Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
Autor(a) principal: | |
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Data de Publicação: | 2019 |
Tipo de documento: | Dissertação |
Idioma: | por |
Título da fonte: | Biblioteca Digital de Teses e Dissertações da UFRPE |
Texto Completo: | http://www.tede2.ufrpe.br:8080/tede2/handle/tede2/8208 |
Resumo: | The agroindustrial residue of seriguela is rich in phenolic compounds, substances with antioxidant properties, however, in view of the sensitivity of these substances, it is necessary to employ technology with a view to promoting its stability and bioavailability, allowing its use in food and / or packaging. Thus, in order to evaluate the viability of the microencapsulation by atomization of the seriguela agroindustrial residue extract, the process conditions related to the entry temperature and maltodextrin concentration (10 DE) were investigated. The hydroethanolic extract was obtained from the dry residue and, to define the best microencapsulation conditions, the factorial design 22 was applied with three central points, with the concentration of maltodextrin (10%, 15%, 20%) as the independent variables. (100°C, 120°C, 140°C), the drying air flow rate of 28m³/h and the feed rate of 0.60mL/min were kept constant. Moisture content, water activity, hygroscopicity, apparent density, solubility, total phenolic content, antioxidant activity and encapsulation efficiency were the dependent variables. The phenolic profile of the extract, before and after the microencapsulation, was determined by high performance chromatography. The temperature and the concentration of maltodextrin exerted significant influence (p <0.05) on moisture, apparent density and total phenolic content, without influencing the other parameters studied. Microencapsulated with lower moisture content was observed when using maltodextrin in the concentration between 15 to 20%. The solubility was above 80%, regardless of the inlet temperature and maltodextrin concentration. Total phenolic content, in particular, was significantly influenced by the concentration of maltodextrin and little influence of the inlet temperature. Galician, p-coumaric and syringogenic acids were the major compounds present in the hydroethanolic extract, and there was a change in the qualitative and quantitative profile of the microencapsulated phenolics, thus, the 10 DE maltodextrin used as an encapsulating agent was not efficient to promote the stability of the compounds phenolics, in this way, it is evident the need of studies that aim at the optimization of the process. |
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MELO, Enayde de AlmeidaSANTOS, Andrelina Maria PinheiroVASCONCELOS, Margarida Angélica da SilvaANDRADE, Samara Alvachian CardosoMACIEL, Maria Inês Sucupirahttp://lattes.cnpq.br/5576747518833531ALMEIDA, Hákylla Rayanne Mota de2019-09-19T13:57:21Z2019-01-30ALMEIDA, Hákylla Rayanne Mota de. Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização. 2019. 84 f. Dissertação (Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos) - Universidade Federal Rural de Pernambuco, Recife.http://www.tede2.ufrpe.br:8080/tede2/handle/tede2/8208The agroindustrial residue of seriguela is rich in phenolic compounds, substances with antioxidant properties, however, in view of the sensitivity of these substances, it is necessary to employ technology with a view to promoting its stability and bioavailability, allowing its use in food and / or packaging. Thus, in order to evaluate the viability of the microencapsulation by atomization of the seriguela agroindustrial residue extract, the process conditions related to the entry temperature and maltodextrin concentration (10 DE) were investigated. The hydroethanolic extract was obtained from the dry residue and, to define the best microencapsulation conditions, the factorial design 22 was applied with three central points, with the concentration of maltodextrin (10%, 15%, 20%) as the independent variables. (100°C, 120°C, 140°C), the drying air flow rate of 28m³/h and the feed rate of 0.60mL/min were kept constant. Moisture content, water activity, hygroscopicity, apparent density, solubility, total phenolic content, antioxidant activity and encapsulation efficiency were the dependent variables. The phenolic profile of the extract, before and after the microencapsulation, was determined by high performance chromatography. The temperature and the concentration of maltodextrin exerted significant influence (p <0.05) on moisture, apparent