Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)

Detalhes bibliográficos
Autor(a) principal: Silva, Gisela Benatti
Data de Publicação: 2015
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)
Texto Completo: http://repositorio.ufes.br/handle/10/1522
Resumo: The aim of this study was to develop and characterize a water-soluble extract sesame-based to be used as a possible substitute for cow's milk and soy extract. A model kinetic of the absorption of water has been proposed during the maceration stage in which estimated ideal time to beat of the sesame mash and this stage influences the yield of the product. Afterwards with the aim to know the influence of the beat time (0.45 min to 14.55 min) and the extract concentration (1.925% to 23.07%) were evaluated by a central composite rotational design (CCRD) that is, a design 22 including 4 test axial conditions and the 5 repetitions at the central point totaling 13 experiments. All design of the tests was carried out analysis of viscosity, color, soluble solids and yield. The same analyzes were carried out in samples of commercial cow's milk and soy water soluble extract with the purpose of comparison. After the realization this step was possible to selection of some samples for preparation of water soluble extract of sesame and then was carried out physicochemical analysis (protein, ash, lipids, carbohydrates) and determined the antioxidant capacity by ABTS and level of compounds phenolics such samples. As regards the yield analysis there was no significant difference of the amount of extract obtained at different temperatures for maceration by Tukey test (p> 0.05). The CCRD was performed in the Statistica software and were selected for trials 1, 2, 6, 7, CP (center point) which more samples were similar with commercial samples studied. In these samples was carried out physico-chemical analysis in addition to antioxidant capacity and phenolic compounds. The total solids content in the sample 6 was higher than the other samples, differing significantly from the other samples (p> 0.05). As for the lipids, ash and proteins found in samples 6 and PC were higher than the other samples, while the sample 7 exhibited the lowest level of lipids and proteins, considering that the ash content samples 1,2 and 7 were statistically the same. The carbohydrate content calculated by difference was higher in samples 1,2 and 7 and the lowest value in the sample 6. The values of antioxidant capacity and phenolic compounds were not statistically different from each other at 5% probability. It is has therefore concluded that the soaking step did not affect the yield of the final product, this step is unnecessary. From the physico-chemical analysis it can be concluded that the sesame water soluble extract in certain samples showed a better performance in terms of nutritional value compared to the soy extract.
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spelling Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)Cinética de maceraçãoSubstituto lácteoExtrato aquosoTempo de batimento (Alimentos)MaceraçãoDCCRSubstituto lácteoMacerationMilk substituteGergelimCiência e Tecnologia de Alimentos664The aim of this study was to develop and characterize a water-soluble extract sesame-based to be used as a possible substitute for cow's milk and soy extract. A model kinetic of the absorption of water has been proposed during the maceration stage in which estimated ideal time to beat of the sesame mash and this stage influences the yield of the product. Afterwards with the aim to know the influence of the beat time (0.45 min to 14.55 min) and the extract concentration (1.925% to 23.07%) were evaluated by a central composite rotational design (CCRD) that is, a design 22 including 4 test axial conditions and the 5 repetitions at the central point totaling 13 experiments. All design of the tests was carried out analysis of viscosity, color, soluble solids and yield. The same analyzes were carried out in samples of commercial cow's milk and soy water soluble extract with the purpose of comparison. After the realization this step was possible to selection of some samples for preparation of water soluble extract of sesame and then was carried out physicochemical analysis (protein, ash, lipids, carbohydrates) and determined the antioxidant capacity by ABTS and level of compounds phenolics such samples. As regards the yield analysis there was no significant difference of the amount of extract obtained at different temperatures for maceration by Tukey test (p> 0.05). The CCRD was performed in the Statistica software and were selected for trials 1, 2, 6, 7, CP (center point) which more samples were similar with commercial samples studied. In these samples was carried out physico-chemical analysis in addition to antioxidant capacity and phenolic compounds. The total solids content in the sample 6 was higher than the other samples, differing