Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation

Detalhes bibliográficos
Autor(a) principal: Carvalho, Alex V. [UNESP]
Data de Publicação: 2008
Outros Autores: Scalvi, Luis V. A. [UNESP], Maciel Jr., Jorge L. B. [UNESP]
Tipo de documento: Artigo de conferência
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://hdl.handle.net/11449/225385
Resumo: Aiming identification of the components most affected by corrosion under saline environment conditions, we have carried out X-ray diffraction measurements in ceramic and bond materials, all in the powder form. The ceramic is analyzed before and after thermal annealing at 1000°C, showing the same DRX peaks, although better defined after annealing. Identification suggests the presence of Al6Si2O13 (Mullite) and SiO 2 (Quartz). Analysis of the junction (bond) material shows similar peaks, but a metallic preponderance is observed. Thermal annealing of the junction is done at much lower temperature, because it melts in the range 135°C-170°C, when a whitish smoke begins to show up along with strong sulfur odor.
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spelling Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulationCeramicCorrosionFuse cutoutsMulliteX-ray diffractionAiming identification of the components most affected by corrosion under saline environment conditions, we have carried out X-ray diffraction measurements in ceramic and bond materials, all in the powder form. The ceramic is analyzed before and after thermal annealing at 1000°C, showing the same DRX peaks, although better defined after annealing. Identification suggests the presence of Al6Si2O13 (Mullite) and SiO 2 (Quartz). Analysis of the junction (bond) material shows similar peaks, but a metallic preponderance is observed. Thermal annealing of the junction is done at much lower temperature, because it melts in the range 135°C-170°C, when a whitish smoke begins to show up along with strong sulfur odor.Depto. Física - FC - UNESP POSMAT, Bauru - SPDepto. Física - FC - UNESP, Bauru - SPDepto. Química - FC - UNESP, Bauru - SPDepto. Física - FC - UNESP POSMAT, Bauru - SPDepto. Física - FC - UNESP, Bauru - SPDepto. Química - FC - UNESP, Bauru - SPUniversidade Estadual Paulista (UNESP)Carvalho, Alex V. [UNESP]Scalvi, Luis V. A. [UNESP]Maciel Jr., Jorge L. B. [UNESP]2022-04-28T20:48:13Z2022-04-28T20:48:13Z2008-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/conferenceObject548-553Materials Science Forum, v. 591-593, p. 548-553.1662-97520255-5476http://hdl.handle.net/11449/2253852-s2.0-58149129022Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengMaterials Science Foruminfo:eu-repo/semantics/openAccess2024-04-25T17:40:55Zoai:repositorio.unesp.br:11449/225385Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-04-25T17:40:55Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation
title Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation
spellingShingle Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation
Carvalho, Alex V. [UNESP]
Ceramic
Corrosion
Fuse cutouts
Mullite
X-ray diffraction
title_short Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation
title_full Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation
title_fullStr Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation
title_full_unstemmed Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation
title_sort Powder diffraction of components subject to corrosion in fuse cutouts with ceramiclnsulation
author Carvalho, Alex V. [UNESP]
author_facet Carvalho, Alex V. [UNESP]
Scalvi, Luis V. A. [UNESP]
Maciel Jr., Jorge L. B. [UNESP]
author_role author
author2 Scalvi, Luis V. A. [UNESP]
Maciel Jr., Jorge L. B. [UNESP]
author2_role author
author
dc.contributor.none.fl_str_mv Universidade Estadual Paulista (UNESP)
dc.contributor.author.fl_str_mv Carvalho, Alex V. [UNESP]
Scalvi, Luis V. A. [UNESP]
Maciel Jr., Jorge L. B. [UNESP]
dc.subject.por.fl_str_mv Ceramic
Corrosion
Fuse cutouts
Mullite
X-ray diffraction
topic Ceramic
Corrosion
Fuse cutouts
Mullite
X-ray diffraction
description Aiming identification of the components most affected by corrosion under saline environment conditions, we have carried out X-ray diffraction measurements in ceramic and bond materials, all in the powder form. The ceramic is analyzed before and after thermal annealing at 1000°C, showing the same DRX peaks, although better defined after annealing. Identification suggests the presence of Al6Si2O13 (Mullite) and SiO 2 (Quartz). Analysis of the junction (bond) material shows similar peaks, but a metallic preponderance is observed. Thermal annealing of the junction is done at much lower temperature, because it melts in the range 135°C-170°C, when a whitish smoke begins to show up along with strong sulfur odor.
publishDate 2008
dc.date.none.fl_str_mv 2008-01-01
2022-04-28T20:48:13Z
2022-04-28T20:48:13Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/conferenceObject
format conferenceObject
status_str publishedVersion
dc.identifier.uri.fl_str_mv Materials Science Forum, v. 591-593, p. 548-553.
1662-9752
0255-5476
http://hdl.handle.net/11449/225385
2-s2.0-58149129022
identifier_str_mv Materials Science Forum, v. 591-593, p. 548-553.
1662-9752
0255-5476
2-s2.0-58149129022
url http://hdl.handle.net/11449/225385
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Materials Science Forum
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 548-553
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv
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