)
instacron_str SBQ
institution SBQ
reponame_str Journal of the Brazilian Chemical Society (Online)
collection Journal of the Brazilian Chemical Society (Online)
repository.name.fl_str_mv Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)
repository.mail.fl_str_mv ||office@jbcs.sbq.org.br
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