density and total phenolic content, without influencing the other parameters studied. Microencapsulated with lower moisture content was observed when using maltodextrin in the concentration between 15 to 20%. The solubility was above 80%, regardless of the inlet temperature and maltodextrin concentration. Total phenolic content, in particular, was significantly influenced by the concentration of maltodextrin and little influence of the inlet temperature. Galician, p-coumaric and syringogenic acids were the major compounds present in the hydroethanolic extract, and there was a change in the qualitative and quantitative profile of the microencapsulated phenolics, thus, the 10 DE maltodextrin used as an encapsulating agent was not efficient to promote the stability of the compounds phenolics, in this way, it is evident the need of studies that aim at the optimization of the process.O resíduo agroindustrial de seriguela é rico em compostos fenólicos, substâncias com propriedade antioxidante, entretanto, frente à sensibilidade destas substâncias se faz necessário empregar tecnologia com vistas a promover sua estabilidade e biodisponibilidade, possibilitando sua utilização em alimentos e/ou em embalagens. Assim, com o objetivo de avaliar a viabilidade da microencapsulação por atomização do extrato do resíduo agroindustrial de seriguela, as condições de processo referentes à temperatura de entrada e concentração de maltodextrina (10 DE) foram investigadas. O extrato hidroetanólico foi obtido a partir do resíduo seco, e para definir as melhores condições de microencapsulação foi aplicado o planejamento fatorial 22, com três pontos centrais, tendo como variáveis independentes a concentração de maltodextrina (10%; 15%; 20%) e a temperatura de entrada (100°C; 120°C; 140°C), mantendo-se constante a vazão do ar de secagem de 28m³/h e a taxa de alimentação de 0,60mL/min. O teor de umidade, atividade de água, higroscopicidade, densidade aparente, solubilidade, teor de fenólicos totais, atividade antioxidante e eficiência da encapsulação foram as variáveis dependentes. O perfil de fenólicos do extrato, antes e após a microencapsulação, foi determinado por cromatografia de alta performance. A temperatura e a concentração de maltodextrina exerceram influência significativa (p<0,05) sobre a umidade, densidade aparente e teor de fenólicos totais, não exercendo influência sobre os demais parâmetros estudados. Microencapsulados com menor teor de umidade foi visto ao empregar maltodextrina na concentração entre 15 a 20%. A solubilidade se mostrou acima de 80%, independente da temperatura de entrada e concentração de maltodextrina. O teor de fenólicos totais, particularmente, sofreu influência significativa da concentração de maltodextrina e pouca influência da temperatura de entrada. O ácido gálico, p-cumárico e siríngico, foram os compostos majoritários presentes no extrato hidroetanólico, havendo alteração no perfil qualitativo e quantitativo dos fenólicos do microencapsulado. Assim, a maltodextrina 10 DE usada como agente encapsulante não foi eficiente para promover a estabilidade dos compostos fenólicos, evidenciando-se a necessidade de estudos que objetivem a otimização do processo.Submitted by Mario BC (mario@bc.ufrpe.br) on 2019-09-19T13:57:21Z No. of bitstreams: 1 Hakylla Rayanne Mota de Almeida.pdf: 1495413 bytes, checksum: 7c7ee18ae080862815d7b28ff7289c5d (MD5)Made available in DSpace on 2019-09-19T13:57:21Z (GMT). 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dc.title.por.fl_str_mv |
Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização |
title |
Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização |
spellingShingle |
Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização ALMEIDA, Hákylla Rayanne Mota de Resíduo agroindustrial Resíduo de seriguela Microencapsulação Atomização CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS |
title_short |
Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização |
title_full |
Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização |
title_fullStr |
Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização |
title_full_unstemmed |
Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização |
title_sort |
Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização |
author |
ALMEIDA, Hákylla Rayanne Mota de |
author_facet |
ALMEIDA, Hákylla Rayanne Mota de |
author_role |
author |
dc.contributor.advisor1.fl_str_mv |
MELO, Enayde de Almeida |
dc.contributor.advisor-co1.fl_str_mv |
SANTOS, Andrelina Maria Pinheiro |
