Spot-test identification and rapid quantitative sequential analys is of dipyrone

Detalhes bibliográficos
Autor(a) principal: Tubino, M.
Data de Publicação: 2010
Outros Autores: Biondo, A. C., Vila, M. M.D.C., Pezza, L. [UNESP], Pezza, H. R. [UNESP]
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://dx.doi.org/10.26850/1678-4618EQJ.V35.1.2010.P41-46
http://hdl.handle.net/11449/222640
Resumo: A qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drug and in pharmaceutical preparations is proposed. The formation of a reddish-violet color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian Pharmacopoeia, using the Student fst and the F tests. Considering the concentration in a 100 μL aliquot, the qualitative visual limit of detection is about (Formula Presented) instrumental (Formula Presented)
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spelling Spot-test identification and rapid quantitative sequential analys is of dipyroneAnalysisDipyroneQualitativeQuantitativeSpot-testA qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drug and in pharmaceutical preparations is proposed. The formation of a reddish-violet color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian Pharmacopoeia, using the Student fst and the F tests. Considering the concentration in a 100 μL aliquot, the qualitative visual limit of detection is about (Formula Presented) instrumental (Formula Presented)State University of Campinas - UNICAMP Institute of Chemistry, P.O. Box 6154, SPSorocaba University UNISO, SPSão Paulo State University- UNESP Chemistry Institute of Araraquara, SPSão Paulo State University- UNESP Chemistry Institute of Araraquara, SPUniversidade Estadual de Campinas (UNICAMP)UNISOUniversidade Estadual Paulista (UNESP)Tubino, M.Biondo, A. C.Vila, M. M.D.C.Pezza, L. [UNESP]Pezza, H. R. [UNESP]2022-04-28T19:45:55Z2022-04-28T19:45:55Z2010-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article41-46http://dx.doi.org/10.26850/1678-4618EQJ.V35.1.2010.P41-46Ecletica Quimica, v. 35, n. 1, p. 41-46, 2010.1678-46180100-4670http://hdl.handle.net/11449/22264010.26850/1678-4618EQJ.V35.1.2010.P41-462-s2.0-85117034255Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengEcletica Quimicainfo:eu-repo/semantics/openAccess2022-04-28T19:45:55Zoai:repositorio.unesp.br:11449/222640Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-05-23T11:15:41.032232Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Spot-test identification and rapid quantitative sequential analys is of dipyrone
title Spot-test identification and rapid quantitative sequential analys is of dipyrone
spellingShingle Spot-test identification and rapid quantitative sequential analys is of dipyrone
Tubino, M.
Analysis
Dipyrone
Qualitative
Quantitative
Spot-test
title_short Spot-test identification and rapid quantitative sequential analys is of dipyrone
title_full Spot-test identification and rapid quantitative sequential analys is of dipyrone
title_fullStr Spot-test identification and rapid quantitative sequential analys is of dipyrone
title_full_unstemmed Spot-test identification and rapid quantitative sequential analys is of dipyrone
title_sort Spot-test identification and rapid quantitative sequential analys is of dipyrone
author Tubino, M.
author_facet Tubino, M.
Biondo, A. C.
Vila, M. M.D.C.
Pezza, L. [UNESP]
Pezza, H. R. [UNESP]
author_role author
author2 Biondo, A. C.
Vila, M. M.D.C.
Pezza, L. [UNESP]
Pezza, H. R. [UNESP]
author2_role author
author
author
author
dc.contributor.none.fl_str_mv Universidade Estadual de Campinas (UNICAMP)
UNISO
Universidade Estadual Paulista (UNESP)
dc.contributor.author.fl_str_mv Tubino, M.
Biondo, A. C.
Vila, M. M.D.C.
Pezza, L. [UNESP]
Pezza, H. R. [UNESP]
dc.subject.por.fl_str_mv Analysis
Dipyrone
Qualitative
Quantitative
Spot-test
topic Analysis
Dipyrone
Qualitative
Quantitative
Spot-test
description A qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drug and in pharmaceutical preparations is proposed. The formation of a reddish-violet color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian Pharmacopoeia, using the Student fst and the F tests. Considering the concentration in a 100 μL aliquot, the qualitative visual limit of detection is about (Formula Presented) instrumental (Formula Presented)
publishDate 2010
dc.date.none.fl_str_mv 2010-01-01
2022-04-28T19:45:55Z
2022-04-28T19:45:55Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.26850/1678-4618EQJ.V35.1.2010.P41-46
Ecletica Quimica, v. 35, n. 1, p. 41-46, 2010.
1678-4618
0100-4670
http://hdl.handle.net/11449/222640
10.26850/1678-4618EQJ.V35.1.2010.P41-46
2-s2.0-85117034255
url http://dx.doi.org/10.26850/1678-4618EQJ.V35.1.2010.P41-46
http://hdl.handle.net/11449/222640
identifier_str_mv Ecletica Quimica, v. 35, n. 1, p. 41-46, 2010.
1678-4618
0100-4670
10.26850/1678-4618EQJ.V35.1.2010.P41-46
2-s2.0-85117034255
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Ecletica Quimica
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 41-46
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv
_version_ 1803045795121856512

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