Spot-test identification and rapid quantitative sequential analys is of dipyrone
Autor(a) principal: | |
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Data de Publicação: | 2010 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://dx.doi.org/10.26850/1678-4618EQJ.V35.1.2010.P41-46 http://hdl.handle.net/11449/222640 |
Resumo: | A qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drug and in pharmaceutical preparations is proposed. The formation of a reddish-violet color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian Pharmacopoeia, using the Student fst and the F tests. Considering the concentration in a 100 μL aliquot, the qualitative visual limit of detection is about (Formula Presented) instrumental (Formula Presented) |
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Repositório Institucional da UNESP |
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Spot-test identification and rapid quantitative sequential analys is of dipyroneAnalysisDipyroneQualitativeQuantitativeSpot-testA qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drug and in pharmaceutical preparations is proposed. The formation of a reddish-violet color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian Pharmacopoeia, using the Student fst and the F tests. Considering the concentration in a 100 μL aliquot, the qualitative visual limit of detection is about (Formula Presented) instrumental (Formula Presented)State University of Campinas - UNICAMP Institute of Chemistry, P.O. Box 6154, SPSorocaba University UNISO, SPSão Paulo State University- UNESP Chemistry Institute of Araraquara, SPSão Paulo State University- UNESP Chemistry Institute of Araraquara, SPUniversidade Estadual de Campinas (UNICAMP)UNISOUniversidade Estadual Paulista (UNESP)Tubino, M.Biondo, A. C.Vila, M. M.D.C.Pezza, L. [UNESP]Pezza, H. R. [UNESP]2022-04-28T19:45:55Z2022-04-28T19:45:55Z2010-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article41-46http://dx.doi.org/10.26850/1678-4618EQJ.V35.1.2010.P41-46Ecletica Quimica, v. 35, n. 1, p. 41-46, 2010.1678-46180100-4670http://hdl.handle.net/11449/22264010.26850/1678-4618EQJ.V35.1.2010.P41-462-s2.0-85117034255Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengEcletica Quimicainfo:eu-repo/semantics/openAccess2022-04-28T19:45:55Zoai:repositorio.unesp.br:11449/222640Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T13:47:00.102955Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Spot-test identification and rapid quantitative sequential analys is of dipyrone |
title |
Spot-test identification and rapid quantitative sequential analys is of dipyrone |
spellingShingle |
Spot-test identification and rapid quantitative sequential analys is of dipyrone Tubino, M. Analysis Dipyrone Qualitative Quantitative Spot-test |
title_short |
Spot-test identification and rapid quantitative sequential analys is of dipyrone |
title_full |
Spot-test identification and rapid quantitative sequential analys is of dipyrone |
title_fullStr |
Spot-test identification and rapid quantitative sequential analys is of dipyrone |
title_full_unstemmed |
Spot-test identification and rapid quantitative sequential analys is of dipyrone |
title_sort |
Spot-test identification and rapid quantitative sequential analys is of dipyrone |
author |
Tubino, M. |
author_facet |
Tubino, M. Biondo, A. C. Vila, M. M.D.C. Pezza, L. [UNESP] Pezza, H. R. [UNESP] |
author_role |
author |
author2 |
Biondo, A. C. Vila, M. M.D.C. Pezza, L. [UNESP] Pezza, H. R. [UNESP] |
author2_role |
author author author author |
dc.contributor.none.fl_str_mv |
Universidade Estadual de Campinas (UNICAMP) UNISO Universidade Estadual Paulista (UNESP) |
dc.contributor.author.fl_str_mv |
Tubino, M. Biondo, A. C. Vila, M. M.D.C. Pezza, L. [UNESP] Pezza, H. R. [UNESP] |
dc.subject.por.fl_str_mv |
Analysis Dipyrone Qualitative Quantitative Spot-test |
topic |
Analysis Dipyrone Qualitative Quantitative Spot-test |
description |
A qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drug and in pharmaceutical preparations is proposed. The formation of a reddish-violet color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian Pharmacopoeia, using the Student fst and the F tests. Considering the concentration in a 100 μL aliquot, the qualitative visual limit of detection is about (Formula Presented) instrumental (Formula Presented) |
publishDate |
2010 |
dc.date.none.fl_str_mv |
2010-01-01 2022-04-28T19:45:55Z 2022-04-28T19:45:55Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.26850/1678-4618EQJ.V35.1.2010.P41-46 Ecletica Quimica, v. 35, n. 1, p. 41-46, 2010. 1678-4618 0100-4670 http://hdl.handle.net/11449/222640 10.26850/1678-4618EQJ.V35.1.2010.P41-46 2-s2.0-85117034255 |
url |
http://dx.doi.org/10.26850/1678-4618EQJ.V35.1.2010.P41-46 http://hdl.handle.net/11449/222640 |
identifier_str_mv |
Ecletica Quimica, v. 35, n. 1, p. 41-46, 2010. 1678-4618 0100-4670 10.26850/1678-4618EQJ.V35.1.2010.P41-46 2-s2.0-85117034255 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Ecletica Quimica |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
41-46 |
dc.source.none.fl_str_mv |
Scopus reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1808128275380174848 |