Rapid and selective UV spectrophotometric method for the analysis of ceftazidime

Detalhes bibliográficos
Autor(a) principal: Moreno, Andréiade Haro [UNESP]
Data de Publicação: 2009
Outros Autores: Salgado, Hérida Regina Nunes [UNESP]
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://dx.doi.org/10.1093/jaoac/92.3.820
http://hdl.handle.net/11449/231881
Resumo: A new UV spectrophotometric method was developed for quantitative evaluation of ceftazidime preparations. The UV detector was set at 255 nm. Beer's law is obeyed in the concentration range of 7.0-14.0 μg/mL. The method was found to be selective, linear, accurate, and precise in the specified ranges. Intra- and interday variability for the method were <2% relative standard deviation. Common excipients used as additives in pharmaceutical preparations do not interfere with the proposed method. This method was successfully used for quantification of ceftazidime in pure form and in pharmaceutical preparations.
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spelling Rapid and selective UV spectrophotometric method for the analysis of ceftazidimeA new UV spectrophotometric method was developed for quantitative evaluation of ceftazidime preparations. The UV detector was set at 255 nm. Beer's law is obeyed in the concentration range of 7.0-14.0 μg/mL. The method was found to be selective, linear, accurate, and precise in the specified ranges. Intra- and interday variability for the method were <2% relative standard deviation. Common excipients used as additives in pharmaceutical preparations do not interfere with the proposed method. This method was successfully used for quantification of ceftazidime in pure form and in pharmaceutical preparations.Programa de Pós-graduação em Ciências Farmacêuticas Faculdade de Ciências Farmacêuticas de Araraquara UNESP, Rodovia Araraquara-Jaú, Km 1, CEP: 14801-902, Araraquara-SPPrograma de Pós-graduação em Ciências Farmacêuticas Faculdade de Ciências Farmacêuticas de Araraquara UNESP, Rodovia Araraquara-Jaú, Km 1, CEP: 14801-902, Araraquara-SPUniversidade Estadual Paulista (UNESP)Moreno, Andréiade Haro [UNESP]Salgado, Hérida Regina Nunes [UNESP]2022-04-29T08:47:54Z2022-04-29T08:47:54Z2009-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article820-823http://dx.doi.org/10.1093/jaoac/92.3.820Journal of AOAC International, v. 92, n. 3, p. 820-823, 2009.1060-3271http://hdl.handle.net/11449/23188110.1093/jaoac/92.3.8202-s2.0-68349105029Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of AOAC Internationalinfo:eu-repo/semantics/openAccess2024-06-24T13:45:18Zoai:repositorio.unesp.br:11449/231881Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T15:05:46.240715Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Rapid and selective UV spectrophotometric method for the analysis of ceftazidime
title Rapid and selective UV spectrophotometric method for the analysis of ceftazidime
spellingShingle Rapid and selective UV spectrophotometric method for the analysis of ceftazidime
Moreno, Andréiade Haro [UNESP]
title_short Rapid and selective UV spectrophotometric method for the analysis of ceftazidime
title_full Rapid and selective UV spectrophotometric method for the analysis of ceftazidime
title_fullStr Rapid and selective UV spectrophotometric method for the analysis of ceftazidime
title_full_unstemmed Rapid and selective UV spectrophotometric method for the analysis of ceftazidime
title_sort Rapid and selective UV spectrophotometric method for the analysis of ceftazidime
author Moreno, Andréiade Haro [UNESP]
author_facet Moreno, Andréiade Haro [UNESP]
Salgado, Hérida Regina Nunes [UNESP]
author_role author
author2 Salgado, Hérida Regina Nunes [UNESP]
author2_role author
dc.contributor.none.fl_str_mv Universidade Estadual Paulista (UNESP)
dc.contributor.author.fl_str_mv Moreno, Andréiade Haro [UNESP]
Salgado, Hérida Regina Nunes [UNESP]
description A new UV spectrophotometric method was developed for quantitative evaluation of ceftazidime preparations. The UV detector was set at 255 nm. Beer's law is obeyed in the concentration range of 7.0-14.0 μg/mL. The method was found to be selective, linear, accurate, and precise in the specified ranges. Intra- and interday variability for the method were <2% relative standard deviation. Common excipients used as additives in pharmaceutical preparations do not interfere with the proposed method. This method was successfully used for quantification of ceftazidime in pure form and in pharmaceutical preparations.
publishDate 2009
dc.date.none.fl_str_mv 2009-01-01
2022-04-29T08:47:54Z
2022-04-29T08:47:54Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.1093/jaoac/92.3.820
Journal of AOAC International, v. 92, n. 3, p. 820-823, 2009.
1060-3271
http://hdl.handle.net/11449/231881
10.1093/jaoac/92.3.820
2-s2.0-68349105029
url http://dx.doi.org/10.1093/jaoac/92.3.820
http://hdl.handle.net/11449/231881
identifier_str_mv Journal of AOAC International, v. 92, n. 3, p. 820-823, 2009.
1060-3271
10.1093/jaoac/92.3.820
2-s2.0-68349105029
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Journal of AOAC International
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 820-823
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv
_version_ 1808128459335008256

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