dc.contributor.referee1.fl_str_mv |
VASCONCELOS, Margarida Angélica da Silva |
dc.contributor.referee2.fl_str_mv |
ANDRADE, Samara Alvachian Cardoso |
dc.contributor.referee3.fl_str_mv |
MACIEL, Maria Inês Sucupira |
dc.contributor.authorLattes.fl_str_mv |
http://lattes.cnpq.br/5576747518833531 |
dc.contributor.author.fl_str_mv |
ALMEIDA, Hákylla Rayanne Mota de |
contributor_str_mv |
MELO, Enayde de Almeida SANTOS, Andrelina Maria Pinheiro VASCONCELOS, Margarida Angélica da Silva ANDRADE, Samara Alvachian Cardoso MACIEL, Maria Inês Sucupira |
dc.subject.por.fl_str_mv |
Resíduo agroindustrial Resíduo de seriguela Microencapsulação Atomização |
topic |
Resíduo agroindustrial Resíduo de seriguela Microencapsulação Atomização CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS |
dc.subject.cnpq.fl_str_mv |
CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS |
description |
The agroindustrial residue of seriguela is rich in phenolic compounds, substances with antioxidant properties, however, in view of the sensitivity of these substances, it is necessary to employ technology with a view to promoting its stability and bioavailability, allowing its use in food and / or packaging. Thus, in order to evaluate the viability of the microencapsulation by atomization of the seriguela agroindustrial residue extract, the process conditions related to the entry temperature and maltodextrin concentration (10 DE) were investigated. The hydroethanolic extract was obtained from the dry residue and, to define the best microencapsulation conditions, the factorial design 22 was applied with three central points, with the concentration of maltodextrin (10%, 15%, 20%) as the independent variables. (100°C, 120°C, 140°C), the drying air flow rate of 28m³/h and the feed rate of 0.60mL/min were kept constant. Moisture content, water activity, hygroscopicity, apparent density, solubility, total phenolic content, antioxidant activity and encapsulation efficiency were the dependent variables. The phenolic profile of the extract, before and after the microencapsulation, was determined by high performance chromatography. The temperature and the concentration of maltodextrin exerted significant influence (p <0.05) on moisture, apparent density and total phenolic content, without influencing the other parameters studied. Microencapsulated with lower moisture content was observed when using maltodextrin in the concentration between 15 to 20%. The solubility was above 80%, regardless of the inlet temperature and maltodextrin concentration. Total phenolic content, in particular, was significantly influenced by the concentration of maltodextrin and little influence of the inlet temperature. Galician, p-coumaric and syringogenic acids were the major compounds present in the hydroethanolic extract, and there was a change in the qualitative and quantitative profile of the microencapsulated phenolics, thus, the 10 DE maltodextrin used as an encapsulating agent was not efficient to promote the stability of the compounds phenolics, in this way, it is evident the need of studies that aim at the optimization of the process. |
publishDate |
2019 |
dc.date.accessioned.fl_str_mv |
2019-09-19T13:57:21Z |
dc.date.issued.fl_str_mv |
2019-01-30 |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/masterThesis |
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masterThesis |
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publishedVersion |
dc.identifier.citation.fl_str_mv |
ALMEIDA, Hákylla Rayanne Mota de. Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização. 2019. 84 f. Dissertação (Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos) - Universidade Federal Rural de Pernambuco, Recife. |
dc.identifier.uri.fl_str_mv |
http://www.tede2.ufrpe.br:8080/tede2/handle/tede2/8208 |
identifier_str_mv |
ALMEIDA, Hákylla Rayanne Mota de. Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização. 2019. 84 f. Dissertação (Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos) - Universidade Federal Rural de Pernambuco, Recife. |
url |
http://www.tede2.ufrpe.br:8080/tede2/handle/tede2/8208 |
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openAccess |
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Universidade Federal Rural de Pernambuco |
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UFRPE |
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Brasil |
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Universidade Federal Rural de Pernambuco |
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