Análise isotópica do carbono em néctares de caju
Autor(a) principal: | |
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Data de Publicação: | 2011 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | por |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://serv-bib.fcfar.unesp.br/seer/index.php/alimentos/article/viewArticle/1501 http://hdl.handle.net/11449/137160 |
Resumo: | The objective of this work were to determine the isotopic composition of commercial cashew nectar and by mixture models, to quantify the carbon from plants holding the C3 photosynthetic cycle so as to identify beverages that don’t abide with the rules from the Brazilian legislation. The nectars were produced in a laboratory according to Brazilian law. Adulterated nectar was also produced with a quantity of cashew pulp below the allowed limit. In these beverages were calculated the theoretical percentages of C3 source, by using the mass balance of soluble solids. For the isotope analysis the isotope values of cane sugar, cashew nectars and its fractions purifi ed sugar and insoluble solids were measured. With these values were calculated the practical percentage of C3 (real) source through the isotopic analysis in a mass spectrometer. The practical results were compared with the theoretical ones to defi ne the best way to quantify the C3 source. To identify the adulterated commercial nectars was measured to the legality limit according to the Brazilian legislation. Four trademarks of cashew nectars were analyzed and all of them classifi ed legal. The legal limit enabled to identify the beverages in accordance with Brazilian law. The methodology was effi cient for measuring the carbon from C3 source in commercial cashew nectar. |
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Análise isotópica do carbono em néctares de cajuCarbon isotope analysis in cashew nectarsBeveragesAdulterationQualityCarbon-13IRMSAnacardium occidentaleBebidasAdulteraçãoQualidadeCarbono-13IRMSAnacardium occidentaleThe objective of this work were to determine the isotopic composition of commercial cashew nectar and by mixture models, to quantify the carbon from plants holding the C3 photosynthetic cycle so as to identify beverages that don’t abide with the rules from the Brazilian legislation. The nectars were produced in a laboratory according to Brazilian law. Adulterated nectar was also produced with a quantity of cashew pulp below the allowed limit. In these beverages were calculated the theoretical percentages of C3 source, by using the mass balance of soluble solids. For the isotope analysis the isotope values of cane sugar, cashew nectars and its fractions purifi ed sugar and insoluble solids were measured. With these values were calculated the practical percentage of C3 (real) source through the isotopic analysis in a mass spectrometer. The practical results were compared with the theoretical ones to defi ne the best way to quantify the C3 source. To identify the adulterated commercial nectars was measured to the legality limit according to the Brazilian legislation. Four trademarks of cashew nectars were analyzed and all of them classifi ed legal. The legal limit enabled to identify the beverages in accordance with Brazilian law. The methodology was effi cient for measuring the carbon from C3 source in commercial cashew nectar.Os objetivos deste trabalho foram determinar a composição isotópica de néctares comerciais de caju e, por meio de modelos de mistura, quantifi car aporcentagem de carbono proveniente de plantas do ciclo fotossintético C3 , a fi m de identifi car as bebidas que não estavam em conformidade com as normas do Ministério da Agricultura, Pecuária e Abastecimento (MAPA). Para isso, foram produzidos néctares em laboratório conforme a legislação brasileira. Também foi produzida bebida adulterada com quantidade de polpa de caju abaixo do limite estabelecido. Nesses néctares, as porcentagens teóricas de fonte C3 foram calculadas por meio do balanço de massa de sólidos solú- veis. Para a análise isotópica foram mensurados os valores isotópicos dos açúcares de cana, dos néctares de caju e de suas frações açúcares purifi cados e sólidos insolúveis. Com esses valores, foram calculadas as porcentagens práticas de fonte C3 (reais) por meio da análise isotópica, em espectrô- metro de massa. Os resultados práticos foram comparados com os teóricos para defi nir a melhor forma de quantifi - cação de fonte C3 . Para identifi car os néctares comerciais adulterados, foi desenvolvido um limite de legalidade conforme a legislação brasileira. Quatro marcas de néctares de caju foram analisadas e todas classifi cadas como legais. O limite de legalidade possibilitou identifi car as bebidas em conformidade com a lei. A metodologia foi efi ciente para quantifi car o carbono de origem C3 em néctares comerciais de caju.Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Universidade Estadual Paulista Júlio de Mesquita Filho, Departamento de Gestão e Tecnologia Agroindustrial, Botucatu, Fazenda Experimental Lageado, CEP 18603970, SP, BrasilUniversidade Estadual Paulista Júlio de Mesquita Filho, Departamento de Bioestatística, Instituto de Biociências, SP, BrasilUniversidade Estadual Paulista Júlio de Mesquita Filho, Departamento de Gestão e Tecnologia Agroindustrial, Botucatu, Fazenda Experimental Lageado, CEP 18603970, SP, BrasilUniversidade Estadual Paulista Júlio de Mesquita Filho, Departamento de Bioestatística, Instituto de Biociências, SP, BrasilCNPq: 505031/2008-6FAPESP: 2009/51661-1Universidade Estadual Paulista (Unesp)Figueira, Ricardo [UNESP]Nogueira, Andressa Milene Parente [UNESP]Ducatti, Carlos [UNESP]Mischan, Martha Maria [UNESP]Venturini Filho, Waldemar Gastoni [UNESP]2016-04-01T18:44:27Z2016-04-01T18:44:27Z2011info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article561-569application/pdfhttp://serv-bib.fcfar.unesp.br/seer/index.php/alimentos/article/viewArticle/1501Alimentos e Nutrição, v. 22, n. 4, p. 561-569, 2011.0103-4235http://hdl.handle.net/11449/137160ISSN0103-4235-2011-22-04-561-569.pdf10302517439432175493452207047677Currículo Lattesreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPporAlimentos e Nutriçãoinfo:eu-repo/semantics/openAccess2024-01-25T06:34:26Zoai:repositorio.unesp.br:11449/137160Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T23:58:04.749400Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Análise isotópica do carbono em néctares de caju Carbon isotope analysis in cashew nectars |
title |
Análise isotópica do carbono em néctares de caju |
spellingShingle |
Análise isotópica do carbono em néctares de caju Figueira, Ricardo [UNESP] Beverages Adulteration Quality Carbon-13 IRMS Anacardium occidentale Bebidas Adulteração Qualidade Carbono-13 IRMS Anacardium occidentale |
title_short |
Análise isotópica do carbono em néctares de caju |
title_full |
Análise isotópica do carbono em néctares de caju |
title_fullStr |
Análise isotópica do carbono em néctares de caju |
title_full_unstemmed |
Análise isotópica do carbono em néctares de caju |
title_sort |
Análise isotópica do carbono em néctares de caju |
author |
Figueira, Ricardo [UNESP] |
author_facet |
Figueira, Ricardo [UNESP] Nogueira, Andressa Milene Parente [UNESP] Ducatti, Carlos [UNESP] Mischan, Martha Maria [UNESP] Venturini Filho, Waldemar Gastoni [UNESP] |
author_role |
author |
author2 |
Nogueira, Andressa Milene Parente [UNESP] Ducatti, Carlos [UNESP] Mischan, Martha Maria [UNESP] Venturini Filho, Waldemar Gastoni [UNESP] |
author2_role |
author author author author |
dc.contributor.none.fl_str_mv |
Universidade Estadual Paulista (Unesp) |
dc.contributor.author.fl_str_mv |
Figueira, Ricardo [UNESP] Nogueira, Andressa Milene Parente [UNESP] Ducatti, Carlos [UNESP] Mischan, Martha Maria [UNESP] Venturini Filho, Waldemar Gastoni [UNESP] |
dc.subject.por.fl_str_mv |
Beverages Adulteration Quality Carbon-13 IRMS Anacardium occidentale Bebidas Adulteração Qualidade Carbono-13 IRMS Anacardium occidentale |
topic |
Beverages Adulteration Quality Carbon-13 IRMS Anacardium occidentale Bebidas Adulteração Qualidade Carbono-13 IRMS Anacardium occidentale |
description |
The objective of this work were to determine the isotopic composition of commercial cashew nectar and by mixture models, to quantify the carbon from plants holding the C3 photosynthetic cycle so as to identify beverages that don’t abide with the rules from the Brazilian legislation. The nectars were produced in a laboratory according to Brazilian law. Adulterated nectar was also produced with a quantity of cashew pulp below the allowed limit. In these beverages were calculated the theoretical percentages of C3 source, by using the mass balance of soluble solids. For the isotope analysis the isotope values of cane sugar, cashew nectars and its fractions purifi ed sugar and insoluble solids were measured. With these values were calculated the practical percentage of C3 (real) source through the isotopic analysis in a mass spectrometer. The practical results were compared with the theoretical ones to defi ne the best way to quantify the C3 source. To identify the adulterated commercial nectars was measured to the legality limit according to the Brazilian legislation. Four trademarks of cashew nectars were analyzed and all of them classifi ed legal. The legal limit enabled to identify the beverages in accordance with Brazilian law. The methodology was effi cient for measuring the carbon from C3 source in commercial cashew nectar. |
publishDate |
2011 |
dc.date.none.fl_str_mv |
2011 2016-04-01T18:44:27Z 2016-04-01T18:44:27Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://serv-bib.fcfar.unesp.br/seer/index.php/alimentos/article/viewArticle/1501 Alimentos e Nutrição, v. 22, n. 4, p. 561-569, 2011. 0103-4235 http://hdl.handle.net/11449/137160 ISSN0103-4235-2011-22-04-561-569.pdf 1030251743943217 5493452207047677 |
url |
http://serv-bib.fcfar.unesp.br/seer/index.php/alimentos/article/viewArticle/1501 http://hdl.handle.net/11449/137160 |
identifier_str_mv |
Alimentos e Nutrição, v. 22, n. 4, p. 561-569, 2011. 0103-4235 ISSN0103-4235-2011-22-04-561-569.pdf 1030251743943217 5493452207047677 |
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por |
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por |
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Alimentos e Nutrição |
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info:eu-repo/semantics/openAccess |
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openAccess |
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561-569 application/pdf |
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Currículo Lattes reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
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Universidade Estadual Paulista (UNESP) |
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UNESP |
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Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
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1808129567904235520 |