Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico

Detalhes bibliográficos
Autor(a) principal: Lüdtke, Fernanda Luisa
Data de Publicação: 2016
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Manancial - Repositório Digital da UFSM
Texto Completo: http://repositorio.ufsm.br/handle/1/5794
Resumo: The rice is one of the cereals most consumed in world, consumption carried out mostly in the form of grains whose processing generates by-products such a rice bran, from which is obtained the rice bran oil. Due the presence of phospholipids, gums, waxes, this oil has a darker color and higher viscosity as compared to other vegetable oils. Also contains γ-orizanol, composed absent in other oils, which have been assigned antioxidants and hypocholesterolemics effects; but to become fit for consumed, the rice bran oil needs to be refined. The refining method modifies the oil composition; the chemical refining cause significant losses or changes in composition of rice bran oil; in the physical refining loss of these components is minimized, however the rice bran oil must have a phosphorus content below to 10 mg.kg-1 before to desodorization step, for to perform the physical refining. Thus, the aim of this study was to conduct studies on the degumming in order to make it fit the physical refining; and on the clarification, so that besides fit the physical refining, this is attractive to the consumer. Clarifying activity tests were performed two clarifiers lands: Tonsil ® Supreme 180 FF Tonsil ® and Actisil FF 280 added in different proportions (1.0, 1.5 and 2.0); degumming with water (0.6 and 5%) and phosphoric acid (0.2%), citric (0.5%); and clarification tests using the land and proportions that showed the best clarifying activity. There was the physicochemical characterization of crude, degummed oil and clarified oil with 2% of the earth Tonsil ® Supreme 180 FF and profile of fatty acids, γ-oryzanol content, tocopherols and tocotrienols content. The clarifier earth Tonsil ® Supreme 180 FF was the one with the best clarifying activity in the proportion of 2%, and when added at the rate of 1.5% showed the same activity clarifying that the earth Tonsil ® Actisil 280 FF added at a ratio of 2 0%; which was verified both in the clarifier activity tests, for the clarification test. The degumming with 5% water caused a reduction of the phosphorus content to less than 10 mg.kg-1. Thus, the degumming with 5% water, followed by clarification test using citric acid (50%) in the proportion of 0.5% to 2.0% addition of the clarifier earth Tonsil ® Supreme 180 FF, to provide a suitable oil physical refining, and the physical and chemical characteristics similar to crude oil and within the requirements specified by law.
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spelling Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físicoStudy of degumming and clarification of crude oil of rice (Oryza sativa) bran aiming physical refinigArrozÓleo de arrozFareloRefino físicoγ-orizanolRiceRice bran oilPhysical refiningBranCNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOSThe rice is one of the cereals most consumed in world, consumption carried out mostly in the form of grains whose processing generates by-products such a rice bran, from which is obtained the rice bran oil. Due the presence of phospholipids, gums, waxes, this oil has a darker color and higher viscosity as compared to other vegetable oils. Also contains γ-orizanol, composed absent in other oils, which have been assigned antioxidants and hypocholesterolemics effects; but to become fit for consumed, the rice bran oil needs to be refined. The refining method modifies the oil composition; the chemical refining cause significant losses or changes in composition of rice bran oil; in the physical refining loss of these components is minimized, however the rice bran oil must have a phosphorus content below to 10 mg.kg-1 before to desodorization step, for to perform the physical refining. Thus, the aim of this study was to conduct studies on the degumming in order to make it fit the physical refining; and on the clarification, so that besides fit the physical refining, this is attractive to the consumer. Clarifying activity tests were performed two clarifiers lands: Tonsil ® Supreme 180 FF Tonsil ® and Actisil FF 280 added in different proportions (1.0, 1.5 and 2.0); degumming with water (0.6 and 5%) and phosphoric acid (0.2%), citric (0.5%); and clarification tests using the land and proportions that showed the best clarifying activity. There was the physicochemical characterization of crude, degummed oil and clarified oil with 2% of the earth Tonsil ® Supreme 180 FF and profile of fatty acids, γ-oryzanol content, tocopherols and tocotrienols content. The clarifier earth Tonsil ® Supreme 180 FF was the one with the best clarifying activity in the proportion of 2%, and when added at the rate of 1.5% showed the same activity clarifying that the earth Tonsil ® Actisil 280 FF added at a ratio of 2 0%; which was verified both in the clarifier activity tests, for the clarification test. The degumming with 5% water caused a reduction of the phosphorus content to less than 10 mg.kg-1. Thus, the degumming with 5% water, followed by clarification test using citric acid (50%) in the proportion of 0.5% to 2.0% addition of the clarifier earth Tonsil ® Supreme 180 FF, to provide a suitable oil physical refining, and the physical and chemical characteristics similar to crude oil and within the requirements specified by law.O arroz é um dos cereais mais consumidos no mundo, principalmente na forma de grãos. O beneficiamento gera subprodutos, como o farelo de arroz, de onde se obtém o óleo bruto de arroz. Devido a presença de fosfolipídios, gomas, ceras este óleo apresenta uma coloração escura e maior viscosidade, quando comparado a outros óleos vegetais. Além disso, contem 1-2% de γ-orizanol, composto ausente em outros óleos, ao qual têm-se atribuído efeitos antioxidantes e hipocolesterolêmicos. Para tornar-se apto ao consumo, o óleo bruto necessita ser refinado. O método de refino modifica a composição do óleo; no refino químico, há perdas significativas de componentes durante o processo; no refino físico a perda desses componentes é minimizada, porém é necessário que o óleo chegue na etapa de desodorização com um teor de fósforo inferior a 10 mg.kg-1, para que seja possível realizar o refino físico. Portanto,o objetivo deste trabalho foi realizar estudos sobre a degomagem, a fim de torná-lo apto ao refino físico, e sobre a clarificação, para que este seja atraente para o consumidor. Foram realizados testes de atividade clarificante utilizando duas terras clarificantes: Tonsil ® Supreme 180 FF e Tonsil ® Actisil 280 FF adicionadas em diferentes proporções (1,0; 1,5; e 2,0%); de degomagem com água (0,6 e 5%) e ácidos fósforico (0,2%) e cítrico (0,5%); e testes de clarificação utilizando as terras e proporções que apresentaram a melhor atividade clarificante. Realizou-se a caracterização físico-química do óleo bruto, óleo degomado e óleo clarificado com 2% da terra Tonsil ® Supreme 180 FF, bem como perfil de ácidos graxos, teor de γ-orizanol, teor de tocoferóis e tocotrienóis. A terra clarificante Tonsil ® Supreme 180 FF foi a que apresentou a melhor atividade clarificante na proporção de 2%, e quando adicionada na proporção de 1,5% apresentou a mesma atividade clarificante que a terra Tonsil ® Actisil 280 FF adicionada na proporção de 2,0%; o que foi verificado tanto nos testes de atividade clarificante, quanto no teste de clarificação. A degomagem com 5% de água promoveu a redução do conteúdo de fósforo para valores menores que 10 mg.kg-1. Assim, a degomagem com 5% de água, seguida da clarificação utilizando ácido cítrico (50%) na proporção de 0,5% e adição de 2,0 % da terra clarificante Tonsil ® Supreme 180 FF, forneceram um óleo apto ao refino físico e com as características físico-químicas semelhantes ao óleo bruto e dentro dos requisitos especificados pela legislação.Universidade Federal de Santa MariaBRCiência e Tecnologia dos AlimentosUFSMPrograma de Pós-Graduação em Ciência e Tecnologia dos AlimentosFries, Leadir Lucy Martinshttp://lattes.cnpq.br/5099404254254292Oliveira, Mari Silvia Rodrigues dehttp://lattes.cnpq.br/9983312363799789Milani, Liana Inês Guidolinhttp://lattes.cnpq.br/5067130014563977Lüdtke, Fernanda Luisa2016-07-082016-07-082016-02-18info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisapplication/pdfapplication/pdfLÜDTKE, Fernanda Luisa. Study of degumming and clarification of crude oil of rice (Oryza sativa) bran aiming physical refinig. 2016. 86 f. Dissertação (Mestrado em Ciência e Tecnologia dos Alimentos) - Universidade Federal de Santa Maria, Santa Maria, 2016.http://repositorio.ufsm.br/handle/1/5794porinfo:eu-repo/semantics/openAccessreponame:Manancial - Repositório Digital da UFSMinstname:Universidade Federal de Santa Maria (UFSM)instacron:UFSM2022-05-03T19:33:27Zoai:repositorio.ufsm.br:1/5794Biblioteca Digital de Teses e Dissertaçõeshttps://repositorio.ufsm.br/ONGhttps://repositorio.ufsm.br/oai/requestatendimento.sib@ufsm.br||tedebc@gmail.comopendoar:2022-05-03T19:33:27Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)false
dc.title.none.fl_str_mv Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico
Study of degumming and clarification of crude oil of rice (Oryza sativa) bran aiming physical refinig
title Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico
spellingShingle Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico
Lüdtke, Fernanda Luisa
Arroz
Óleo de arroz
Farelo
Refino físico
γ-orizanol
Rice
Rice bran oil
Physical refining
Bran
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
title_short Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico
title_full Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico
title_fullStr Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico
title_full_unstemmed Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico
title_sort Estudo da degomagem e clarificação de óleo bruto do farelo de arroz (Oryza sativa) visando refino físico
author Lüdtke, Fernanda Luisa
author_facet Lüdtke, Fernanda Luisa
author_role author
dc.contributor.none.fl_str_mv Fries, Leadir Lucy Martins
http://lattes.cnpq.br/5099404254254292
Oliveira, Mari Silvia Rodrigues de
http://lattes.cnpq.br/9983312363799789
Milani, Liana Inês Guidolin
http://lattes.cnpq.br/5067130014563977
dc.contributor.author.fl_str_mv Lüdtke, Fernanda Luisa
dc.subject.por.fl_str_mv Arroz
Óleo de arroz
Farelo
Refino físico
γ-orizanol
Rice
Rice bran oil
Physical refining
Bran
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
topic Arroz
Óleo de arroz
Farelo
Refino físico
γ-orizanol
Rice
Rice bran oil
Physical refining
Bran
CNPQ::CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
description The rice is one of the cereals most consumed in world, consumption carried out mostly in the form of grains whose processing generates by-products such a rice bran, from which is obtained the rice bran oil. Due the presence of phospholipids, gums, waxes, this oil has a darker color and higher viscosity as compared to other vegetable oils. Also contains γ-orizanol, composed absent in other oils, which have been assigned antioxidants and hypocholesterolemics effects; but to become fit for consumed, the rice bran oil needs to be refined. The refining method modifies the oil composition; the chemical refining cause significant losses or changes in composition of rice bran oil; in the physical refining loss of these components is minimized, however the rice bran oil must have a phosphorus content below to 10 mg.kg-1 before to desodorization step, for to perform the physical refining. Thus, the aim of this study was to conduct studies on the degumming in order to make it fit the physical refining; and on the clarification, so that besides fit the physical refining, this is attractive to the consumer. Clarifying activity tests were performed two clarifiers lands: Tonsil ® Supreme 180 FF Tonsil ® and Actisil FF 280 added in different proportions (1.0, 1.5 and 2.0); degumming with water (0.6 and 5%) and phosphoric acid (0.2%), citric (0.5%); and clarification tests using the land and proportions that showed the best clarifying activity. There was the physicochemical characterization of crude, degummed oil and clarified oil with 2% of the earth Tonsil ® Supreme 180 FF and profile of fatty acids, γ-oryzanol content, tocopherols and tocotrienols content. The clarifier earth Tonsil ® Supreme 180 FF was the one with the best clarifying activity in the proportion of 2%, and when added at the rate of 1.5% showed the same activity clarifying that the earth Tonsil ® Actisil 280 FF added at a ratio of 2 0%; which was verified both in the clarifier activity tests, for the clarification test. The degumming with 5% water caused a reduction of the phosphorus content to less than 10 mg.kg-1. Thus, the degumming with 5% water, followed by clarification test using citric acid (50%) in the proportion of 0.5% to 2.0% addition of the clarifier earth Tonsil ® Supreme 180 FF, to provide a suitable oil physical refining, and the physical and chemical characteristics similar to crude oil and within the requirements specified by law.
publishDate 2016
dc.date.none.fl_str_mv 2016-07-08
2016-07-08
2016-02-18
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv LÜDTKE, Fernanda Luisa. Study of degumming and clarification of crude oil of rice (Oryza sativa) bran aiming physical refinig. 2016. 86 f. Dissertação (Mestrado em Ciência e Tecnologia dos Alimentos) - Universidade Federal de Santa Maria, Santa Maria, 2016.
http://repositorio.ufsm.br/handle/1/5794
identifier_str_mv LÜDTKE, Fernanda Luisa. Study of degumming and clarification of crude oil of rice (Oryza sativa) bran aiming physical refinig. 2016. 86 f. Dissertação (Mestrado em Ciência e Tecnologia dos Alimentos) - Universidade Federal de Santa Maria, Santa Maria, 2016.
url http://repositorio.ufsm.br/handle/1/5794
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Universidade Federal de Santa Maria
BR
Ciência e Tecnologia dos Alimentos
UFSM
Programa de Pós-Graduação em Ciência e Tecnologia dos Alimentos
publisher.none.fl_str_mv Universidade Federal de Santa Maria
BR
Ciência e Tecnologia dos Alimentos
UFSM
Programa de Pós-Graduação em Ciência e Tecnologia dos Alimentos
dc.source.none.fl_str_mv reponame:Manancial - Repositório Digital da UFSM
instname:Universidade Federal de Santa Maria (UFSM)
instacron:UFSM
instname_str Universidade Federal de Santa Maria (UFSM)
instacron_str UFSM
institution UFSM
reponame_str Manancial - Repositório Digital da UFSM
collection Manancial - Repositório Digital da UFSM
repository.name.fl_str_mv Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)
repository.mail.fl_str_mv atendimento.sib@ufsm.br||tedebc@gmail.com
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