Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização

Detalhes bibliográficos
Autor(a) principal: ALMEIDA, Hákylla Rayanne Mota de
Data de Publicação: 2019
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Biblioteca Digital de Teses e Dissertações da UFRPE
Texto Completo: http://www.tede2.ufrpe.br:8080/tede2/handle/tede2/8208
Resumo: The agroindustrial residue of seriguela is rich in phenolic compounds, substances with antioxidant properties, however, in view of the sensitivity of these substances, it is necessary to employ technology with a view to promoting its stability and bioavailability, allowing its use in food and / or packaging. Thus, in order to evaluate the viability of the microencapsulation by atomization of the seriguela agroindustrial residue extract, the process conditions related to the entry temperature and maltodextrin concentration (10 DE) were investigated. The hydroethanolic extract was obtained from the dry residue and, to define the best microencapsulation conditions, the factorial design 22 was applied with three central points, with the concentration of maltodextrin (10%, 15%, 20%) as the independent variables. (100°C, 120°C, 140°C), the drying air flow rate of 28m³/h and the feed rate of 0.60mL/min were kept constant. Moisture content, water activity, hygroscopicity, apparent density, solubility, total phenolic content, antioxidant activity and encapsulation efficiency were the dependent variables. The phenolic profile of the extract, before and after the microencapsulation, was determined by high performance chromatography. The temperature and the concentration of maltodextrin exerted significant influence (p <0.05) on moisture, apparent density and total phenolic content, without influencing the other parameters studied. Microencapsulated with lower moisture content was observed when using maltodextrin in the concentration between 15 to 20%. The solubility was above 80%, regardless of the inlet temperature and maltodextrin concentration. Total phenolic content, in particular, was significantly influenced by the concentration of maltodextrin and little influence of the inlet temperature. Galician, p-coumaric and syringogenic acids were the major compounds present in the hydroethanolic extract, and there was a change in the qualitative and quantitative profile of the microencapsulated phenolics, thus, the 10 DE maltodextrin used as an encapsulating agent was not efficient to promote the stability of the compounds phenolics, in this way, it is evident the need of studies that aim at the optimization of the process.
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spelling MELO, Enayde de AlmeidaSANTOS, Andrelina Maria PinheiroVASCONCELOS, Margarida Angélica da SilvaANDRADE, Samara Alvachian CardosoMACIEL, Maria Inês Sucupirahttp://lattes.cnpq.br/5576747518833531ALMEIDA, Hákylla Rayanne Mota de2019-09-19T13:57:21Z2019-01-30ALMEIDA, Hákylla Rayanne Mota de. Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização. 2019. 84 f. Dissertação (Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos) - Universidade Federal Rural de Pernambuco, Recife.http://www.tede2.ufrpe.br:8080/tede2/handle/tede2/8208The agroindustrial residue of seriguela is rich in phenolic compounds, substances with antioxidant properties, however, in view of the sensitivity of these substances, it is necessary to employ technology with a view to promoting its stability and bioavailability, allowing its use in food and / or packaging. Thus, in order to evaluate the viability of the microencapsulation by atomization of the seriguela agroindustrial residue extract, the process conditions related to the entry temperature and maltodextrin concentration (10 DE) were investigated. The hydroethanolic extract was obtained from the dry residue and, to define the best microencapsulation conditions, the factorial design 22 was applied with three central points, with the concentration of maltodextrin (10%, 15%, 20%) as the independent variables. (100°C, 120°C, 140°C), the drying air flow rate of 28m³/h and the feed rate of 0.60mL/min were kept constant. Moisture content, water activity, hygroscopicity, apparent density, solubility, total phenolic content, antioxidant activity and encapsulation efficiency were the dependent variables. The phenolic profile of the extract, before and after the microencapsulation, was determined by high performance chromatography. The temperature