significantly from the other samples (p> 0.05). As for the lipids, ash and proteins found in samples 6 and PC were higher than the other samples, while the sample 7 exhibited the lowest level of lipids and proteins, considering that the ash content samples 1,2 and 7 were statistically the same. The carbohydrate content calculated by difference was higher in samples 1,2 and 7 and the lowest value in the sample 6. The values of antioxidant capacity and phenolic compounds were not statistically different from each other at 5% probability. It is has therefore concluded that the soaking step did not affect the yield of the final product, this step is unnecessary. From the physico-chemical analysis it can be concluded that the sesame water soluble extract in certain samples showed a better performance in terms of nutritional value compared to the soy extract.O objetivo do presente estudo foi elaborar e caracterizar um extrato hidrossolúvel à base de gergelim para ser usado como possível substituto do leite de vaca e extrato de soja. Foi proposto um modelo de cinética de absorção de água durante a etapa de maceração no qual estimou o tempo ideal de batimento do gergelim macerado e se essa etapa influencia no rendimento do produto. Posteriormente com o objetivo de saber a influência do tempo de batimento (0,45 min a 14,55 min) e a concentração do extrato (1,925% a 23,07%) foram avaliadas através de um delineamento composto central rotacional (DCCR), ou seja, um delineamento 22 incluindo 4 ensaios nas condições axiais e 5 repetições no ponto central, totalizando 13 experimentos. Para todos os ensaios do delineamento realizou-se análises de viscosidade, cor, sólidos solúveis totais e rendimento. As mesmas análises foram realizadas em amostras comerciais de leite de vaca e extrato hidrossolúvel de soja com o intuito de comparação. Após a realização dessa etapa foi possível à seleção de algumas amostras para elaboração do extrato hidrossolúvel de gergelim e então realizou-se análises físico-químicas (proteína, cinzas, lipídios, carboidratos) e determinou-se a capacidade antioxidante por ABTS e teor de compostos fenólicos de tais amostras. Quanto à análise de rendimento não houve diferença significativa da quantidade de extrato obtido em diferentes temperaturas de maceração pelo teste de Tukey (p> 0,05). O DCCR foi realizado no programa Statistica e selecionaram-se os ensaios 1, 2, 6, 7, PC (ponto central) que foram as amostras que mais se assemelharam com as amostras comerciais estudadas. Nessas amostras realizou-se as análises físico-químicas além de capacidade antioxidante e compostos fenólicos. O conteúdo de sólidos totais na amostra 6 foi superior as demais amostras, diferindo estatisticamente das demais amostras (p> 0,05). Já para o teor de lipídios, cinzas e proteínas encontrados nas amostras 6 e PC foram maiores que as demais amostras, enquanto a amostra 7 exibiu o menor teor de lipídios e proteínas, considerando que o teor de cinzas das amostras 1, 2 e 7 foram estatisticamente iguais. O teor de carboidratos calculado por diferença foi superior nas amostras 1, 2 e 7 e com o menor valor na amostra 6. Os valores de capacidade antioxidante e compostos fenólicos não se diferenciaram estatisticamente entre si ao nível de 5% de probabilidade. Concluiu-se portanto que a etapa de maceração não influenciou no rendimento do produto final. A partir das análises físico-químicas pode-se concluir que o extrato hidrossolúvel de gergelim em determinadas amostras apresentou um melhor desempenho quanto ao valor nutricional comparado ao extrato de soja.CAPESUniversidade Federal do Espírito SantoBRMestrado em Ciência e Tecnologia de AlimentosCentro de Ciências Agrárias e EngenhariasUFESPrograma de Pós-Graduação em Ciência e Tecnologia de AlimentosSaraiva, Sérgio HenriquesTeixeira, Luciano José QuintãoJunqueira, Mateus da SilvaSartori, Marco AntônioSilva, Gisela Benatti2015-09-09T19:31:54Z2016-06-24T06:00:06Z2015-04-102015-04-10info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisTextapplication/pdfhttp://repositorio.ufes.br/handle/10/1522porinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)instname:Universidade Federal do Espírito Santo (UFES)instacron:UFES2024-06-21T16:56:14Zoai:repositorio.ufes.br:10/1522Repositório InstitucionalPUBhttp://repositorio.ufes.br/oai/requestopendoar:21082024-06-21T16:56:14Repositório Institucional da Universidade Federal do Espírito Santo (riUfes) - Universidade Federal do Espírito Santo (UFES)false
dc.title.none.fl_str_mv Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)
title Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)
spellingShingle Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)
Silva, Gisela Benatti
Cinética de maceração
Substituto lácteo
Extrato aquoso
Tempo de batimento (Alimentos)
Maceração
DCCR
Substituto lácteo
Maceration
Milk substitute
Gergelim
Ciência e Tecnologia de Alimentos
664
