Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas

Detalhes bibliográficos
Autor(a) principal: Oliveira, Bruno José Silva de
Data de Publicação: 2015
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da UFSCAR
Texto Completo: https://repositorio.ufscar.br/handle/ufscar/7168
Resumo: Nowadays, titanium and its alloys are the materials of choice for the production of implants for hip arthroplasty, a surgery that aims for the improvement of the quality of life of patients that bear articular pathologies of the hip. With the increase of life expectancy, it becomes more and more important that these implants withstand greater times of implantation, avoiding revision surgeries, which represent higher costs and risks. Today, this need is approached by different ways, among them the functionalization of surfaces, that permit better osseointegration of the prosthesis at the site of implantation and, consequently, better results on the application of products in the long term. One of the ways to perform this functionalization is through chemical etching, one of which (H3PO4+NaOH) has been chosen to perform modification of surfaces previously treated by titanium plasma spray (TPS+AQ) on finished femoral prostheses. As a control, another group of prostheses was employed, treated with technology already in the market, coated by titanium plasma spray with posterior deposition of two phases of calcium phosphate with different solubility (TPS+HA). The prostheses were submitted to topographical analyses via SEM, analyses of roughness profiles and increase of effective surface area by confocal microscopy and transversal analyses of coatings via SEM, subsequently treated by image analysis software for determination of attributes of porous coatings according to ASTM F1854. After that, all prostheses were tested to evaluate their fatigue behavior according to ISO 7206-4 and the presence of cracks via penetrant liquid testing. All the specimens survived the fatigue test, refuting the hypothesis that the modification via TPS+AQ reduces the fatigue resistance of femoral stems when compared to a control group, TPS+HA, under a normalized test protocol.
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spelling Oliveira, Bruno José Silva deBolfarini, Claudemirohttp://lattes.cnpq.br/9231627080617037Oliveira, Nilson Tadeu Camarinho dehttp://lattes.cnpq.br/5165925219822865http://lattes.cnpq.br/39394427056819407b18c503-0189-44ab-b755-805a820126d32016-09-15T13:39:49Z2016-09-15T13:39:49Z2015-07-20OLIVEIRA, Bruno José Silva de. Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas. 2015. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2015. Disponível em: https://repositorio.ufscar.br/handle/ufscar/7168.https://repositorio.ufscar.br/handle/ufscar/7168Nowadays, titanium and its alloys are the materials of choice for the production of implants for hip arthroplasty, a surgery that aims for the improvement of the quality of life of patients that bear articular pathologies of the hip. With the increase of life expectancy, it becomes more and more important that these implants withstand greater times of implantation, avoiding revision surgeries, which represent higher costs and risks. Today, this need is approached by different ways, among them the functionalization of surfaces, that permit better osseointegration of the prosthesis at the site of implantation and, consequently, better results on the application of products in the long term. One of the ways to perform this functionalization is through chemical etching, one of which (H3PO4+NaOH) has been chosen to perform modification of surfaces previously treated by titanium plasma spray (TPS+AQ) on finished femoral prostheses. As a control, another group of prostheses was employed, treated with technology already in the market, coated by titanium plasma spray with posterior deposition of two phases of calcium phosphate with different solubility (TPS+HA). The prostheses were submitted to topographical analyses via SEM, analyses of roughness profiles and increase of effective surface area by confocal microscopy and transversal analyses of coatings via SEM, subsequently treated by image analysis software for determination of attributes of porous coatings according to ASTM F1854. After that, all prostheses were tested to evaluate their fatigue behavior according to ISO 7206-4 and the presence of cracks via penetrant liquid testing. All the specimens survived the fatigue test, refuting the hypothesis that the modification via TPS+AQ reduces the fatigue resistance of femoral stems when compared to a control group, TPS+HA, under a normalized test protocol.Atualmente o titânio e suas ligas são os materiais mais usados para a produção de implantes para artroplastia total de quadril, cirurgia que visa a melhoria da qualidade de vida de pacientes com patologias articulares nessa região do corpo. Com o aumento da expectativa de vida, torna-se cada vez mais importante que esses implantes resistam a tempos maiores de implantação, evitando cirurgias de revisão, que representam riscos e custos mais elevados. Essa necessidade é abordada atualmente por vias diferentes, entre elas a funcionalização de superfícies, que permitem melhor osseointegração da prótese no local de implantação e, consequentemente, melhores resultados de aplicação dos produtos no longo prazo. Uma das maneiras de se realizar essa funcionalização é através de ataques químicos, um dos quais (H3PO4+NaOH) foi escolhido para se realizar modificação de superfícies previamente tratadas por plasma spray de titânio (TPS+AQ) em próteses femorais acabadas. Como controle, foi usado um outro grupo de próteses com tecnologia já presente no mercado, recobertas por plasma spray de titânio com posterior deposição de duas fases de fosfato de cálcio com solubilidades diferentes (TPS+HA). As próteses foram submetidas a análise topográfica via MEV, análise de perfis de rugosidade e aumento de área de superfície efetiva via microscopia confocal e análise transversal de recobrimentos via MEV, tratadas através de software de análise de imagens para determinação de atributos de camadas porosas segundo a norma ASTM F1854. Depois da caracterização, todas as próteses foram ensaiadas em fadiga de acordo com a norma ISO 7206-4 e testadas via ensaio de líquido penetrante. Todos os corpos de prova sobreviveram ao ensaio de fadiga, refutando a hipótese de que modificação via TPS+AQ reduz a resistência à fadiga de hastes femorais em comparação com o grupo de controle, TPS+HA, sob um protocolo de ensaio normalizado.