and the concentration of maltodextrin exerted significant influence (p <0.05) on moisture, apparent density and total phenolic content, without influencing the other parameters studied. Microencapsulated with lower moisture content was observed when using maltodextrin in the concentration between 15 to 20%. The solubility was above 80%, regardless of the inlet temperature and maltodextrin concentration. Total phenolic content, in particular, was significantly influenced by the concentration of maltodextrin and little influence of the inlet temperature. Galician, p-coumaric and syringogenic acids were the major compounds present in the hydroethanolic extract, and there was a change in the qualitative and quantitative profile of the microencapsulated phenolics, thus, the 10 DE maltodextrin used as an encapsulating agent was not efficient to promote the stability of the compounds phenolics, in this way, it is evident the need of studies that aim at the optimization of the process.O resíduo agroindustrial de seriguela é rico em compostos fenólicos, substâncias com propriedade antioxidante, entretanto, frente à sensibilidade destas substâncias se faz necessário empregar tecnologia com vistas a promover sua estabilidade e biodisponibilidade, possibilitando sua utilização em alimentos e/ou em embalagens. Assim, com o objetivo de avaliar a viabilidade da microencapsulação por atomização do extrato do resíduo agroindustrial de seriguela, as condições de processo referentes à temperatura de entrada e concentração de maltodextrina (10 DE) foram investigadas. O extrato hidroetanólico foi obtido a partir do resíduo seco, e para definir as melhores condições de microencapsulação foi aplicado o planejamento fatorial 22, com três pontos centrais, tendo como variáveis independentes a concentração de maltodextrina (10%; 15%; 20%) e a temperatura de entrada (100°C; 120°C; 140°C), mantendo-se constante a vazão do ar de secagem de 28m³/h e a taxa de alimentação de 0,60mL/min. O teor de umidade, atividade de água, higroscopicidade, densidade aparente, solubilidade, teor de fenólicos totais, atividade antioxidante e eficiência da encapsulação foram as variáveis dependentes. O perfil de fenólicos do extrato, antes e após a microencapsulação, foi determinado por cromatografia de alta performance. A temperatura e a concentração de maltodextrina exerceram influência significativa (p<0,05) sobre a umidade, densidade aparente e teor de fenólicos totais, não exercendo influência sobre os demais parâmetros estudados. Microencapsulados com menor teor de umidade foi visto ao empregar maltodextrina na concentração entre 15 a 20%. A solubilidade se mostrou acima de 80%, independente da temperatura de entrada e concentração de maltodextrina. O teor de fenólicos totais, particularmente, sofreu influência significativa da concentração de maltodextrina e pouca influência da temperatura de entrada. O ácido gálico, p-cumárico e siríngico, foram os compostos majoritários presentes no extrato hidroetanólico, havendo alteração no perfil qualitativo e quantitativo dos fenólicos do microencapsulado. Assim, a maltodextrina 10 DE usada como agente encapsulante não foi eficiente para promover a estabilidade dos compostos fenólicos, evidenciando-se a necessidade de estudos que objetivem a otimização do processo.Submitted by Mario BC (mario@bc.ufrpe.br) on 2019-09-19T13:57:21Z No. of bitstreams: 1 Hakylla Rayanne Mota de Almeida.pdf: 1495413 bytes, checksum: 7c7ee18ae080862815d7b28ff7289c5d (MD5)Made available in DSpace on 2019-09-19T13:57:21Z (GMT). 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dc.title.por.fl_str_mv Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
title Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
spellingShingle Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
ALMEIDA, Hákylla Rayanne Mota de
Resíduo agroindustrial
Resíduo de seriguela
Microencapsulação
Atomização
CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
title_short Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
title_full Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
title_fullStr Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
title_full_unstemmed Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
title_sort Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização
author ALMEIDA, Hákylla Rayanne Mota de
author_facet ALMEIDA, Hákylla Rayanne Mota de
author_role author