title_short Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)
title_full Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)
title_fullStr Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)
title_full_unstemmed Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)
title_sort Elaboração e análise de extrato hidrossolúvel de gergelim (Sesamum indicum)
author Silva, Gisela Benatti
author_facet Silva, Gisela Benatti
author_role author
dc.contributor.none.fl_str_mv Saraiva, Sérgio Henriques
Teixeira, Luciano José Quintão
Junqueira, Mateus da Silva
Sartori, Marco Antônio
dc.contributor.author.fl_str_mv Silva, Gisela Benatti
dc.subject.por.fl_str_mv Cinética de maceração
Substituto lácteo
Extrato aquoso
Tempo de batimento (Alimentos)
Maceração
DCCR
Substituto lácteo
Maceration
Milk substitute
Gergelim
Ciência e Tecnologia de Alimentos
664
topic Cinética de maceração
Substituto lácteo
Extrato aquoso
Tempo de batimento (Alimentos)
Maceração
DCCR
Substituto lácteo
Maceration
Milk substitute
Gergelim
Ciência e Tecnologia de Alimentos
664
description The aim of this study was to develop and characterize a water-soluble extract sesame-based to be used as a possible substitute for cow's milk and soy extract. A model kinetic of the absorption of water has been proposed during the maceration stage in which estimated ideal time to beat of the sesame mash and this stage influences the yield of the product. Afterwards with the aim to know the influence of the beat time (0.45 min to 14.55 min) and the extract concentration (1.925% to 23.07%) were evaluated by a central composite rotational design (CCRD) that is, a design 22 including 4 test axial conditions and the 5 repetitions at the central point totaling 13 experiments. All design of the tests was carried out analysis of viscosity, color, soluble solids and yield. The same analyzes were carried out in samples of commercial cow's milk and soy water soluble extract with the purpose of comparison. After the realization this step was possible to selection of some samples for preparation of water soluble extract of sesame and then was carried out physicochemical analysis (protein, ash, lipids, carbohydrates) and determined the antioxidant capacity by ABTS and level of compounds phenolics such samples. As regards the yield analysis there was no significant difference of the amount of extract obtained at different temperatures for maceration by Tukey test (p> 0.05). The CCRD was performed in the Statistica software and were selected for trials 1, 2, 6, 7, CP (center point) which more samples were similar with commercial samples studied. In these samples was carried out physico-chemical analysis in addition to antioxidant capacity and phenolic compounds. The total solids content in the sample 6 was higher than the other samples, differing significantly from the other samples (p> 0.05). As for the lipids, ash and proteins found in samples 6 and PC were higher than the other samples, while the sample 7 exhibited the lowest level of lipids and proteins, considering that the ash content samples 1,2 and 7 were statistically the same. The carbohydrate content calculated by difference was higher in samples 1,2 and 7 and the lowest value in the sample 6. The values of antioxidant capacity and phenolic compounds were not statistically different from each other at 5% probability. It is has therefore concluded that the soaking step did not affect the yield of the final product, this step is unnecessary. From the physico-chemical analysis it can be concluded that the sesame water soluble extract in certain samples showed a better performance in terms of nutritional value compared to the soy extract.
publishDate 2015
dc.date.none.fl_str_mv 2015-09-09T19:31:54Z
2015-04-10
2015-04-10
2016-06-24T06:00:06Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://repositorio.ufes.br/handle/10/1522
url http://repositorio.ufes.br/handle/10/1522
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv Text
application/pdf
dc.publisher.none.fl_str_mv Universidade Federal do Espírito Santo
BR
Mestrado em Ciência e Tecnologia de Alimentos
Centro de Ciências Agrárias e Engenharias
UFES
Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos
publisher.none.fl_str_mv Universidade Federal do Espírito Santo
BR
Mestrado em Ciência e Tecnologia de Alimentos
Centro de Ciências Agrárias e Engenharias
UFES
Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos
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instname_str Universidade Federal do Espírito Santo (UFES)
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institution UFES
reponame_str Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)
collection Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)
repository.name.fl_str_mv Repositório Institucional da Universidade Federal do Espírito Santo (riUfes) - Universidade Federal do Espírito Santo (UFES)
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