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)porUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarTitânioFadigaAtaque químicoPlasma sprayModificação superficialENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA DE TRANSFORMACAOComportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadasFatigue behavior of femoral stems for hip arthroplasty with modified surfacesinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisOnline600600ea2697dd-8d22-4c7a-8bdd-487c739e04c7info:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALDissBJSO.pdfDissBJSO.pdfapplication/pdf12242654https://repositorio.ufscar.br/bitstream/ufscar/7168/1/DissBJSO.pdf46859912b59c4c6962a659c6212f4d3aMD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81957https://repositorio.ufscar.br/bitstream/ufscar/7168/2/license.txtae0398b6f8b235e40ad82cba6c50031dMD52TEXTDissBJSO.pdf.txtDissBJSO.pdf.txtExtracted texttext/plain169579https://repositorio.ufscar.br/bitstream/ufscar/7168/3/DissBJSO.pdf.txt4110ab00b73e93cfda2d44b9f018ce0dMD53THUMBNAILDissBJSO.pdf.jpgDissBJSO.pdf.jpgIM Thumbnailimage/jpeg6447https://repositorio.ufscar.br/bitstream/ufscar/7168/4/DissBJSO.pdf.jpg6a4b993672aac2ccd4a6f5ac09ea6e4aMD54ufscar/71682023-09-18 18:30:44.238oai:repositorio.ufscar.br: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Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-09-18T18:30:44Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas
dc.title.alternative.eng.fl_str_mv Fatigue behavior of femoral stems for hip arthroplasty with modified surfaces
title Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas
spellingShingle Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas
Oliveira, Bruno José Silva de
Titânio
Fadiga
Ataque químico
Plasma spray
Modificação superficial
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA DE TRANSFORMACAO
title_short Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas
title_full Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas
title_fullStr Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas
title_full_unstemmed Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas
title_sort Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas
author Oliveira, Bruno José Silva de
author_facet Oliveira, Bruno José Silva de
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/3939442705681940
dc.contributor.author.fl_str_mv Oliveira, Bruno José Silva de
dc.contributor.advisor1.fl_str_mv Bolfarini, Claudemiro
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/9231627080617037
dc.contributor.advisor-co1.fl_str_mv Oliveira, Nilson Tadeu Camarinho de
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/5165925219822865
dc.contributor.authorID.fl_str_mv 7b18c503-0189-44ab-b755-805a820126d3
contributor_str_mv Bolfarini, Claudemiro
Oliveira, Nilson Tadeu Camarinho de
dc.subject.por.fl_str_mv Titânio
Fadiga
Ataque químico
Plasma spray
Modificação superficial
topic Titânio
Fadiga
Ataque químico
Plasma spray
Modificação superficial
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA DE TRANSFORMACAO
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA::METALURGIA DE TRANSFORMACAO
description Nowadays, titanium and its alloys are the materials of choice for the production of implants for hip arthroplasty, a surgery that aims for the improvement of the quality of life of patients that bear articular pathologies of the hip. With the increase of life expectancy, it becomes more and more important that these implants withstand greater times of implantation, avoiding revision surgeries, which represent higher costs and risks. Today, this need is approached by different ways, among them the functionalization of surfaces, that permit better osseointegration of the prosthesis at the site of implantation and, consequently, better results on the application of products in the long term. One of the ways to perform this functionalization is through chemical etching, one of which (H3PO4+NaOH) has been chosen to perform modification of surfaces previously treated by titanium plasma spray (TPS+AQ) on finished femoral prostheses. As a control, another group of prostheses was employed, treated with technology already in the market, coated by titanium plasma spray with posterior deposition of two phases of calcium phosphate with different solubility (TPS+HA). The prostheses were submitted to topographical analyses via SEM, analyses of roughness profiles and increase of effective surface area by confocal microscopy and transversal analyses of coatings via SEM, subsequently treated by image analysis software for determination of attributes of porous coatings according to ASTM F1854. After that, all prostheses were tested to evaluate their fatigue behavior according to ISO 7206-4 and the presence of cracks via penetrant liquid testing. All the specimens survived the fatigue test, refuting the hypothesis that the modification via TPS+AQ reduces the fatigue resistance of femoral stems when compared to a control group, TPS+HA, under a normalized test protocol.
publishDate 2015
dc.date.issued.fl_str_mv 2015-07-20
dc.date.accessioned.fl_str_mv 2016-09-15T13:39:49Z
dc.date.available.fl_str_mv 2016-09-15T13:39:49Z
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dc.identifier.citation.fl_str_mv OLIVEIRA, Bruno José Silva de. Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas. 2015. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2015. Disponível em: https://repositorio.ufscar.br/handle/ufscar/7168.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/7168
identifier_str_mv OLIVEIRA, Bruno José Silva de. Comportamento em fadiga de hastes femorais para artroplastia de quadril com superfícies modificadas. 2015. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2015. Disponível em: https://repositorio.ufscar.br/handle/ufscar/7168.
url https://repositorio.ufscar.br/handle/ufscar/7168
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dc.publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
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Câmpus São Carlos
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