dc.contributor.advisor1.fl_str_mv MELO, Enayde de Almeida
dc.contributor.advisor-co1.fl_str_mv SANTOS, Andrelina Maria Pinheiro
dc.contributor.referee1.fl_str_mv VASCONCELOS, Margarida Angélica da Silva
dc.contributor.referee2.fl_str_mv ANDRADE, Samara Alvachian Cardoso
dc.contributor.referee3.fl_str_mv MACIEL, Maria Inês Sucupira
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/5576747518833531
dc.contributor.author.fl_str_mv ALMEIDA, Hákylla Rayanne Mota de
contributor_str_mv MELO, Enayde de Almeida
SANTOS, Andrelina Maria Pinheiro
VASCONCELOS, Margarida Angélica da Silva
ANDRADE, Samara Alvachian Cardoso
MACIEL, Maria Inês Sucupira
dc.subject.por.fl_str_mv Resíduo agroindustrial
Resíduo de seriguela
Microencapsulação
Atomização
topic Resíduo agroindustrial
Resíduo de seriguela
Microencapsulação
Atomização
CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
dc.subject.cnpq.fl_str_mv CIENCIAS AGRARIAS::CIENCIA E TECNOLOGIA DE ALIMENTOS
description The agroindustrial residue of seriguela is rich in phenolic compounds, substances with antioxidant properties, however, in view of the sensitivity of these substances, it is necessary to employ technology with a view to promoting its stability and bioavailability, allowing its use in food and / or packaging. Thus, in order to evaluate the viability of the microencapsulation by atomization of the seriguela agroindustrial residue extract, the process conditions related to the entry temperature and maltodextrin concentration (10 DE) were investigated. The hydroethanolic extract was obtained from the dry residue and, to define the best microencapsulation conditions, the factorial design 22 was applied with three central points, with the concentration of maltodextrin (10%, 15%, 20%) as the independent variables. (100°C, 120°C, 140°C), the drying air flow rate of 28m³/h and the feed rate of 0.60mL/min were kept constant. Moisture content, water activity, hygroscopicity, apparent density, solubility, total phenolic content, antioxidant activity and encapsulation efficiency were the dependent variables. The phenolic profile of the extract, before and after the microencapsulation, was determined by high performance chromatography. The temperature and the concentration of maltodextrin exerted significant influence (p <0.05) on moisture, apparent density and total phenolic content, without influencing the other parameters studied. Microencapsulated with lower moisture content was observed when using maltodextrin in the concentration between 15 to 20%. The solubility was above 80%, regardless of the inlet temperature and maltodextrin concentration. Total phenolic content, in particular, was significantly influenced by the concentration of maltodextrin and little influence of the inlet temperature. Galician, p-coumaric and syringogenic acids were the major compounds present in the hydroethanolic extract, and there was a change in the qualitative and quantitative profile of the microencapsulated phenolics, thus, the 10 DE maltodextrin used as an encapsulating agent was not efficient to promote the stability of the compounds phenolics, in this way, it is evident the need of studies that aim at the optimization of the process.
publishDate 2019
dc.date.accessioned.fl_str_mv 2019-09-19T13:57:21Z
dc.date.issued.fl_str_mv 2019-01-30
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
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dc.identifier.citation.fl_str_mv ALMEIDA, Hákylla Rayanne Mota de. Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização. 2019. 84 f. Dissertação (Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos) - Universidade Federal Rural de Pernambuco, Recife.
dc.identifier.uri.fl_str_mv http://www.tede2.ufrpe.br:8080/tede2/handle/tede2/8208
identifier_str_mv ALMEIDA, Hákylla Rayanne Mota de. Microencapsulação por atomização do extrato do resíduo de seriguela e sua caracterização. 2019. 84 f. Dissertação (Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos) - Universidade Federal Rural de Pernambuco, Recife.
url http://www.tede2.ufrpe.br:8080/tede2/handle/tede2/8208
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dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Ciência e Tecnologia de Alimentos
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dc.publisher.country.fl_str_mv Brasil
dc.publisher.department.fl_str_mv Departamento de Ciências Domésticas
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